• 열처리공학회지
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• 제14권5호
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• pp.275-281
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• 2001

To improve the reliability of hardness test results, Rockwell hardness round robin test was carried out for 10 laboratories. The test condition was the same with the ISO(International Standards Organization) standards. Korea Research Institute of Standards and Science(KRISS) supplied the hardness standard blocks and an indenter to laboratories for the measurement. The participating laboratories measured hardness of the specified areas on the blocks for 6 times with their own indenter as well as common indenter, respectively, and reported the results to KRISS. The result showed that quite large amount of the differences came from the indenter and it is necessary to change indenter with better quality for improved reliability in hardness measurement.

• 대한기계학회논문집A
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• 제37권12호
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• pp.1453-1463
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• 2013

본 연구에서는 유한요소해석과 압입시험으로 압입자 형상이 압입균열특성에 미치는 영향을 조사했다. 본 논문에서는 Lee 등(2012)이 제시한 cohesive zone 모델특성 및 균열생성, 진전을 위한 해석조건에 기초해 다양한 균열해석을 수행했다. 우선, 사각뿔 및 삼각뿔 압입균열 시험과 해석을 비교해 해석모델의 유효성을 검증했다. 아울러 비대칭 압입자에 의한 압입시, 압입하부에서 비대칭 균열의 발생여부를 해석적으로 관찰했다. 최종적으로 압입발생 균열수와 균열길이 관계를 조사했다. 균열수와 균열길이 관계 및 동일 압입자형상(압입자 모서리수)에서 압입자각에 따른 균열길이 변화를 이용하면, 특정 압입자 형태의 압입시험에서 얻은 균열길이 만으로 다양한 압입자 형태의 균열길이를 예측할 수 있다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집A
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• pp.256-261
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• 2000

In this study, we derived work-hardening exponent using continuous indentation test technique. Continuous indentation test technique is a powerful method to evaluate mechanical properties, such as hardness, modulus, ${\sigma}-{\varepsilon}$ curves and etc. It has many merits conventional indentation test has. The relationship between true stress and mean contact pressure and between strain and indentation depth were derived. While the indenter pushes the materials, the region around the indenter is deflected elastically. It is called elastic deflection. And pile-up phenomenon related to plastic deformation around the indenter increased the contact depth, and sink-in phenomenon decreases. So we calibrated contact depth change by considering elastic deflection and pile-up/sink-in. Using calibrated contact depth we redefined the relationship between true stress and mean contact pressure and between strain and contact depth. Through these relationship we could derive work-hardening exponent by analyzing load-depth curves. And it showed good agreement with tensile test results.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2003년도 춘계학술대회논문집
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• pp.111-115
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• 2003

Nanoindentation is simply an indentation test in which the length scale of the penetration is measured in nanometres rather than microns or millimetres, the latter being common in conventional hardness tests. Three-dimensional molecular dynamics simulations have been conducted to evaluate the nanoindentation test. Molecular dynamics simulations were carried out on single crystal copper by varying crystal orientations to investigate nano-behavior of material beneath an indenter in nanoindentation. Morse potential function was used as an interatomic force between indenter and thin film. The result of the simulation shows that crystal orientation significantly influenced the slip system, dislocation nucleation and dislocation behavior.

• 대한기계학회논문집A
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• 제32권1호
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• pp.35-42
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• 2008

본 연구에서는 원뿔형 압입자를 이용한 압입시험의 기초 유한요소해석으로부터 자기유사성을 나타내는 Kick's law 계수 C의 영향을 조사하고, 선단반경의 변화가 하중-변위 곡선에 미치는 영향을 회귀분석을 통해 살펴보았다. 아울러 항복강도와 변형경화지수 등의 변수들이 재료 영률평가에 미치는 영향을 분석하였다. 기존 영률 평가에 널리 사용되는 탄성이론에 기초한 Pharr 등의 식을 일반적인 탄소성 금속재료에 적용하기 위하여 다양한 재료에 대한 유한요소해석을 수행하였다. 재료 영률평가 시 압입자 선단반경과 압입깊이의 영향을 최소화하기 위해 Pharr 등의 식에 수정된 보정계수 k를 도입한 영률예측식을 제시하였다. 새로운 영률예측식은 텅스텐 카바이드와 다이아몬드 압입자일 때 모두 2%내의 평균 오차범위에서 각 재료의 영률을 평가할 수 있다.

