• Journal of the Korean Society for Heat Treatment
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• v.14 no.5
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• pp.275-281
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• 2001

To improve the reliability of hardness test results, Rockwell hardness round robin test was carried out for 10 laboratories. The test condition was the same with the ISO(International Standards Organization) standards. Korea Research Institute of Standards and Science(KRISS) supplied the hardness standard blocks and an indenter to laboratories for the measurement. The participating laboratories measured hardness of the specified areas on the blocks for 6 times with their own indenter as well as common indenter, respectively, and reported the results to KRISS. The result showed that quite large amount of the differences came from the indenter and it is necessary to change indenter with better quality for improved reliability in hardness measurement.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.12
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• pp.1453-1463
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• 2013

In this study, we investigated the effect of the indenter geometry on the crack characteristics by indentation cracking test and FEA. We conducted various cohesive finite element simulations based on the findings of Lee et al. (2012), who examined the effect of cohesive model parameters on crack size and formulated conditions for crack initiation and propagation. First, we verified the FE model through comparisons with experimental results that were obtained from Berkovich and Vickers indentations. We observed whether nonsymmetrical cracks formed beneath the surface during Berkovich indentation via FEA. Finally, we examined the relation between the crack size and the number of cracks. Based on this relation and the effect of the indenter angle on the crack size, we can predict from the crack size obtained with an indenter of one shape (such as Berkovich or Vickers) the crack size for an indenter of different shape.

• Proceedings of the KSME Conference
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• 2000.11a
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• pp.256-261
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• 2000

In this study, we derived work-hardening exponent using continuous indentation test technique. Continuous indentation test technique is a powerful method to evaluate mechanical properties, such as hardness, modulus, ${\sigma}-{\varepsilon}$ curves and etc. It has many merits conventional indentation test has. The relationship between true stress and mean contact pressure and between strain and indentation depth were derived. While the indenter pushes the materials, the region around the indenter is deflected elastically. It is called elastic deflection. And pile-up phenomenon related to plastic deformation around the indenter increased the contact depth, and sink-in phenomenon decreases. So we calibrated contact depth change by considering elastic deflection and pile-up/sink-in. Using calibrated contact depth we redefined the relationship between true stress and mean contact pressure and between strain and contact depth. Through these relationship we could derive work-hardening exponent by analyzing load-depth curves. And it showed good agreement with tensile test results.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.111-115
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• 2003

Nanoindentation is simply an indentation test in which the length scale of the penetration is measured in nanometres rather than microns or millimetres, the latter being common in conventional hardness tests. Three-dimensional molecular dynamics simulations have been conducted to evaluate the nanoindentation test. Molecular dynamics simulations were carried out on single crystal copper by varying crystal orientations to investigate nano-behavior of material beneath an indenter in nanoindentation. Morse potential function was used as an interatomic force between indenter and thin film. The result of the simulation shows that crystal orientation significantly influenced the slip system, dislocation nucleation and dislocation behavior.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.1
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• pp.35-42
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• 2008

Instrumented sharp indentation test is a well-directed method to measure hardness and elastic modulus. The sharp indenter such as Berkovich and conical indenters have a geometrical self-similarity in theory, but the self-similarity ceases to work in practice due to inevitable indenter tip-blunting. In this study we analyzed the load-depth curves of conical indenter with finite tip-radius via finite element method. Using the numerical regression data obtained from Kick's law, we first confirmed that loading curvature is significantly affected by tip radius as well as material properties. We then established a new method to evaluate Young's modulus, which successfully provides the value of elastic modulus with an average error of less than 2%, regardless of tip-radius and material properties of both indenter and specimen.

