• Title/Summary/Keyword: micro-voids

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Evaluation of homogenized thermal conductivities of imperfect carbon-carbon textile composites using the Mori-Tanaka method

  • Vorel, Jan;Sejnoha, Michal
    • Structural Engineering and Mechanics
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    • v.33 no.4
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    • pp.429-446
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    • 2009
  • Three-scale homogenization procedure is proposed in this paper to provide estimates of the effective thermal conductivities of porous carbon-carbon textile composites. On each scale - the level of fiber tow (micro-scale), the level of yarns (meso-scale) and the level of laminate (macro-scale) - a two step homogenization procedure based on the Mori-Tanaka averaging scheme is adopted. This involves evaluation of the effective properties first in the absence of pores. In the next step, an ellipsoidal pore is introduced into a new, generally orthotropic, matrix to make provision for the presence of crimp voids and transverse and delamination cracks resulting from the thermal transformation of a polymeric precursor into the carbon matrix. Other sources of imperfections also attributed to the manufacturing processes, including non-uniform texture of the reinforcements, are taken into consideration through the histograms of inclination angles measured along the fiber tow path together with a particular shape of the equivalent ellipsoidal inclusion proposed already in Sko ek (1998). The analysis shows that a reasonable agreement of the numerical predictions with experimental measurements can be achieved.

Novel Preparation of Epoxy/Silica Nanocomposite Using Si-N Precursor (Si-N 전구체를 이용한 에폭시/실리카 나노복합재료의 제조)

  • Kim Lee Ju;Yoon Ho Gyu;Lee Sang-Soo;Kim Junkyung
    • Polymer(Korea)
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    • v.28 no.5
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    • pp.391-396
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    • 2004
  • In order to overcome drawbacks in the conventional preparation of epoxy/silica nanocomposites, such as formation of micro voids and dimensional instability caused by evolution of volatile by-products during curing reaction, a novel preparation method using Si-N precursor has been proposed. When prepared through in-situ reaction of epoxy curing reaction with sol-gel reaction of Si-N precursor, methyltripiperidinylsilane (MTPS) which does not produce by-products during reaction, epoxy/silica nanocomposites of extremely even dispersion of inorganic phase could be successfully prepared, resulting in high enhancement of mechanical and thermal properties as well as outstanding transparency.

Free vibration of imperfect sigmoid and power law functionally graded beams

  • Avcar, Mehmet
    • Steel and Composite Structures
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    • v.30 no.6
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    • pp.603-615
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    • 2019
  • In the present work, free vibration of beams made of imperfect functionally graded materials (FGMs) including porosities is investigated. Because of faults during process of manufacture, micro voids or porosities may arise in the FGMs, and this situation causes imperfection in the structure. Therefore, material properties of the beams are assumed to vary continuously through the thickness direction according to the volume fraction of constituents described with the modified rule of mixture including porosity volume fraction which covers two types of porosity distribution over the cross section, i.e., even and uneven distributions. The governing equations of power law FGM (P-FGM) and sigmoid law FGM (S-FGM) beams are derived within the frame works of classical beam theory (CBT) and first order shear deformation beam theory (FSDBT). The resulting equations are solved using separation of variables technique and assuming FG beams are simply supported at both ends. To validate the results numerous comparisons are carried out with available results of open literature. The effects of types of volume fraction function, beam theory and porosity volume fraction, as well as the variations of volume fraction index, span to depth ratio and porosity volume fraction, on the first three non-dimensional frequencies are examined in detail.

Nonlocal free vibration analysis of porous FG nanobeams using hyperbolic shear deformation beam theory

  • Hadji, Lazreg;Avcar, Mehmet
    • Advances in nano research
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    • v.10 no.3
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    • pp.281-293
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    • 2021
  • This paper presents a new nonlocal Hyperbolic Shear Deformation Beam Theory (HSDBT) for the free vibration of porous Functionally Graded (FG) nanobeams. A new displacement field containing integrals is proposed which involves only three variables. The present model incorporates the length scale parameter (nonlocal parameter) which can capture the small scale effect and its account for shear deformation by a hyperbolic variation of all displacements through the thickness without using the shear correction factor. It has been observed that during the manufacture of Functionally Graded Materials (FGMs), micro-voids and porosities can occur inside the material. Thus, in this work, the investigation of the free vibration analysis of FG beams taking into account the influence of these imperfections is established. Four different porosity types are considered for FG nanobeam. Material characteristics of the FG beam are supposed to vary continuously within thickness direction according to a power-law scheme which is modified to approximate material characteristics for considering the influence of porosities. Based on the nonlocal differential constitutive relations of Eringen, the equations of motion of the nanobeam are derived using Hamilton's principle. The effects of nonlocal parameter, aspect ratio, and the porosity types on the dynamic responses of the nanobeam are discussed.

