• Title/Summary/Keyword: advanced analysis

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Determination of Germanium in Spring Waters by Inductively Coupled Plasma Mass Spectrometry (ICP-MS에 의한 지하수 중의 Germanium 분석에 관한 연구)

  • Park, Kyung Su;Song, Seong Yeon;Shim, Ue Sup;Kim, Sun Tae
    • Analytical Science and Technology
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    • v.11 no.2
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    • pp.120-124
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    • 1998
  • A rapid and accurate determination method of ultra-trace amounts of germanium in spring water by ICP-MS has been developed. Mass number 74 was not only the best mass but also the smallest mass interference. Only 30% of water samples contain germanium more than $0.1{\mu}g/L$, and a few of them has organogermanium species.

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CHARACTERIXATION OF PLASMA ION IMPLANTED SURFACES USING TIME-OF-FLIGHT SECONDARY ION MASS SPECTROMATRY

  • Lee, Yeon-Hee;Han, Seung-Hee;Lee, Jung-Hye;Yoon, Jung-Hyeon
    • Journal of the Korean institute of surface engineering
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    • v.29 no.6
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    • pp.880-883
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    • 1996
  • Plasma Source Ion Implantation (PSII) technique was used for the hydrophilization or hydrophobization of polymer surfaces. Polymers were modified with different plasma gases such as oxygen, nitrogen, argon, and tetrafluoromethane, and for varying lengths of treatment time. Plasma ion treatment of oxygen, nitrogen, argon and their mixtures increased significantly the hydrophilic properties of polymer surfaces. More hydrophobic surfaces of polymers were formed after the treatment with tetrafluoromethane. A study of plasma source ion implanted polymers was performed using contact angle measurements and Time-of-Flight Secondary Ion Mass Spectrometry (TOF-SIMS). The TOF-SIMS spectra and depth profile were used to obtain the information about the treated surfaces of polymers. The permanence of this technique could be evaluated with respect to ageing time. The surfaces treated with PSII gave better stability than other surface modification methods.

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Optimal Design of Trusses Using Advanced Analysis and Genetic Algorithm (고등해석과 유전자 알고리즘을 이용한 트러스 구조물의 최적설계)

  • Choi, Se-Hyu
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.12 no.4
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    • pp.161-167
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    • 2008
  • In this paper, the optimal design of trusses using advanced analysis and genetic algorithm is performed. An advanced analysis takes into account geometric nonlinearity and material nonlinearity. The micro genetic algorithm is used as optimization technique. The weight of structures is treated as the objective function. The constraint functions are defined by load-carrying capacities and displacement requirement. The effectiveness of the proposed method is verified by comparing the results of the proposed method with those of other method.

Genetic diversity, structure analysis and relationship in soybean mutants as revealed by TRAP marker

  • Kim, Dong-Gun;Lyu, Jae-Il;Lee, Min-Kyu;Kim, Jung Min;Hong, Min Jeong;Kim, Jin-Baek;Bae, Chang-Hyu;Kwon, Soon-Jae
    • Proceedings of the Plant Resources Society of Korea Conference
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    • 2018.10a
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    • pp.43-43
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    • 2018
  • Mutation breeding by radiation is useful for improving various crop species. Up to now, a total of 170 soybean mutant varieties have been released in the world, which is the second most registered varieties after rice. Despite the economic importance of soybean, there have been no TRAP marker system studies on genetic relationships between/among mutant lines. To develop a strategy of Mutant Diversity Pool (MDP) conservation, a study on the genetic diversity of 210 soybean mutant lines (8 cultivars and 202 mutants) was performed through a TRAP analysis. Sixteen primer combinations amplified a total of 551 fragments. The highest (84.00%) and lowest (32.35%) polymorphism levels were obtained with primers MIR157B + Ga5 and B14G14B + Ga3, respectively. The mean PIC values 0.15 varied among the primer combination ranging from 0.07 in B14G14B + Sal2 to 0.23 in MIR157B + Sa4. Phylogenetic, principal component analysis (PCA) and structure analysis indicated that the 210 lines belong to four groups based on the 16 combination TRAP markers. AMOVA showed 21.0% and 79.0% variations among and within the population, respectively. Overall, the genetic similarity of each cultivar and its mutants were higher than within other mutant populations. Our results suggest that the TRAP marker system may be useful for assessing the genetic diversity among soybean mutants and help to improve our knowledge of soybean mutation breeding.

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Different Physiological Response to Salt in Salt Tolerant Rice Mutants Induced by Gamma-Mutagenesis

  • Jang, Duk-Soo;Song, Mira;Kim, Sun-hee;Kim, Jin-Baek;Kim, Sang Hoon;Ha, Bo-Keun;Kang, Si-Yong;Kim, Wook;Kim, Dong Sub
    • Journal of Radiation Industry
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    • v.5 no.3
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    • pp.259-266
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    • 2011
  • When plants undergo stress, Reactive oxygen species (ROS) which remove bad elements such as mildew and virus is activated in plant body. However, if ROS is excessively increased, plant will be harmed itself by destruction of cell and signal system and phenomenon of lipid peroxidation. In order to identify content of lipid peroxidation and activity of some enzymes scavenging ROS, phenotypical and physiological analysis was performed with two mutant lines, Till-II-877 and Till-II-894, comparing with cv. Dongan (WT). In phenotype analysis, two mutant lines give to well-conditioned growth better than WT in since 5 days after salt treatment. In enzyme activities, there was a modest difference in the content of catalase (CAT) and peroxidase (POD) between Till-II-877 and Till-II-894, two mutant lines showed high levels in CAT contents than WT. However, they express low levels in POD contents. In MDA analysis, the content of Till-II-877 was higher than that of WT, but Till-II-894 was lower. This result indicates that two mutants have different mechanism against salt stress.

