• Title/Summary/Keyword: exposed specimen

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FRACTURE STRENGTH OF ZIRCONIA MONOLITHIC CROWNS AND METAL-CERAMIC CROWNS AFTER CYCLIC LOADING AND THERMOCYCLING (지르코니아 단일구조 전부도재관과 금속도재관의 파절강도 비교)

  • Lee, Sang-Min;Jeong, Hee-Chan;Jeon, Young-Chan
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.1
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    • pp.12-20
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    • 2007
  • Purpose: The purpose of this study was to compare the fracture strength of the zirconia monolithic all-ceramic crowns according to the thickness (0.5mm, 0.8mm, 1.1mm) and metal-ceramic crowns (1.0mm, 1.5mm) Material and method: Twelve crowns for each of 3 zirconia crown groups were fabricated using CAD/CAM system (Kavo, Germany) and twelve crowns for each of 2 metal-ceramic crown groups were made by the conventional method. All crowns were luted to the metal dies using resin cement. Half of the specimens were exposed to thermocycling ($5-55^{\circ}C$, 1 Hz) and cyclic loading (300,000 cycles, 50N). Subsequently, all crowns were mounted on the testing jig in a universal testing machine. The load was directed at the center of crown with perpendicular to the long axis of each specimen until catastrophic failure occurred. Analysis of variance and Tukey multiple comparison test (P<.05) were used for statistical analysis of all groups, and paired t-test (P<.05) was followed for statistical comparison between each groups' fracture load before and after cyclic loading. Results: 1. The fracture strength of the zirconia monolithic crowns and the metal-ceramic crown increased as thickness increased (P<.05). 2. The cyclic loading and thermocycling significantly decreased the fracture strength of the zirconia monolithic crowns (P<.05). 3. The standard deviation of fracture strength of the zirconia monolithic crowns was very low. Conclusion: The fracture strength of the zirconia monolithic crowns for the posterior area tends to be higher with thickness increased and 0.8mm or over in thickness is recommended to have similar or over the fracture strength of metal-ceramic crowns.

BONE HEALING CAPACITY OF THE COLLAGEN BONE FILLER ($TERUPLUG^{(R)}$) AND RHBMP-2 IN THE RABBIT CRANIUM DEFECT (가토 두개골 결손부에 이식된 Collagen bone filler ($TERUPLUG^{(R)}$) 및 rhBMP-2의 골치유 능력)

  • Kim, Ju-Hoon;Kim, Chul-Hwan;Kim, Kyung-Wook
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.34 no.2
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    • pp.119-130
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    • 2008
  • Absorbable atelo-collagen sponge $TERUPLUG^{(R)}$, Termo Co. Tokyo, Japan) is inserted in the extraction wound where alveolar bone is exposed. It protects wounds and promotes the formation of granulation. This is made of atelo-collagen, to minimize antigenicity, which is cross-linked by heat treatment for biocompatibility. $TERUPLUG^{(R)}$ consists of between 85 and 95 % of collagen type I and between 5 to 15 % of collagen type III. The raw material for the collagen is derived from bovine skin. It features a sponge block design and is shaped for easy insertion in the extraction wound. This study was designed to find out the bone healing capacity of $TERUPLUG^{(R)}$. We implanted $TERUPLUG^{(R)}$ (experimental group I) and $TERUPLUG^{(R)}$ with rhBMP-2 (experimental group II) in the rabbit cranium defect and then histologically analysed the specimen. The results were as follows. 1. In the 4 weeks, a lot of the newly formed collagen fibers around material of the experimental group I implanted $TERUPLUG^{(R)}$ were observed. But, in the experimental group II implanted $TERUPLUG^{(R)}$ with rhBMP-2, a little of newly formed collagen fibers around material were observed. The cell proliferating activity and apoptosis of the experimental group I, II was positive in and around the implanted material. 2. In the 8 weeks, the amount of newly formed and matured bone in the experimental group II was more observed than the experimental group I and control group. The results of this study indicate that absorbable atelo-collagen sponge ($TERUPLUG^{(R)}$) is relatively favorable bone void filler with biocompatibility and has the better bone healing capacity in case of application with rhBMP-2.