Scanning acoustic microscopy for material evaluation

  • Hyunung Yu
    • Applied Microscopy
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    • v.50
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    • pp.25.1-25.11
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    • 2020
  • Scanning acoustic microscopy (SAM) or Acoustic Micro Imaging (AMI) is a powerful, non-destructive technique that can detect hidden defects in elastic and biological samples as well as non-transparent hard materials. By monitoring the internal features of a sample in three-dimensional integration, this technique can efficiently find physical defects such as cracks, voids, and delamination with high sensitivity. In recent years, advanced techniques such as ultrasound impedance microscopy, ultrasound speed microscopy, and scanning acoustic gigahertz microscopy have been developed for applications in industries and in the medical field to provide additional information on the internal stress, viscoelastic, and anisotropic, or nonlinear properties. X-ray, magnetic resonance, and infrared techniques are the other competitive and widely used methods. However, they have their own advantages and limitations owing to their inherent properties such as different light sources and sensors. This paper provides an overview of the principle of SAM and presents a few results to demonstrate the applications of modern acoustic imaging technology. A variety of inspection modes, such as vertical, horizontal, and diagonal cross-sections have been presented by employing the focus pathway and image reconstruction algorithm. Images have been reconstructed from the reflected echoes resulting from the change in the acoustic impedance at the interface of the material layers or defects. The results described in this paper indicate that the novel acoustic technology can expand the scope of SAM as a versatile diagnostic tool requiring less time and having a high efficiency.

Vibrational behavior of porous composite laminated plates using four unknown integral shear deformation theory

  • Hayat Saidi;Abdelouahed Tounsi;Fouad Bourada;Abdelmoumen Anis Bousahla;Abdeldjebbar Tounsi;Firas Ismail Salman Al-Juboori
    • Steel and Composite Structures
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    • v.52 no.3
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    • pp.249-271
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    • 2024
  • In this scientific work, an analytical solution for the dynamic analysis of cross-ply and angle-ply laminated composite plates is proposed. Due to technical issues during the manufacturing of composite materials, porosities and micro-voids can be produced within the composite material samples, which can carry on to a reduction in the density and strength of the materials. In this research, the laminated composite plates are assumed to have new distributions of porosities over the plate cross-section. The structure is modeled using a simple integral shear deformation theory in which the transverse shear deformation effect is included. The governing equations of motion are obtained employing the principle of Hamilton's. The solution is determined via Navier's approach. The Maple program is used to obtain the numerical results. In the numerical examples, the effects of geometry, ratio, modulus ratio, fiber orientation angle, number of layers and porosity parameter on the natural frequencies of symmetric and anti-symmetric laminated composite plates is presented and discussed in detail. Also, the impacts of the kinds of porosity distribution models on the natural frequencies of symmetric and anti-symmetric laminated composite plates are investigated.

Study on the Thermal Characteristics of Concrete Using Micro Form Admixture (마이크로기포제를 사용한 콘크리트의 열적 특성에 관한 연구)

  • Park, Young Shin;Kim, Jung Ho;Jeon, Hyun Kyu;Seo, Chee Ho
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.101-109
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    • 2013
  • Recently, it is certain that the increase of heating and cooling energy consumption by radical change in climate condition has caused serious problems related to environmental and energy concerns associated with increase of fossil fuel usage and carbon dioxide production as well as global warming. So, various actions to reduce greenhouse gas exhaustion and energy consumption have been prepared by world developed countries. Our government has also been trying to seek energy control methods for houses and buildings by proclaiming political polices on low-carbon green growth and construction and performance standards for environment-friendly housing. The energy consumption by buildings approximately reaches 25% of total korea energy consumption, and the increasing rate of energy consumption by buildings is stiffer than the rate by the other industries. The greatest part in the buildings of the energy consumption is building facade. While lots of research projects for reducing energy consumption of the facade have been conducted, but a few research projects on concrete comprising more than 70% of outsider of buildings has been tried. This research presents here a study to improve the insulation property of structural concrete formed by micro form admixture (MFA) with experimentally reviewing the physical, mechanical and thermal characteristics of the concrete. As the results of this experiment, in the case of concrete mixed with MFA, slump loss has been improved. As the mixing ratio of MFA increases, the compressive strength is decreased and thermal conductivity is increased. Also it was found that water-cement ratio increases, the compressive strength is decreased and thermal conductivity is increased. but, there was not big influence by the change of fine aggregate ratio.

