• Title/Summary/Keyword: Vapor flow

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Preparation of Ultrafine Silica Powders by Chemical Vapor Deposition Process (기상반응(CVD)법 의한 실리카 미분말의 제조)

  • Choi, Eun-Young;Lee, Yoon-Bok;Shin, Dong-Woo;Kim, Kang-Ho
    • Korean Journal of Materials Research
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    • v.12 no.11
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    • pp.850-855
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    • 2002
  • Silica powders were prepared from $SiCl_4$-$H_2$O system by chemical vapor deposition process, and investigated on size control of the products with reaction conditions. The products were amorphous and nearly spherical particles with 130nm~50nm in size. The size distribution became narrow with the increase of [$H_2$O]/[SiCl$_4$] concentration ratio. The particle size decreased with the increase of reaction temperature, [$H_2$O]/[SiCl$_4$] concentration ratio and total flow rate. The specific surface area measured by BET method was about three times larger than that of electron microscope method.

Graphene Synthesized by Plasma Enhanced Chemical Vapor Deposition at Low-Temperature

  • Ma, Yifei;Kim, Dae-Kyoung;Xin, Guoqing;Chae, Hee-Yeop
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.248-248
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    • 2012
  • Synthesis graphene on Cu substrate by plasma-enhanced chemical vapor deposition (PE-CVD) is investigated and its quality's affection factors are discussed in this work. Compared with the graphene synthesized at high temperature in chemical vapor deposition (CVD), the low-temperature graphene film by PE-CVD has relatively low quality with many defects. However, the advantage of low-temperature is also obvious that low melting point materials will be available to synthesize graphene as substrate. In this study, the temperature will be kept constant in $400^{\circ}C$ and the graphene was grown in plasma environment with changing the plasma power, the flow rate of precursors, and the distance between plasma generator coil and substrates. Then, we investigate the effect of temperature and the influence of process variables to graphene film's quality and characterize the film properties with Raman spectroscopy and sheet resistance and optical emission spectroscopy.

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Design and Application of Thermal Vapor Compressor for Multi-Effect Desalination Plant (열증기압축기 설계와 MED 담수설비에의 적용)

  • Park, Il-Seok;Park, Sang-Min;Ha, Ji-Soo
    • Proceedings of the KSME Conference
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    • 2004.11a
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    • pp.1670-1675
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    • 2004
  • A thermal vapor compressor in which the subsonic/supersonic flow appears simultaneously, has been accurately designed through the CFD analysis for the various shape parameters such as the primary nozzle shape, converging duct shape. mixing tube diameter, and so on. The performance of the developed thermal vapor compressor has been experimentally verified to be installed in a Multi Effect Desalination(MED) plant as an important element, In this paper, the experimental results for Various boundary conditions(motive pressure, suction pressure, and discharge pressure) are presented in comparing with CFD results. The two results show a good agreement with each other within 3.5 % accuracy with regard to the entrainment ratio.

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Characterization of Fe-Co Nanocomposite Powders Produced by Chemical Vapor Condensation Methods (화학기상응축법으로 제조한 Fe-Co 나노복합 분말의 미세구조와 자기적 특성)

  • ;Z. H. Wang;;;Z. D. Zhang
    • Journal of Powder Materials
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    • v.9 no.5
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    • pp.322-328
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    • 2002
  • Fe-Co nanocomposite powders with different composition were prepared by chemical vapor condensation (CVC) process and their characterizations were studied by means of X-ray diffraction, transmission electron microscopy, and vibrating sample magnetometer. The particles having the mean size of 5~25 nm consisted of metallic cores and oxide shells. The Co contents and particle size increased with increasing the carrier gas flow rate of Co precursor. The saturation magnetization and coercivity increased with increasing Co content. and the saturation magnetization maximized at the 40 wt.%Co. The Fe-Co nanocomposite powder oxidized at $400^{\circ}C$ showed the maximum coercivity of 1739 Oe.

Condensation Heat Transfer for the R-11 Superheated Vapor with and without Noncondensable Gas (R-11의 응축열전달에 미치는 부응축가스 및 과열의 영향)

  • CHO Kwon-Ok;KUM Jong-Soo;OH HOO-Kyu
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.18 no.2
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    • pp.85-93
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    • 1985
  • An experimental investigation on condensing heat transfer for the Refrigerant-11 superheated vapor during condensation on the 40 mm O.D by 75 mm long horizontal tube is carried out under the various conditions of air contents as noncondensable gas, condensing pressure, and coolant temperature. The data span a refrigerant flow range from 23 to 63 kg/h and weight fractions of noncondensable gas range from 0 to $15\%$. The comparisons are made using data obtained by the authors and further data obtained from other sources. The characteristics of the condensing heat transfer of refrigerant superheated vapor with and without noncondensable gas flowing horizontally are revealed experimentally, and on the basis of the data obtained, correlations for predicting heat transfer coefficient during condensation on the tube are proposed.

