• 폴리머
• /
• 제38권1호
• /
• pp.98-102
• /
• 2014

실크 피브로인은 뛰어난 생체적합성 및 생분해성으로 인해 의료용 천연고분자소재로 각광받고 있으며 다양한 형태로 제조되어 이용되고 있다. 전기분사법은 고분자 용액에 고전압을 적용하여 미세입자를 제조하는 방법으로 진행과정이 간단하고 첨가제를 필요로 하지 않는다는 장점을 지닌다. 본 연구에서는 실크 피브로인 다공성 미세입자를 제조하기 위하여 폴리(에틸렌 글리콜)(PEG)을 첨가한 후 전기분사를 실시하였다. PEG를 첨가함으로써 분사원액의 전도도는 감소하였고 점도는 증가하였다. 제조된 미세입자의 크기는 PEG 첨가에 따라 감소하였는데 이는 분사용액의 전도도 및 점도보다는 피브로인과 PEG간의 상분리에 의한 효과인 것으로 보인다. 제조된 실크 피브로인 미세입자를 물에 침지한 결과 PEG가 제거되었으며 최종적으로 실크 피브로인 다공성 입자를 제조할 수 있었다. 제조된 다공성 실크 피브로인 미세입자는 약물전달체 및 조직공학용 세포전달체로 이용가능성이 높을 것으로 기대된다.

• Advances in nano research
• /
• 제5권4호
• /
• pp.281-301
• /
• 2017

In this disquisition, an exact solution method is developed for analyzing the vibration characteristics of magneto-electro-elastic functionally graded (MEE-FG) beams by considering porosity distribution and various boundary conditions via a four-variable shear deformation refined beam theory for the first time. Magneto-electroelastic properties of porous FG beam are supposed to vary through the thickness direction and are modeled via modified power-law rule which is formulated using the concept of even and uneven porosity distributions. Porosities possibly occurring inside functionally graded materials (FGMs) during fabrication because of technical problem that lead to creation micro-voids in FG materials. So, it is necessary to consider the effect of porosities on the vibration behavior of MEE-FG beam in the present study. The governing differential equations and related boundary conditions of porous MEE-FG beam subjected to physical field are derived by Hamilton's principle based on a four-variable tangential-exponential refined theory which avoids the use of shear correction factor. An analytical solution procedure is used to achieve the natural frequencies of porous-FG beam supposed to magneto-electrical field which satisfies various boundary conditions. A parametric study is led to carry out the effects of material graduation exponent, porosity parameter, external magnetic potential, external electric voltage, slenderness ratio and various boundary conditions on dimensionless frequencies of porous MEE-FG beam. It is concluded that these parameters play noticeable roles on the vibration behavior of MEE-FG beam with porosities. Presented numerical results can be applied as benchmarks for future design of MEE-FG structures with porosity phases.

• Corrosion Science and Technology
• /
• 제20권5호
• /
• pp.249-255
• /
• 2021

In this work, we proposed a facile method to fabricate the three-dimensional porous copper current collector (3D Cu CC) for a Si-dominant anode in a Li-ion battery (LiB). The 3D Cu CC was prepared by combining chemical etching and thermal reduction from a planar copper foil. It had a porous layer employing micro-sized Cu balls with a large surface area. In particular, it had strengthened attachment of Si-dominant active material on the CC compared to a planar 2D copper foil. Moreover, the increased contact area between a Si-dominant active material and the 3D Cu could minimize contact loss of active materials from a CC. As a result of a battery test, Si-dominant active materials on 3D Cu showed higher cyclic performance and rate-capability than those on a conventional planar copper foil. Specifically, the Si electrode employing 3D Cu exhibited an areal capacity of 0.9 mAh cm^-2 at the 300^th cycles (@ 1.0 mA cm^-2), which was 5.6 times higher than that on the 2D copper foil (0.16 mAh cm^-2).

• 접착 및 계면
• /
• 제19권4호
• /
• pp.163-166
• /
• 2018

이 딥펜 나노리소그라피(DPN)는 원자 힘 현미경(AFM)을 기반으로 하는 나노 및 마이크로 패턴 제조 기술이다. 다양한 잉크 물질을 AFM 탐침에 코팅하여 탐침과 기판 사이에 형성된 물 메니스커스를 통해 기판으로 전이시켜 패턴을 제조한다. 본 연구에서는, 실란 전처리된 AFM 탐침 표면에 불소 실란 잉크 용액을 코팅하고 하이드록시기로 개질된 실리콘 기판 위에 접촉시킨 후, DPN 기술을 이용하여 표면으로 잉크 물질을 전이시키는 연구를 진행하였다. HDFDTMS 잉크 물질의 dot 어레이 패턴을 안정적으로 제조하였으며, AFM 탐침과 기판 사이의 접촉시간에 따라 패턴 크기가 선형적으로 증가하는 전형적인 DPN의 확산 메커니즘을 보였다.

• 한국전자통신학회논문지
• /
• 제14권5호
• /
• pp.871-876
• /
• 2019

본 논문에서는 플루오린화 수소산(Hydrofluoric acid: HF) 수용액과 광섬유에 인가된 $1.55{\mu}m$ 파장의 레이저를 통해 유도된 광열 효과를 이용하여 오목한 광섬유 팁을 제작하였다. 제작 과정에서 인가한 레이저의 세기, 식각 시간, HF 수용액의 농도에 따른 광섬유 팁 오목 면의 곡률 반경을 광학 현미경을 이용하여 측정하였으며 곡률 반경이 세 변인에 대하여 어떻게 변화하는지 분석하였다. 또한, Free Spectral Range(FSR)와 Scanning electron microscope(SEM) 촬영을 통해 현미경을 이용한 측정 방법의 신뢰성을 검증하였다. 본 논문을 통해 광섬유 팁의 오목 면 제작 과정에서 변인에 따라 곡률 반경을 조절할 수 있게 됨으로써 기존의 HF 수용액을 이용한 광섬유 식각 방법의 한계점을 극복할 수 있었다.

