• Title/Summary/Keyword: adhesion energy

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Effects of Tape Thickness and Inorganic Fillers on the Adhesion Properties of Double-sided Acrylic Adhesive Tape by Ultraviolet Curing (자외선 경화형 아크릴 양면 점착테이프의 두께 및 무기물 충전제 종류에 따른 접착특성)

  • Kim, Dong-Bok
    • Polymer(Korea)
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    • v.38 no.3
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    • pp.397-405
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    • 2014
  • To manufacture of high-performance semi-structural double-sided adhesive tape, 2-ethylhexyl acrylate (2-EHA) and acrylic acid (AAC) were used, and the syrup was prepared by UV irradiation in this study. The effects of the thickness, various inorganic filler contents, and filler types on the semi-structural properties of acrylic double-sided adhesive tape were investigated. The peel strength increased with increasing thickness and wetting time. In case of the thin thickness (under $250{\mu}m$) with decreasing true density of inorganic filler, the peel strength increased with increasing wetting time. The initial peel strength showed a higher value at a big size of inorganic filler, and the filler's size in adhesive tapes was confirmed by SEM images. The peel strength and dynamic shear strength increased as a proportional relationship with various inorganic fillers and contents, and these inorganic fillers in $0.1{\mu}m$ thickness indicated more effect on the dynamic shear strength of double-sided adhesive tape. From these results the thin acrylic double-sided adhesive tape determined to be use for applications as a high-performance semi-structural.

Surface characteristics and bioactivity of an anodized titanium surface

  • Kim, Kyul;Lee, Bo-Ah;Piao, Xing-Hui;Chung, Hyun-Ju;Kim, Young-Joon
    • Journal of Periodontal and Implant Science
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    • v.43 no.4
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    • pp.198-205
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    • 2013
  • Purpose: The aim of this study was to evaluate the surface properties and biological response of an anodized titanium surface by cell proliferation and alkaline phosphatase activity analysis. Methods: Commercial pure titanium (Ti) disks were prepared. The samples were divided into an untreated machined Ti group and anodized Ti group. The anodization of cp-Ti was formed using a constant voltage of 270 V for 60 seconds. The surface properties were evaluated using scanning electron microscopy, X-ray photoelectron spectroscopy, and an image analyzing microscope. The surface roughness was evaluated by atomic force microscopy and a profilometer. The contact angle and surface energy were analyzed. Cell adhesion, cell proliferation, and alkaline phosphatase activity were evaluated using mouse $MC_3T_3-E_1$ cells. Results: The anodized Ti group had a more porous and thicker layer on its surface. The surface roughness of the two groups measured by the profilometer showed no significant difference (P>0.001). The anodized Ti dioxide ($TiO_2$) surface exhibited better corrosion resistance and showed a significantly lower contact angle than the machined Ti surface (P>0.001). Although there was no significant difference in the cell viability between the two groups (P>0.001), the anodized $TiO_2$ surface showed significantly enhanced alkaline phosphatase activity (P<0.001). Conclusions: These results suggest that the surface modification of Ti by anodic oxidation improved the osteogenic response of the osteoblast cells.

Effect of Ball Milling on Photosensitive Carbon Nanotube Pastes and Their Field Emission Properties (감광성 CNT paste에 대한 저에너지 Ball Milling 처리 효과)

  • Jang, Eun-Soo;Lee, Han-Sung;Lee, Nae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.154-154
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    • 2008
  • Although the screen printing technology using photosensitive carbon nanotube (CNT) paste has many advantages such as low cost, simple process, uniform emission, and capability of mass production, the CNT paste needs to be improved further in CNT dispersion, printability, adhesion, electrical conductivity, population of CNT emitters, etc. Ball milling has been frequently employed to prepare the CNT paste as ball milling can mix its ingredients very well and easily cut the long, entangled CNTs. This study carried out a parametric approach to fabricating the CNT paste in terms of low-energy ball milling and a paste composition. Field emission properties of the CNT paste was characterized with CNT dispersion and electrical conductivity which were measured by a UV-Vis spectrophotometer and a 4-point probe method, respectively. Main variables in formulating the CNT paste include a length of milling time, and amounts of CNTs and conductive inorganic fillers. In particular, we varied not only the contents of conductive fillers but also used two different sizes of filler particles of ${\mu}m$ and nm ranges. Among many variations of conductive fillers, the best field emission characteristics occurred at the 5 wt% fillers with the mixing ratio of 3:1 for ${\mu}m$-and nm-sizes. The amount and size of fillers has a great effect on the morphology, processing stability, and field emission characteristics of CNT emitter dots. The addition a small amount of nm-size fillers considerably improved the field emission characteristics of the photosensitive CNT paste.