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Characterization of Low-Temperature Graphene Growth with Plasma Enhanced Chemical Vapor Deposition

  • Ma, Yifei;Kim, Dae-Kyoung;Xin, Guoqing;Chae, Hee-Yeop
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.421-421
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    • 2012
  • Graphene has drawn enormous attention owing to its outstanding properties, such as high charge mobility, excellent transparence and mechanical property. Synthesis of Graphene by chemical vapor deposition (CVD) is an attractive way to produce large-scale Graphene on various substrates. However the fatal limitation of CVD process is high temperature requirement(around $1,000^{\circ}C$), at which many substrates such as Al substrate cannot endure. Therefore, we propose plasma enhanced CVD (PECVD) and decrease the temperature to $400^{\circ}C$. Fig. 1 shows the typical structure of RF-PECVD instrument. The quality of Graphene is affected by several variables. Such as plasma power, distance between substrate and electronic coil, flow rate of source gas and growth time. In this study, we investigate the influence of these factors on Graphene synthesis in vacuum condition. And the results were checked by Raman spectra and conductivity measurement.

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Effects of Non-absorbable Gases in the Absorption of Water Vapor by Aqueous LiBr Solution Film on Horizontal Tube Banks

  • Kwon, Ky-Seok;Kim, Byong-Joo
    • International Journal of Air-Conditioning and Refrigeration
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    • v.9 no.2
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    • pp.19-27
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    • 2001
  • In the present study, the effects of film Reynolds number (60∼200) and volumetric content of non-absorbable gases (0∼10%) in water vapor on the absorption process of aqueous LiBr solution were investigated experimentally. The formation of solution film on the horizontal tubes of six rows was observed to be complete for Re>100. Transition film Reynolds number was found to exist above which the Nusselt number and Schmidt number diminishes with solution flow rate. As the concentration of non-absorbable gases increased, mass transfer rate decreased more seriously than heat transfer rate did. the degradation effects of non-absorbable gases seemed to be significant especially when small amount of non-absorbable gases was introduced to the pure water vapor.

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Synthesis and Characteristics of FePt Nanopowder by Chemical Vapor Condensation Process

  • Yu, Ji-Hun;Lee, Dong-Won;Kim, Byoung-Kee;Jang, Tae-Suk
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1196-1197
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    • 2006
  • FePt binary-alloy nanopowder has been successfully synthesized by chemical vapor condensation process with two metal organic precursors, i.e., iron pentacarbonyl and platinum acetylacetonate. Average particle size of the powder was less than 50 nm with very narrow size distribution, revealing high dispersion capability. Characteristics of the powder could be controlled by changing process parameters such as reaction temperature, chamber pressure, as well as gas flow rate. Magnetic properties of the synthesized FePt nanopowder were investigated and analyzed in terms of the powder characteristics.

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Development of a Flat-Plate Cooling Device for Electronic Packaging

  • Moon, Seok-Hwan;Hwang, Gunn;Lim, Hyun-Taeck
    • ETRI Journal
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    • v.33 no.4
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    • pp.645-647
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    • 2011
  • In this study, a microcapillary pumped loop (MCPL) that can be used as a cooling device for small electronic and telecommunications equipment has been developed. For thin devices such as an MCPL, securing a vapor flow space is a critical issue for enhancing the thermal performance. In this letter, such enhancement in thermal performance was accomplished by eliminating condensed droplets from the vapor line. By fabricating the grooves in the vapor line to eliminate droplets, a decrease in thermal resistance of about 63.7% was achieved.

Effects of Inner Jet Injection on Particle Deposition in the Annular Modified Chemical Vapor Deposition Process Using Concentric Tubes (환상형원관을 사용하는 수정된 화학증착(MCVD)방법에서 내부 제트분사가 입자부착에 미치는 영향)

  • 최만수;박경순
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.1
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    • pp.212-222
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    • 1994
  • In the annular Modified Chemical Vapor Deposition process using two concentric tubes, the inner tube is heated to maintain high temperature gradients to have high thermophoretic force which can increase particle deposition efficiency. However, higher axial velocity in a narrow gap between inner and outer tubes can result in a longer tapered entry length. In the present paper, a new concept using an annular jet from the inner tube is presented and shown to significantly reduce the tapered entry length with maintaining high efficiency. Effects of a jet injection on heat transfer, fluid flow and particle deposition have been studied. Of particular interests are the effects of jet velocity, jet location and temperature on the deposition efficiency and tapered length . Torch heating effects from both the previous and present passes are included and the effect of surface radiation between inner and outer tubes is also considered.