• 제목/요약/키워드: Ultrasonic dispersion

검색결과 165건 처리시간 0.029초

직조된 SiC 섬유에 무전해 구리도금 시 도금 조건의 영향 (Effect of Plating Conditions on Electroless Copper Plating on SiC Fabric)

  • 이기환;손유한;한태양;이경진;김혜성;한준현
    • 한국표면공학회지
    • /
    • 제50권4호
    • /
    • pp.244-250
    • /
    • 2017
  • Effects of plating conditions (dispersant concentration, plating time, and ultrasonication) on electroless Cu plating on SiC fabric woven by crossing of SiC continuous fibers vertically were studied. The ultrasonic dispersion treatment not only did not improve the dispersion of the SiC fibers, but also did not change the plating thickness. The ultrasonication in the pretreatment step of electroless plating did not improve the dispersion of the fibers, while the ultrasonication in the plating step enhanced the dispersion of the fibers and decreased the thickness of the Cu films. It was possible to control the thickness of the Cu coating layer as well as the dispersion of the fibers in the fabric by changing the plating conditions such as dispersant concentration, plating time, and ultrasonication, but it was very difficult to coat copper on the intersection of vertical fibers in the fabric.

분산방법에 따른 CNT를 혼입한 섬유보강 시멘트복합체의 유동성 평가 (Table Flow Evaluation of CNT-Mixed Fiber Reinforced Cement Composite by Dispersion Method)

  • 김문규;김규용;편수정;최병철;박준영;남정수
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2023년도 봄 학술논문 발표대회
    • /
    • pp.95-96
    • /
    • 2023
  • In this study, the table flow of fiber reinforced cement composites mixed with CNTs dispersed differently according to the dispersion method was evaluated. The mixture was composed of plain mixture according to the presence or absence of ultrasonic dispersion and PCE-based dispersants A and B of 0.5% and 1.0%, respectively, CNT was mixed with 0.03% of cement weight and fiber was mixed with 1.5% of total volume. As a result of the experiment, NC-A0.5 showed a fluidity similar to that of P without CNT. The fluidity of NC-A0.5 and P-N showed a similar tendency, which is considered to be due to the distribution of evenly dispersed CNT particles without agglomeration between cement particles due to the dispersant. NC-B0.5 showed a similar level of firmness to P-U, but after hitting 250 mm, B Agent seems to have a significant effect on liquidity improvement.Both NC-A1.0 and NC-B1.0 seem to have increased flow due to excessive dispersion.

  • PDF

램파를 이용한 2.25Cr-lMo재의 열화평가에 관한 연구 (A Study on Degradation Estimation of 2.25Cr-1Mo Steel Using Ultrasonic Lamb Wave)

  • 이상용;박익근;박은수;권숙인;조윤호
    • 한국공작기계학회:학술대회논문집
    • /
    • 한국공작기계학회 2001년도 추계학술대회(한국공작기계학회)
    • /
    • pp.324-329
    • /
    • 2001
  • The destructive method is reliable and widely used for the estimation of material degradation but, it have time-consuming and a great difficulty in preparing specimens from in-service industrial facilities. Therefore, the estimation of degraded structural materials by nondestructive evaluation is strongly desired. In this paper, the use of guided wave was suggested for the evaluation of thermally damaged 2.25 Cr-lMo steel as an alternative way to compensate for limitations of fracture tests. The observation of microstructure variations of the material including carbide precipitation increase and spheroidization near grain boundary was conducted and the correlation with the guided wave features such as energy loss ratio and group velocity changes was investigated. Through this study, the feasibility of ultrasonic guided wave evaluation for thermally damaged materials was explored.

  • PDF

Recent Advances in Scanning Acoustic Microscopy for Adhesion Evaluation of Thin Films

  • Ju, Hyeong-Sick;Tittmann, Bernhard R.
    • 비파괴검사학회지
    • /
    • 제29권6호
    • /
    • pp.534-549
    • /
    • 2009
  • As the thin film technology has emerged in various fields, adhesion of the film interface becomes an important issue in terms of the longevity and durability of thin film devices. Diverse nondestructive methods utilizing acoustic techniques have been developed to assess the interfacial integrity. As an effective technique based on the ultrasonic wave focusing and the surface acoustic wave(SAW) generation, scanning acoustic microscopy(SAM) has been investigated for adhesion evaluation. Visualization of film microstructures and quantification of adhesion weakness levels by SAW dispersion are the recent achievements of SAM. To overcome the limitations in the theoretical dispersion model only suitable for perfectly elastic and isotropic materials, a new model has been more recently developed in consideration of film anisotropy and viscoelasticity and applied to the adhesion evaluation of polymeric films fabricated on semiconductive wafers.