• Journal of the Korean Society for Precision Engineering
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• v.21 no.3
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• pp.139-146
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• 2004

In this study, to achieve the optimal conditions for mechanical hyper-fine pattern fabrication process, deformation behavior of the materials during indentation scratch test was studied with numerical method by ABAQUS S/W. Brittle materials (Si, Pyrex glass 7740) were used as specimens, and forming conditions to reduce the elastic recovery and pile-up were proposed. The indenter was modeled as a rigid surface. Minimum mesh sizes of specimens are 1-l0nm. Variables of the nanoindentation scratch test analysis are scratching speed, scratching load, tip radius and tip geometry. The nano-indentation scratch tests were performed by using the Berkovich pyramidal diamond indenter. Comparison between the experimental data and numerical result demonstrated that the FEM approach can be a good model of the nanoindentation scratch test. The result of the investigation will be applied to the fabrication of the hyper-fine pattern.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.38 no.9
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• pp.943-951
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• 2014

The tip geometries of the pyramidal and conical indenters used for micro/nano-indentation tests are not sharp. They are inevitably rounded because of their manufacturability and wear. In many indentation studies, the tip geometries of the pyramidal indenters are simply assumed to be spherical, and the theoretical solution for spherical indentation is simply applied to the geometry at a shallow indentation depth. This assumption, however, has two problems. First, the accuracy of the theoretical solution depends on the material properties and indenter shape. Second, the actual shapes of pyramidal indenter tips are not perfectly spherical. Hence, we consider the effects of these two problems on indentation tests via finite element analysis. We first show the relationship between the Poisson's ratio and load-displacement curve for spherical indentation, and suggest improved solutions. Then, using a possible geometry for a Berkovich indenter tip, we analyze the characteristics of the load-displacement curve with respect to the indentation depth.

• Journal of the Korean Society for Heat Treatment
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• v.14 no.6
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• pp.336-344
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• 2001

For the establishment of the world wide unified scales of the Rockwell hardness test with conical indenters, round robin test was carried from 1998 to 2000. The pilot laboratory was MPA-NRW and 12 laboratories from 11 countries participated In this RRT. Rockwell hardness of 74 specially prepared blocks was measured for the scales of C, A, D, 45N, 30N, and 15N and the results were compared. It was found that the geometric form of indenter affects on the results very significantly and standardization in the measurement and evaluation of indenter should be established in short time for the reliable hardness measurement. KRISS showed good results in general for all of the ranges except 15N scale which showed relatively large difference compare to the mean value. It was concluded that poor control in loading velocity of the dash pot was the major reason.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.60 no.11
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• pp.2088-2092
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• 2011

The accelerated thermal aging of CSPE(chloro sulfonate polyethylene) of test cables were carried out for the period equal to 10, 20 and 30 years in air at $100^{\circ}C$, respectively. The CSPE cables(TAIHAN electric wire Co. Ltd) which installed in nuclear power plant for three years were used as starting materials. Condition monitering methods of the accelerated thermal aging of CSPE cables were estimated through indenter modulus and OIT(oxidation induction time) of IEC 62582, and those were newly estimated through volume electrical resistivity, ultrasound reflection time, density, FE-SEM(field emission scanning electron microscopy), XPS(x-ray photoelectron spectroscopy), EDS(energy dispersive spectroscopy), and WD-XRF(wavelength dispersive x-ray fluorescence). A new condition monitoring methods of the accelerated thermal aging of CSPE cables were generally coincident with trend of indenter modulus expect EDS, XPS and XRF. A volume electrical resistivity among new condition monitoring methods of the accelerated thermal aging of CSPE cables is excellent. It is considered that life-time of CSPE cable can be predicted through volume electrical resistivity, if CSPE jacket was aged for period such as more than 20 years.

• Corrosion Science and Technology
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• v.20 no.6
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• pp.484-490
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• 2021

Instrumented indentation testing has been widely used for residual stress measurement. The Knoop indentation is mainly selected for determining anisotropic mechanical properties and non-equibiaxial residual stress. However, the measurement of equibiaxial stress state and compressive residual stress on a specimen surface using Knoop indentation is neither fully comprehended nor unavailable. In this study, we investigated stress conversion factors for measuring Knoop indentation on equibiaxial stress state through indentation depth using finite element analysis. Knoop indentation was conducted for specimens to determine tensile and compressive equibiaxial residual stress. Both were found to be increased proportionally according to indentation depth. The stress field beneath the indenter during each indentation test was also analyzed. Compressive residual stress suppressed the in-plane expansion of stress field during indentation. In contrast, stress fields beneath the indenter developed diagonally downward for tensile residual stress. Furthermore, differences between trends of stress fields at long and short axes of Knoop indenter were observed due to difference in indenting angles and the projected area of plastic zone that was exposed to residual stress.