• Current Optics and Photonics
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• v.3 no.6
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• pp.577-582
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• 2019

We report on a continuous-wave (cw) optical parametric oscillator (OPO) optimized for mid-infrared emission above 5.0 ㎛. The OPO is based on a magnesium-oxide-doped periodically poled LiNbO₃(MgO:PPLN) crystal with a fan-out grating design. A linear two-mirror cavity resonating both at the pump and signal wavelengths is stabilized to the pump laser by using the modified Pound-Drever-Hall (PDH) method. The idler wavelength is continuously tunable from 4.7 ㎛ up to 5.3 ㎛ by varying the poling period of the fan-out grating crystal. Pumped by a diode-pumped solid state (DPSS) laser with a power of 1.1 W at 1064 nm, the maximum idler output power is measured to be 5.3 mW at 4.8 ㎛. The output power above 5.0 ㎛ is reduced to the hundreds of ㎼ level due to increased absorption in the crystal, but is stable and strong enough to be measured with a conventional detector.

• Journal of Sensor Science and Technology
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• v.14 no.6
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• pp.395-401
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• 2005

A highly stable quartz crystal microbalance (QCM) that showed a stability of frequencies and exhibited a very low noise level has been developed. The long-term drift was <0.05 Hz/h over a period of 10 h, and the short-term rms (root mean square) noise was <0.015 Hz. Our QCM sensor was used as a humidity sensor employing a poly(methyl methacrylate) (PMMA) polymer film as a hygroscopic layer, which showed good characteristics in the relative humidity (RH) range of $2{\sim}90%$ RH. Comparing the characteristics of the QCM sensor with those of other types of humidity sensors employing PMMA film as a hygroscopic layer, and with other QCM sensors employing other hygroscopic layers is represented.

• Journal of Sensor Science and Technology
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• v.18 no.2
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• pp.116-121
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• 2009

Pressure-controlled sodium heat pipe furnace was designed and fabricated, and its characteristics was investigated. Pressure control system was controlled within ${\pm}0.5\;Pa$ at 150 kPa and the stability of pressure was decreased to ${\pm}2.5\;Pa$, when the pressure-controlled system connected with the heat pipe. The melting curve of Ag fixed-point realized well by the adiabatic method using the pressure-controlled sodium heat pipe furnace and its accuracy showed ${\pm}2.27\;mK$ from the calculation of 20% to 80% at the plateau. The freezing curve of Ag fixed-point also realized and its plateau value was 2.23 mK lower than that of the melting curve.

• Journal of the Korean Society for Precision Engineering
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• v.32 no.2
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• pp.185-190
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• 2015

This paper presents a new method to determine sensitivity coefficients of temperature and humidity of torque transducers by using a natural and seasonal variation of ambient conditions at the laboratory. We had measured the sensitivities of the torque transducers over almost one year using the KRISS 2 kN m torque standard machine. The sensitivity data acquired at various ambient conditions were processed using our measurement model to extract the sensitivity coefficients of temperature and humidity simultaneously with high precision. A comparison with a previous method using an environmental control chamber was carried out to test the feasibility of using our new method. Two results agreed within the uncertainty. We revealed that the torque measuring errors could be 8 times higher than the measurement and calibration capability of KRISS torque standard machine if the sensitivity changes due to the temperature and humidity are not properly corrected during a calibration.

• Analytical Science and Technology
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• v.12 no.4
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• pp.332-340
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• 1999

Homemade cryogenic preconcentration system is constructed to preconcentrate the VOCs in the ambient air collected in canister. Homemade preconcentrator equipped with GC-MS was used for analysis of air sample containing VOCs at ppb level identified in EPA TO-14 method. The system was evaluated for analytical performance by comparison with the results of adsorption tube method widely used in the past, and shows good agreement for concentrations of benzene, toluene, ethylbenzene, and xylenes.

• Journal of Sensor Science and Technology
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• v.13 no.6
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• pp.405-410
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• 2004

Compensation wires for Pt/Pd thermocouple was manufactured using Cu/Ni alloys. Their thermoelectric voltage has been tested from room temperature to about $150^{\circ}C$. Alloys of $Cu_{95.5}Ni_{4.5}$ and $Cu_{89.5}Ni_{10.5}$ introduced only small emf differences to Pt/Pd thermocouples, indicating a real possibility of industrial use. Above $1000^{\circ}C$, the temperature difference was expected to he small as ${\pm}0.5^{\circ}C$, and the difference would be minimized by adjusting the Ni content with a small amount.

• Bulletin of the Korean Chemical Society
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• v.28 no.8
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• pp.1383-1388
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• 2007

Recently, the semiconductor and display industries have tried to reduce the emissions of perfluorocompounds (PFCs) from the globally environmental regulation. Total amount of PFC emission can be calculated from the flow rate and the partial pressures of PFCs. For the precise measurement of PFC emission amount, the mass flow controlled helium gas was continuously injected into the equipment of which scrubber efficiency is being measured. The partial pressures of PFCs and helium were accurately measured using a mass spectrometer in each sample extracted from inlet and outlet of the scrubber system. The flow rates are calculated from the partial pressures of helium and also, PFC destruction and removal efficiency (DRE) of the scrubber is calculated from the partial pressure of PFC and the flow rate. Under this method, the relative expanded uncertainties of the flow rate and the partial pressures of PFCs are ± 2% (k = 2) in case the concentrations of NF3 and SF6 are as low as 100 μmol/mol.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.17 no.4 s.107
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• pp.387-392
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• 2006

In this paper, measurement scheme and uncertainty estimation of the K-band attenuation standard fitted with 3.5 mm coaxial connectors are described. The standard comprises a build-up chain of four steps of power ratio mea-surement and operates in the frequency range of 18 GHz to 26.5 GHz. The nominal attenuation of each step is around 20 dB and total dynamic range is 80 dB. The expanded uncertainty of the overall system is 0.01 dB at the confidence level of approximately 95%.

• Journal of Magnetics
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• v.16 no.3
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• pp.225-228
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• 2011

Magnetic properties and Rockwell hardness of 1Cr-0.5Mo steel have been investigated as a function of isothermal aging time. Our results showed that coercivity, hysteresis loss and Rockwell hardness in the aged samples decreased as aging time increased. This phenomenon was analyzed using optical microscopy and scanning electron microscopy. A significant diffusion of Cr and Mo atoms formed $M_2C$ and $M_7C$ carbides, lowering the matrix strength. $M_2C$ and $M_7C$ carbides partially segregated inside grains, diffused into grain boundaries, and finally resulted in a soft ferrite matrix and a hard grain boundary. The magnetic and mechanical softening of the matrix is likely to govern the properties of the sample more than the hardening of the grain boundary by carbide precipitations.

• Bulletin of the Korean Chemical Society
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• v.31 no.12
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• pp.3663-3667
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• 2010

Acetaminophen (N-acetyl-p-aminophenol) is one of the most popular analgesic and antipyretic drugs. An isotope dilution mass spectrometric method based on LC/MS was developed as a candidate reference method for the accurate determination of acetaminophen in pharmaceutical product. After spiking an isotope labeled acetaminophen (acetyl-$^{13}C_2$, $^{15}N$-acetaminophen) as an internal standard, tablet extracts were analyzed by LC/MS in a selected reaction monitoring (SRM) mode to detect ions at m/z $152{\rightarrow}110$ and m/z $155{\rightarrow}111$ for acetaminophen and acetyl-$^{13}C_2$, $^{15}N$-acetaminophen, respectively. The repeatability and reproducibility of the developed ID/LC-MS method were tested for the validation and assessment of metrological quality of the method.