Measurement of CTE Change in a Composite Laminate with Aging under Space Environment using Fiber Optic Sensors (광섬유센서를 이용한 우주환경하에서 복합재료 적층시편의 노화에 따른 열팽창계수변화 측정)

  • Gang,Sang-Guk;Gang,Dong-Hun;Kim,Cheon-Gon;Hong,Chang-Seon
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.31 no.10
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    • pp.21-26
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    • 2003
  • In this research, the change of coefficient of thermal expansion (CTE) of graphite/epoxy composite laminate under space environment was measured using fiber optic sensors. Two fiber Bragg grating (FBG) sensors have been adopted for the simultaneous measurement of thermal strain and temperature. Low Earth Orbit (LEO) conditions with high vacuum, ultraviolet and thermal cycling environments were simulated in a thermal vacuum chamber. As a pre-test, a FBG temperature sensor was calibrated and a FBG strain sensor was verified through the comparison with the electric strain gauge (ESG) attached on an aluminun specimen at high and low temperature respectively. The change of the CTE in a composite laminate exposed to space environment was measured for intervals of aging cycles in real time. As a whole, there was no abrupt change of the CTE after 1000 aging cycles. After aging, however, the CTE decreased a Little all over the test temperature range. These changes are caused by outgassing, moisture desorption, matrix cracking etc.

Nanoparticle Formation from a Commercial Air Freshener at Real-exposure Concentrations of Ozone

  • Vu, Thai Phuong;Kim, Sun-Hwa;Lee, Seung-Bok;Shim, Shang-Gyoo;Bae, Gwi-Nam;Sohn, Jong-Ryeul
    • Asian Journal of Atmospheric Environment
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    • v.5 no.1
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    • pp.21-28
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    • 2011
  • Occupational nanomaterial exposure is an important issue in the manufacture of such products. People are also exposed to various nanoparticles in their living environments. In this study, we investigated nanoparticle formation during the reaction of ozone and volatile organic compounds (VOCs) emitted from a commercial air freshener, one of many widely used consumer products, in a $1-m^3$ reaction chamber. The air freshener contained various VOCs, particularly terpenes. A petri dish containing 0.5 mL of the air freshener specimen was placed in the bottom of the chamber, and ozone was continuously injected into the center of the chamber at a flow rate of 4 L/min with an ozone concentration of either 50, 100 or 200 ppb. Each test was conducted over a period of about 4 h. The higher ozone concentrations produced larger secondary nanoparticles at a faster rate. The amount of ozone reacted was highly correlated with the amount of aerosol formation. Ratios of reacted ozone concentration and of formed particle mass concentration for the three injected ozone concentrations of 50, 100 and 200 ppb were similar to one other; 4.6 : 1.9 : 1.0 and 4.7 : 2.2 : 1.0 for ozone and aerosol mass, respectively.

Tensile Behavior Characteristics of CANDU Pressure Tube Material Degraded by Neutron Irradiations (중수로 압력관 재료의 조사 열화에 따른 인장거동 특성)

  • An, Sang-Bok;Kim, Yeong-Seok;Kim, Jeong-Gyu
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.1
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    • pp.188-195
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    • 2002
  • To investigate the degradation of mechanical properties induced mainly by neutron irradiation, the tensile tests were conducted from room temperature to 300\\`c using the irradiated and the unirradiated Zr-2.5Nb pressure tube materials. The irradiated longitudinal and transverse specimens were collected from the coolant inlet, middle, and outlet parts of M-11 tube which had been operated in Wolsung CANDU Unit-1 and exposed to different operating temperatures and irradiation fluences. The different tensile behavior was characterized not by the fluences of irradiation but by the tensile loading direction. The transverse specimen showed the higher strength and lower elongation than those of the longitudinal one. It was believed that these phenomena resulted from the microstructure anisotropy caused by the extrusion process. The increased strength hardening and decreased elongation embrittlement of the irradiated material were compard to those of the unirradiated one. While the tensile strength of the inlet was higher than that of the outlet, the elongation of the inlet was lower than that of outlet. Considering the operation condition, it was proposed that the operating temperature could be a more effective parameter than the irradiation fluence for long-time life. Through the TEM observation, it was found that while the a-type dislocation density was increased, the c-type dislocation was not changed in the irradiated. The fact that the higher dislocation density was sequentially distributed over the inlet, the middle, and the outlet parts was consistent with the distribution of the tensile strength.