Efficient Recycling of Printed Circuit Boards from Disassembly/Separation Process of waste LCD TVs: Composition Analysis and Value-wise Classification (LCD TV 해체 시 발생하는 PCB의 효율적 재활용을 위한 구조 분석 및 등급별 분류)

  • Hong, Myung Hwan;Park, Kyung-Soo;Swain, Basudev;Kang, Lee-Seung;Suk, Han Gil;Hong, Hyun Seon
    • Resources Recycling
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    • v.24 no.1
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    • pp.66-72
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    • 2015
  • Various waste PCBs arose during disassembly of LCD TVs and monitors in which they originally functioned for transmission of imaging signal, power supply, and imaging control. In those functional PCBs, gold and copper are contained at far more acceptable level, exceeding mining grade ores. Those valuable metals and their contents widely vary with functionality and end use of PCBs. Therefore, compositional analysis of individual waste PCBs from disassembled LCD TVs and monitors were performed in the present study to classify them into three categories: high gold yield and low gold yield PCBs and those without gold contents. Besides, additional chemical analysis was made to reveal gold and copper contents in the waste PCBs arising from actual disassembly/separation of end-of-life LCD TVs and monitors.

Structural Performance of an Advanced Compsites Bridge Superstructure for Rapid Installation (급속시공용 복합신소재 교량상부구조의 구조 성능)

  • Ji, Hyo-Seon
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.1 no.1
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    • pp.34-45
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    • 2010
  • This paper describes the design, manufacturing process, testing, application, and assessment of capacity-ratings of the first all advanced composites bridge on a public highway system. In order to verify the bridge design prior to the field application, a sub-scale bridge superstructure was built and tested in the laboratory. The field load test results were compared with those of the finite element analysis for the verification of validity. To investigate its in-service performance, field load testing and visual inspections were conducted under an actual service environment. The paper includes the presentation and discussion for advanced composites bridge capacity rating based on the stress modification coefficients obtained from the test results. The test result indicates that the advanced composites bridge has no structural problems and is structurally performing well in-service as expected. Since these composite materials are new to bridge applications, reliable data is not available for their in-service performance. The results may provide a baseline data for future field advanced composites bridge capacity rating assessments and also serve as part of a long-term performance of advanced composites bridge.

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Detection of phenobarbital adulteration in dietary supplements: simultaneous analysis of 16 sedative-hypnotics and sleep-inducers by ultra-high-performance liquid chromatography with UV detection (UPLC-UV) and quadruple Orbitrap mass spectrometry (Q-Orbitrap-MS)

  • Lee, Ji Hyun;Choi, Ji Yeon;Park, Hanna;Min, Ah Young;Kim, Nam Sook;Park, Seong Soo;Park, Sung-Kwan;Kang, Ho-il
    • Analytical Science and Technology
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    • v.32 no.1
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    • pp.24-34
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    • 2019
  • The safety of food is occasionally questionable, as there have been some reports of products contaminated with illegal adulterants. In this study, the presence of 16 sedative-hypnotics and sleep inducers in dietary supplements was determined by ultra-high-performance liquid chromatography with UV detection (UPLC-UV) and quadruple Orbitrap mass spectrometry (Q-Orbitrap-MS). The UPLC method was validated, providing a linearity (R2) of more than 0.999, and LODs and LOQs that ranged from 0.2 to 0.5 and 0.6 to $1.5{\mu}g\;mL^{-1}$, respectively. The repeatabilities were 0.2-8.4 % (intra-day) and 0.3-4.5 % (inter-day), and the accuracies were 89.0-117.0 % (intra-day) and 87.8-111.9 % (inter-day). The mean recoveries of the spiked samples ranged from 98.7 to 107.3 %. The relative standard deviation (%RSD) of the stability was less than 2.4 %. Using the developed method, one sedative-hypnotic compound, phenobarbital, was detected in one of the nineteen samples tested. In addition, the major characteristic fragment ions of each target compound were confirmed using Q-Orbitrap-MS for higher accuracy. Monitoring the presence of these 16 sedative-hypnotics and sleep inducers in dietary supplements should be pursued in the interest of human health, and the results of this study confirmed that the developed method has value for this application.

Seismic design of irregular space steel frames using advanced methods of analysis

  • Vasilopoulos, A.A.;Bazeos, N.;Beskos, D.E.
    • Steel and Composite Structures
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    • v.8 no.1
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    • pp.53-83
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    • 2008
  • A rational and efficient seismic design methodology for irregular space steel frames using advanced methods of analysis in the framework of Eurocodes 8 and 3 is presented. This design methodology employs an advanced static or dynamic finite element method of analysis that takes into account geometrical and material non-linearities and member and frame imperfections. The inelastic static analysis (pushover) is employed with multimodal load along the height of the building combining the first few modes. The inelastic dynamic method in the time domain is employed with accelerograms taken from real earthquakes scaled so as to be compatible with the elastic design spectrum of Eurocode 8. The design procedure starts with assumed member sections, continues with the checking of the damage and ultimate limit states requirements, the serviceability requirements and ends with the adjustment of member sizes. Thus it can sufficiently capture the limit states of displacements, rotations, strength, stability and damage of the structure and its individual members so that separate member capacity checks through the interaction equations of Eurocode 3 or the usage of the conservative and crude q-factor suggested in Eurocode 8 are not required. Two numerical examples dealing with the seismic design of irregular space steel moment resisting frames are presented to illustrate the proposed method and demonstrate its advantages. The first considers a seven storey geometrically regular frame with in-plan eccentricities, while the second a six storey frame with a setback.