• 한국정밀공학회지
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• 제21권3호
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• pp.139-146
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• 2004

In this study, to achieve the optimal conditions for mechanical hyper-fine pattern fabrication process, deformation behavior of the materials during indentation scratch test was studied with numerical method by ABAQUS S/W. Brittle materials (Si, Pyrex glass 7740) were used as specimens, and forming conditions to reduce the elastic recovery and pile-up were proposed. The indenter was modeled as a rigid surface. Minimum mesh sizes of specimens are 1-l0nm. Variables of the nanoindentation scratch test analysis are scratching speed, scratching load, tip radius and tip geometry. The nano-indentation scratch tests were performed by using the Berkovich pyramidal diamond indenter. Comparison between the experimental data and numerical result demonstrated that the FEM approach can be a good model of the nanoindentation scratch test. The result of the investigation will be applied to the fabrication of the hyper-fine pattern.

• 대한기계학회논문집A
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• 제38권9호
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• pp.943-951
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• 2014

마이크로/나노 압입시험에 사용되는 각뿔 혹은 원뿔형 압입자의 선단 형상은 제작한계 및 사용 중 마모 등으로 인해 필수적으로 곡면 형태를 띄게 된다. 많은 압입시험 관련 연구에서 각뿔형 압입자의 선단 형상은 편의상 구형으로 가정한 후, 얕은 압입에 대한 구형압입 이론식을 적용하고 있다. 이러한 가정에는 근본적으로 두 가지 문제점이 있는데, 첫 번째로 이론해의 정확성은 재료 물성치 및 압입자 형상에 따라 변화한다는 점이며, 두 번째로 각뿔형 압입자의 실제 선단 형상은 이상적인 구형이 아니라는 점이다. 본 연구에서는 유한요소해석에 기반하여 압입시험에 미치는 이 두 요소의 영향을 분석한다. 먼저 탄성 구형 압입시험에 대해 푸아송비와 하중-변위 곡선의 상관관계를 살펴보고, 이를 기반으로 수정된 구형 탄성 압입 관계식을 제시한다. 이어 가정된 Berkovich 선단 형상의 3차원 유한요소해석으로부터 압입깊이에 따른 하중-변위 곡선의 특성을 분석한다.

• 열처리공학회지
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• 제14권6호
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• pp.336-344
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• 2001

For the establishment of the world wide unified scales of the Rockwell hardness test with conical indenters, round robin test was carried from 1998 to 2000. The pilot laboratory was MPA-NRW and 12 laboratories from 11 countries participated In this RRT. Rockwell hardness of 74 specially prepared blocks was measured for the scales of C, A, D, 45N, 30N, and 15N and the results were compared. It was found that the geometric form of indenter affects on the results very significantly and standardization in the measurement and evaluation of indenter should be established in short time for the reliable hardness measurement. KRISS showed good results in general for all of the ranges except 15N scale which showed relatively large difference compare to the mean value. It was concluded that poor control in loading velocity of the dash pot was the major reason.

• 전기학회논문지
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• 제60권11호
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• pp.2088-2092
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• 2011

The accelerated thermal aging of CSPE(chloro sulfonate polyethylene) of test cables were carried out for the period equal to 10, 20 and 30 years in air at $100^{\circ}C$, respectively. The CSPE cables(TAIHAN electric wire Co. Ltd) which installed in nuclear power plant for three years were used as starting materials. Condition monitering methods of the accelerated thermal aging of CSPE cables were estimated through indenter modulus and OIT(oxidation induction time) of IEC 62582, and those were newly estimated through volume electrical resistivity, ultrasound reflection time, density, FE-SEM(field emission scanning electron microscopy), XPS(x-ray photoelectron spectroscopy), EDS(energy dispersive spectroscopy), and WD-XRF(wavelength dispersive x-ray fluorescence). A new condition monitoring methods of the accelerated thermal aging of CSPE cables were generally coincident with trend of indenter modulus expect EDS, XPS and XRF. A volume electrical resistivity among new condition monitoring methods of the accelerated thermal aging of CSPE cables is excellent. It is considered that life-time of CSPE cable can be predicted through volume electrical resistivity, if CSPE jacket was aged for period such as more than 20 years.

• Corrosion Science and Technology
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• 제20권6호
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• pp.484-490
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• 2021

Instrumented indentation testing has been widely used for residual stress measurement. The Knoop indentation is mainly selected for determining anisotropic mechanical properties and non-equibiaxial residual stress. However, the measurement of equibiaxial stress state and compressive residual stress on a specimen surface using Knoop indentation is neither fully comprehended nor unavailable. In this study, we investigated stress conversion factors for measuring Knoop indentation on equibiaxial stress state through indentation depth using finite element analysis. Knoop indentation was conducted for specimens to determine tensile and compressive equibiaxial residual stress. Both were found to be increased proportionally according to indentation depth. The stress field beneath the indenter during each indentation test was also analyzed. Compressive residual stress suppressed the in-plane expansion of stress field during indentation. In contrast, stress fields beneath the indenter developed diagonally downward for tensile residual stress. Furthermore, differences between trends of stress fields at long and short axes of Knoop indenter were observed due to difference in indenting angles and the projected area of plastic zone that was exposed to residual stress.