A Combustion Characteristic Analysis of Quercus Variabilis and Pinus Densiflora Fallen Leaves Using Radiation Heat Flux (복사열을 이용한 소나무와 굴참나무 낙엽의 연소특성 분석)

  • Park, Hyung-Ju;Kim, Eung-Sik;Kim, Jang-Hwan;Kim, Dong-Hyun
    • Fire Science and Engineering
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    • v.21 no.3
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    • pp.41-46
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    • 2007
  • The combustion characteristics of surface forest fire fuels was analysed using variable external irradiation level. The characteristics such as ignition time, ignition temperature, critical heat flux and mass loss rate were measured. Fuel samples were exposed to incident heat fluxes from 8 to $50\;kW/m^2$. For the measurement of various combustion characteristics, the size of specimen holder was $100\;mm{\times}100\;mm{\times}12\;mm$ and the fuel samples grinded by electric mill were the fallen leaves of Quercus variabilis and Pinus densiflora. As results, the occurrence of ignition is possible to the heat flux more than $9\;kW/m^2$. The fuel of Pinus densiflora keeps its high temperature longer than that of Quercus variabilis during the combustion process. The results of measurement shows that the maximun and average mass loss rate of Quercus variabilis larger than that of Pinus densiflora.

Effect of Welding Thermal Cycle on Microstructure and Pitting Corrosion Property of Multi-pass Weldment of Super-duplex Stainless Steel (슈퍼 듀플렉스 스테인리스강 다층용접부의 미세조직 및 공식(Pitting Corrosion)에 미치는 용접열사이클의 영향)

  • Nam, Seong-Kil;Park, Se-Jin;Na, Hye-Sung;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.28 no.4
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    • pp.18-25
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    • 2010
  • Super-duplex stainless steels (SDSS) have a good balance of mechanical property and corrosion resistance when they consist of approximately equal amount of austenite and ferrite. The SDSS needs to avoid the detrimental phases such as sigma(${\sigma}$), chi(${\chi}$), secondary austenite(${\gamma}2$), chromium carbide & nitride and to maintain the ratio of ferrite & austenite phase as well known. However, the effects of the subsequent weld thermal cycle were seldom experimentally studied on the micro-structural variation of weldment & pitting corrosion property. Therefore, the present study investigated the effect of the subsequent thermal cycle on the change of weld microstructure and pitting corrosion property at $40^{\circ}C$. The thermal history of root side was measured experimentally and the change of microstructure of weld root & the weight loss by pitting corrosion test were observed as a function of the thermal cycle of each weld layer. The ferrite contents of root weld were reduced with the subsequent weld thermal cycles. The pitting corrosion was occurred in the weld root region in case of the all pitted specimen & in the middle weld layer in some cases. And the weight loss by pitting corrosion was increased in proportional to the time exposed at high temperature of the root weld and also by the decrease of ferrite content. The subsequent weld thermal cycles destroy the phase balance of ferrite & austenite at the root weld. Conclusively, It is thought that as the more subsequent welds were added, the more the phase balance of ferrite & austenite was deviated from equality, therefore the pitting corrosion property was deteriorated by galvanic effect of the two phases and the increase of 2nd phases & grain boundary energy.