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Development of Perfluoroalkyl Derivative for $Cr^{3+}$ Adsorbent Promotion Process (3가 크롬 흡착 증진용 과불소 알킬유도체 제조 및 적용공정 개발)

  • Shin, Jong-Sub;Kum, Chang-Hun;Yun, Jong-Kuk;Park, Il-Kyu
    • Clean Technology
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    • v.14 no.3
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    • pp.193-203
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    • 2008
  • A surfactant is used to assist the effect of cleaning, dispersibility and adhesion during leather manufacturing process. Existing surfactant for that process includes many hydrophilic groups that may cause problem such as stain, bad water resistance and poor durability, etc. It is potential problem to make high-performance property for future leather market. In this study, we have synthesized the fluorinated surfactant of which property decreases surface tension, increases dispersion, cleaning effect and the better chrome absorption by the high bond energy of C-F to complement weakness that the present alkyl derivative surfactants have. Using fluorinated surfactant, we can confirm that dispersion is increased, chrome absorption ratio is augmented with high osmosis and coherence, chrome content in the tanning waste water is reduced, BOD and COD contents are diminished and physical characteristics are improved.

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COMBUSTION CHARACTERISTICS OF A MICRO-SOLID PROPELLANT ROCKET ARRAY THRUSTER

  • Kazuyuki Kondo;Shuji Tanaka;Hiroto Habu;Tokudome, Shin-ichiro;Keiichi Hori;Hirobumi Saito;Akihito Itoh;Masashi Watanabe;Masayoshi Esashi
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2004.03a
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    • pp.593-596
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    • 2004
  • We are developing a micro-solid propellant rocket array thruster for simple attitude control of a 10 kg class micro-spacecraft. The prototype has ø 0.8 mm solid propellant micro-rockets arrayed at a pitch of 1.2 mm on a 22 x 22 mm substrate. In previous studies, an impulse thrust of 4.6 x 10$^{-4}$ Ns was obtained in vacuum, but we found the problems of unacceptably low ignition success rate and incomplete combustion. This paper describes experiments to improve the ignition rate. In order to achieve this goal, we tried to solidify paste-like ignition aid (RK) on the ignition heaters with strong adhesion. To make the paste-like RK, isoamyl acetate was added to RK powder. We tested 9 rockets, but only 2 rockets were ignited with huge ignition energy. This is because the heat con-duction between the ignition heater and the RK was too low to ignite the RK, since dried RK had a lot of pores. Also, a large cavity was sometimes found just above the ignition heater.

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Properties of Ga-doped ZnO transparent conducting oxide fabricated on PET substrate by RF magnetron sputtering (RF 마그네트론 스퍼터링 공정으로 PET 기판 위에 제조한 Ga-doped ZnO 투명전도막의 특성)

  • Kim, Jeong-Yeon;Kim, Byeong-Guk;Lee, Yong-Koo;Kim, Jae-Hwa;Woo, Duck-Hyun;Kweon, Soon-Yong;Lim, Dong-Gun;Park, Jae-Hwan
    • Journal of the Microelectronics and Packaging Society
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    • v.17 no.1
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    • pp.19-24
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    • 2010
  • The effects of $O_2$ plasma pretreatment on the properties of Ga-doped ZnO films on PET substrate were studied. GZO films were fabricated by RF magnetron sputtering process. To improve surface energy and adhesion between the PET substrate and the GZO film, $O_2$ plasma pretreatment process was used prior to GZO sputtering. As the RF power and the treatment time increased, the crystallinity increased and the contact angle decreased significantly. When the RF power was 100 W and the treatment time was 600 sec in $O_2$ plasma pretreatment process, the resistivity of GZO films on the PET substrate was $1.90{\times}10^{-3}{\Omega}-cm$.