Modeling and Analysis of Size-Dependent Structural Problems by Using Low-Order Finite Elements with Strain Gradient Plasticity (변형률 구배 소성 저차 유한요소에 의한 크기 의존 구조 문제의 모델링 및 해석)

  • Park, Moon-Shik;Suh, Yeong-Sung;Song, Seung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.9
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    • pp.1041-1050
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    • 2011
  • An elasto-plastic finite element method using the theory of strain gradient plasticity is proposed to evaluate the size dependency of structural plasticity that occurs when the configuration size decreases to micron scale. For this method, we suggest a low-order plane and three-dimensional displacement-based elements, eliminating the need for a high order, many degrees of freedom, a mixed element, or super elements, which have been considered necessary in previous researches. The proposed method can be performed in the framework of nonlinear incremental analysis in which plastic strains are calculated and averaged at nodes. These strains are then interpolated and differentiated for gradient calculation. We adopted a strain-gradient-hardening constitutive equation from the Taylor dislocation model, which requires the plastic strain gradient. The developed finite elements are tested numerically on the basis of typical size-effect problems such as micro-bending, micro-torsion, and micro-voids. With respect to the strain gradient plasticity, i.e., the size effects, the results obtained by using the proposed method, which are simple in their calculation, are in good agreement with the experimental results cited in previously published papers.

Mechanical Properties of Polypropylene/Talc Composites Prepared via Solid-State Extrusion (고상 압출된 폴리프로필렌/탈크 복합재료의 기계적 물성)

  • Lee, Jaechoon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
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    • v.17 no.4
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    • pp.131-135
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    • 2016
  • We investigated the specific gravity and mechanical property changes of solid-state extruded polypropylene (PP)/talc composites before and after orientation. The specific gravity of the composites increases with increasing the filler contents. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more micro-voids. It was found that the tensile properties of the composites are increased up to the talc content of 10 wt%, but after the contents exceeding 10 wt%, the tensile properties are decreased. For oriented specimens, the tensile strength of the composites showed monotonously decrease with increasing talc contents. When the contents of talc is 10 wt%, the theoretical values according to Halpin-Tsai equation are close to the experimental values but over 20 wt% of talc contents, the deviation of the experimental values from the theoretical prediction becomes higher. The maximum flexural strength and modulus were observed for PP/talc composites when the talc contents was 10 wt% for both pre-specimen and oriented specimen.

A Study of Properties of Sn-3Ag-0.5Cu Solder Based on Phosphorous Content of Electroless Ni-P Layer (Sn-3Ag-0.5Cu Solder에 대한 무전해 Ni-P층의 P함량에 따른 특성 연구)

  • Shin, An-Seob;Ok, Dae-Yool;Jeong, Gi-Ho;Kim, Min-Ju;Park, Chang-Sik;Kong, Jin-Ho;Heo, Cheol-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.6
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    • pp.481-486
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    • 2010
  • ENIG (electroless Ni immersion gold) is one of surface finishing which has been most widely used in fine pitch SMT (surface mount technology) and BGA (ball grid array) packaging process. The reliability for package bondability is mainly affected by interfacial reaction between solder and surface finishing. Since the behavior of IMC (intermetallic compound), or the interfacial reaction between Ni and solder, affects to some product reliabilities such as solderability and bondability, understanding behavior of IMC should be important issue. Thus, we studied the properties of ENIG with P contents (9 wt% and 13 wt%), where the P contents is one of main factors in formation of IMC layer. The effect of P content was discussed using the results obtained from FE-SEM(field-emission scanning electron microscope), EPMA(electron probe micro analyzer), EDS(energy dispersive spectroscopy) and Dual-FIB(focused ion beam). Especially, we observed needle type irregular IMC layer with decreasing Ni contents under high P contents (13 wt%). Also, we found how IMC layer affects to bondability with forming continuous Kirkendall voids and thick P-rich layer.