Interfacial modulus mapping of layered dental ceramics using nanoindentation

  • Theocharopoulos, Antonios L;Bushby, Andrew J;P'ng, Ken MY;Wilson, Rory M;Tanner, K Elizabeth;Cattel, Michael J
    • The Journal of Advanced Prosthodontics
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    • v.8 no.6
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    • pp.479-488
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    • 2016
  • PURPOSE. The aim of this study was to test the modulus of elasticity (E) across the interfaces of yttria stabilized zirconia (YTZP) / veneer multilayers using nanoindentation. MATERIALS AND METHODS. YTZP core material (KaVo-Everest, Germany) specimens were either coated with a liner (IPS e.max ZirLiner, Ivoclar-Vivadent) (Type-1) or left as-sintered (Type-2) and subsequently veneered with a pressable glass-ceramic (IPS e.max ZirPress, Ivoclar-Vivadent). A $5{\mu}m$ (nominal tip diameter) spherical indenter was used with a UMIS CSIRO 2000 (ASI, Canberra, Australia) nanoindenter system to test E across the exposed and polished interfaces of both specimen types. The multiple point load - partial unload method was used for E determination. All materials used were characterized using Scanning Electron Microscopy (SEM) and X - ray powder diffraction (XRD). E mappings of the areas tested were produced from the nanoindentation data. RESULTS. A significantly (P<.05) lower E value between Type-1 and Type-2 specimens at a distance of $40{\mu}m$ in the veneer material was associated with the liner. XRD and SEM characterization of the zirconia sample showed a fine grained bulk tetragonal phase. IPS e-max ZirPress and IPS e-max ZirLiner materials were characterized as amorphous. CONCLUSION. The liner between the YTZP core and the heat pressed veneer may act as a weak link in this dental multilayer due to its significantly (P<.05) lower E. The present study has shown nanoindentation using spherical indentation and the multiple point load - partial unload method to be reliable predictors of E and useful evaluation tools for layered dental ceramic interfaces.

A case of abnormally exposed nodular shaped-bronchial vessel occurred massive hemorrhage during bronchoscopy (기관지 내시경 하 조직 생검 중 대량 출혈을 일으킨 기관지 강 내 돌출된 결절모양의 혈관 1예)

  • Chae, Soo-Youb;You, Moon-Bin;Kang, Ki-Hoon;Lee, Byung-Soo;Chae, Eun-Ha;Joo, Eun-Hyun;Kim, Myung-Chan;Cho, Wook-Hyun;Oh, Yong-Leul;Lee, Soon-Il;Kim, Hui-Jung;Lee, Hyo-Jin
    • Tuberculosis and Respiratory Diseases
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    • v.53 no.2
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    • pp.216-220
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    • 2002
  • A 43 years old woman with a previous history of healed tuberculosis presented with a recurrent hemoptysis. On a bronchoscopy inspection, three nodular shaped mass-like lesions (0.5cm in diameter) were found on the right lower lobar bronchus. Massive hemoptysis occurred when the specimen were taken during bronchoscopy. The bleeding could not be controlled by non-surgical treatment. Consequently, she underwent a right lower lobectomy in order to control the bleeding. The patient died of respiratory failure 3 days later. A bronchoscopic biopsy revealed an abnormal blood vessel just beneath the bronchial respiratory epithelium.

A Combustion Characteristic Analysis of Sandwich Panel Core Using Radiation Heat Flux (복사열을 이용한 샌드위치 패널 심재의 연소특성 분석)

  • Park, Hyung-Ju
    • Fire Science and Engineering
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    • v.21 no.4
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    • pp.25-31
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    • 2007
  • The combustion characteristics and combustion heat of sandwich panel cores were analysed using variable external irradiation level. The characteristics such as ignition time, critical heat flux, ignition temperature and surface temperature profile were measured. Fuel samples were exposed to incident heat fluxes from 15 to $50\;kW/m^2$. For the measurement of various combustion characteristics, the size of specimen was $100\;mm\;{\times}\;100\;mm\;{\times}\;50\;mm$ and the samples were 3 different kinds. As results, Type B showed the best characteristics in measurement of combustion heat and ignition temperature and Type C showd the best characteristics in critical heat flux and surface temperature profile than that of the other two. In conclusion, we knew that Type C had the best performance in fire safety from all data of this study.