A Study on the Quality Improvement of Recycled Coarse Aggregate by High Speed Rotating Grinder (고속회전형 마쇄기술을 통한 순환골재 품질향상에 관한 연구)

  • Lee, Ki-Won;Yeo, Woon-Ho
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.4
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    • pp.341-348
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    • 2019
  • In this study, we analyzed the problems of existing construction waste shredding technology to diagnose the problems of low quality recycled aggregates and to develop a new mortar peeling technique to produce high-quality recycled coarse aggregate for concrete. The purpose of this study is to verify the effectiveness of mortar peeling technique by doing simulation prior to on-site application and to check the quality properties of recycled coarse aggregate produced by applying a mortar peeling technique. We manufactured and installed High speed Rotating Grinder on-site and analyzed the correlation between mortar adhesion amount, dry density and water absorption rate of recycled coarse aggregate.

Etch resist patterning of printed circuit board by ink jet printing technology (잉크젯 인쇄기술을 이용한 인쇄회로기판의 에칭 레지스터 패터닝)

  • Seo, Shang-Hoon;Lee, Ro-Woon;Kim, Yong-Sik;Kim, Tae-Gu;Park, Sung-Jun;Yun, Kwan-Soo;Park, Jae-Chan;Jeong, Kyoung-Jin;Joung, Jae-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.108-108
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    • 2007
  • Inkjet printing is a non-contact and direct writing associated with a computer. In the industrial field, there have been many efforts to utilize the inkjet printing as a new way of manufacturing, especially for electronic devices. The etching resist used in this process is an organic polymer which becomes solidified when exposed to ultraviolet lights and has high viscosity of 300 cPs at ambient temperature. A piezoelectric-driven ink jet printhead is used to dispense $20-40\;{\mu}m$ diameter droplets onto the copper substrate to prevent subsequent etching. In this study, factors affecting the pattern formation such as printing resolution, jetting property, adhesion strength, etching and strip mechanism, UV pinning energy have been investigated. As a result, microscale Etch resist patterning of printed circuit board with tens of ${\mu}m$ high have been fabricated.

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Effects of $N_2/H_2$ plasma treatments on enhancement of neuronal cell affinity on single-walled carbon nanotube paper scaffolds

  • Yoon, Ok-Ja;Lee, Hyun-Jung;Jang, Yeong-Mi;Kim, Hyun-Woo;Lee, Won-Bok;Kim, Sung-Su;Lee, Nae-Eung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.393-393
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    • 2010
  • The biocompatibility of materials used for biomedical applications depends on chemical composition, mechanical stiffness, surface energy, and roughness. The plasma treatment and etching process is a very important technology in the biomedical fields due to possibility of controlling the surface chemistry and properties of materials. In this work, $N_2/H_2$ plasma were treated on single-walled carbon nanotubes (SWCNTs) paper and characterization of treated SWCNTs paper was carried out. Also we investigated neurite outgrowth from SH-SY5Y on treated SWCNTs paper. The results indicated that $N_2/H_2$ plasma-modified SWCNTs paper enhanced neuronal cell adhesion, viability, neurite outgrowth and branching in vitro and exerted a positive role on the health of neural cells.

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Flexural Behavior of Highly Ductile Cement Composites Mimicking Boundary Conditions of Shellfish Skin Layer (패류 껍질층의 경계면을 모방한 고연성 시멘트 복합재료의 휨 거동)

  • Kwon, Ki-Seong;Chun, Jae-Yeong;Bang, Jin-Wook;Kim, Yun-Yong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.24 no.1
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    • pp.108-115
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    • 2020
  • In this study, the flexural performance of Highly Ductile Cement Composites(HDCC) mimicking boundary conditions of shellfish skin layer was evaluated. To improve ductility by mimicking the boundary skin layer structure of shellfish, the method of stratification by charging between precast panels using HDCC and the method of distributing PE-mesh to the interface surface were applied. Evaluation of flexural performance of layered cement composite materials mimicking boundary conditions of shellfish skin layer resulted in increased ductility of all test specimens applied with stratified cross-section compared to typical bending test specimens. The layered method by inserting PE-mesh showed excellent ductility. This is most likely because the inserted PE-mesh made an interface for separating the layers while the HDCC pillars in the PE-mesh gave adhesion between layers.