• 한국기계가공학회지
• /
• 제20권2호
• /
• pp.107-119
• /
• 2021

The cross-flow turbine is one of the most famous and widely used hydraulic power systems for a long time. The cross-flow turbine is especially popular in many countries and remote regions where off-grided because of its many benefits such as low cost, high efficiency at low head, simple structure, and easy maintenance. However, most modern turbines, including the cross-flow turbine, are unsuitable for the ultra-low head situation, known as less than 3m water head or zero head with over 0.5m/s flow velocity. In this study, we demonstrated a 20kW class inverted-type cross-flow turbine's performance. First, we reevaluated our previous studies and introduced how to design the inverted-type cross-flow turbine. Secondly, we fabricated the 20kW class inverted-type cross-flow turbine for the performance test. And then, we designed a testbed and installed the turbine system in the demonstration facility. In the end, we compare the demonstration with its previous CFD results. The comparing result shows that both CFD and real model fitted on guide vane angle at 10 degrees. At the demonstration, we achieved 42% turbine efficiency at runner speed 125 RPM.

• 대한금속재료학회지
• /
• 제50권11호
• /
• pp.861-866
• /
• 2012

A dense nanostructured TiN-AlN composite was prepared from high-energy ball milled TiN-AlN mixture powders by pulsed current activated sintering (PCAS). A highly dense TiN-AlN bulk composite was obtained within 2 minutes at $1500^{\circ}C$ with the simultaneous application of 80 MPa pressure and pulsed current. The fine crystalline structure of the TiN-AlN mixture, which was obtained by high-energy milling, was effectively maintained during PCAS and resulted in the enhancement of the mechanical properties. The micro hardness and fracture toughness of TiN-AlN composite were $1780kg/mm^2$ and $5MPa.m^{1/2}$, respectively. The mechanical properties were higher than monolithic AlN or TiN.

• 한국전기전자재료학회논문지
• /
• 제35권1호
• /
• pp.18-23
• /
• 2022

이젯 프린팅은 직접적인 비접촉 마이크로 팹기술의 하나로서 노즐과 기판 사이에 강한 전기장을 가함으로써 넓은 범위의 마이크로/나노패턴 어레이를 구현할 수 있는 다목적 팹공정이다. 제조된 고분자/퀀텀닷 마이이크로 패턴의 모양과 두께는 자동화된 프린트 기계에 설치된 노즐 직경과 공정에 사용된 잉크 성분에 일반적으로 정밀한 의존성을 갖는다. 본 논문의 목적은 실험 결과에 영향을 미칠 수 있는 각각의 공정 변수 효과를 설명하기 위해서 이젯 프린팅된 고분자/퀀텀닷의 전형적인 실제 예를 설명하는데 있다. 여기서 우리는 마이크로/나노 해상도로 두께가 정밀하게 제어된 고분자/퀀텀닷 패턴을 제조할 수 있는 몇 가지 이젯 프린팅 공정을 구현하였다.

• Tribology and Lubricants
• /
• 제38권5호
• /
• pp.185-190
• /
• 2022

Among the operating limits of a heat pipe, the capillary limit is significantly affected by the characteristics of the wick, which is determined by the capillary performance. The major parameters for determining capillary performance are the maximum capillary pressure and the spreading characteristics that can be expected through the wick. A well-designed wick structure improves capillary performance and helps improve the stability of the heat pipe by enhancing the capillary limit. The capillary performance can be improved by forming a porous microstructure on the surface of the wick structure through surface modification techniques. In this study, a microstructure is formed on the surface of the wick by using a surface modification method (i.e., an electrochemical etching process). In the experiment, specimens are prepared using stainless-steel screen mesh wicks with various fabrication conditions. In addition, the spreading and capillary rise performances are observed with low-surface-tension fluid to quantify the capillary performance. In the experiments, the capillary performance, such as spreading characteristics, maximum capillary pressure, and capillary rise rate, improves in the specimens with microstructures formed through surface modification compared with the specimens without microstructures on the surface. The improved capillary performance can have a positive effect on the capillary limit of the heat pipe. It is believed that the surface microstructures can enhance the operational stability of heat pipes.

• 한국염색가공학회지
• /
• 제35권4호
• /
• pp.239-245
• /
• 2023

Cellulose is an abundant biodegradable material in nature with excellent properties, but due to its poor processability, it has been widely studied for processing through modification. Cellulose acetate propionate (CAP) is a cellulose derivative in which the hydroxyl group of cellulose is replaced by acetyl and propionyl groups. CAP has several advantages, such as excellent solubility, structural stability, light and weather resistance, and good transparency. Porous nanofibers with excellent specific surface area, which can be applied in various fields, can be easily formed by the phase separation method using highly volatile solvents. High speed centrifugal spinning is a nano/micro fiber preparation method with advantages such as fast spinning and easy alignment control. In this study, a CAP/polybutylene succinate (PBS) spinning solution with chloroform as solvent was prepared to prepare porous microfibers and the fiber morphology was examined as a function of the disk rotation speed in an high speed centrifugal spinning device.