SiC Whisker의 분산과 $Al_2O_3-SiC Whisker$ 복합재료의 기계적 성질 (SiC-Whisker Dispersion and Mechanical Properties of $Al_2O_3-SiC Whisker$ Whisker Composite)

  • 정수종;이주완;김득중;신유선;강석중
    • 한국세라믹학회지
    • /
    • 제30권6호
    • /
    • pp.492-498
    • /
    • 1993
  • The pretreatment condition for uniform distribution of SiC whisker in A2O3-SiCw composites has been determined and the mechanical properties of the composites with various whisker contents have been measured. Good dispersion of the whisker can be obtained in a solution of pH=10.45 by ball milling and ultrasonic treatment. The relative density of hot pressed composites decreases with the whisker content up to 40vol%, but is found to be satisfactory, over 98% for all samples. The mechanical property of the composites is sensitive to the whisker dispersion. Uniform distributjion of the whisker is critical in order to guarantee good mechanical property.The samples containing 20~30vol% whisker show the best mechanical property within the studied range.

  • PDF

Effect of Atmospheric Plasma Treatments on Mechanical Properties of VGCF/Epoxy

  • Khuyen, Nguyen Quang;Kim, Jin-Bong;Kim, Byung-Sun;Lee, Soo
    • Advanced Composite Materials
    • /
    • 제17권2호
    • /
    • pp.167-175
    • /
    • 2008
  • Vapor grown carbon fibers (VGCF) were treated with atmospheric plasma enhancing the surface area in order to improve the bonding to the matrix in epoxy composites. The changes in the mechanical properties of VGCF/epoxy nanocompostes, such as tensile modulus and tensile strength were investigated in this study. VGCF with and without atmospheric plasma treatment for surface modification were used in this investigation. The interdependence of these properties on the VGCF contents and interfacial bonding between VGCF/epoxy matrix were discussed. The mechanical properties of atmospheric plasma treated (APT) VGCF/epoxy were compared with raw VGCF/epoxy. The tensile strength of APT VGCF/epoxy nanocomposites showed higher value than that of raw VGCF. The tensile strength was increased with atmospheric plasma treatment, due to better adhesion at VGCF/epoxy interface. The tensile modulus of raw VGCF and APT VGCF/epoxy matrix were of the similar value. The dispersion of the VGCF was investigated by scanning electron microscopy (SEM), SEM micrographs showed an excellent dispersion of VGCF in epoxy matrix by ultrasonic method.

Effect of Ultrasound on the Mechanical Properties of Electrodeposited Ni-SiC Nano Composite

  • Gyawali, Gobinda;Cho, Sung-Hun;Woo, Dong-Jin;Lee, Soo-Wohn
    • 한국재료학회지
    • /
    • 제20권8호
    • /
    • pp.439-443
    • /
    • 2010
  • Nano sized SiC particles (270 nm) are easily agglomerated in nickel sulfamate electrolytic bath during a composite electrodeposition process. The agglomeration of nano particles in composite coatings can significantly reduce the mechanical properties of the composite coatings. In this study, Ni-SiC nano composite coatings were fabricated using a conventional electrodeposition process with the aid of ultrasound. Nano particles were found to be distributed homogeneously with reduced agglomeration in the ultrasonicated samples. Substantial improvements in mechanical properties were observed in the composite coatings prepared in presence of ultrasound over those without ultrasound. Ni-SiC composite coatings were prepared with variable ultrasonic frequencies ranging from 24 kHz to 78 kHz and ultrasonic powers up to 300 watts. The ultrasonic frequency of 38 kHz with ultrasonic power of 200 watt was revealed to be the best ultrasonic conditions for homogeneous dispersion of nano SiC particles with improved mechanical properties in the composite coatings. The microstructures, phase compositions, and mechanical properties of the composite coatings were observed and evaluated using SEM, XRD, Vickers microhardness, and wear test. The Vickers microhardness of composite coatings under ultrasonic condition was significantly improved as compared to the coatings without ultrasound. The friction coefficient of the composite coating prepared with an ultrasonic condition was also smaller than the pure nickel coatings. A synergistic combination of superior wear resistance and improved microhardness was found in the Ni-SiC composite coatings prepared with ultrasonic conditions.

가공액의 초음파 진동 및 절연 공구를 이용한 미세방전가공 (Micro Hole Machining by EDM Using Insulated Tool Combined with Ultrasonic Vibration of Dielectric Fluid)

  • 박민수;정도관;이강희;주종남
    • 한국생산제조학회지
    • /
    • 제20권2호
    • /
    • pp.180-186
    • /
    • 2011
  • This paper describes a micro electrical discharge machining (MEDM) technique that uses an insulated tool in combination with ultrasonic vibration to drill micro holes. As the machining depth becomes deeper, the dispersion of debris and circulation of the dielectric fluid are difficult to occur. Consequently, machining becomes unstable in the machining region and unnecessary electrochemical dissolution and secondary discharge sparking occur at the tool side face. To reduce the amount of unnecessary side machining, an insulated tool was used. Ultrasonic vibration was applied to the MEDM work fluid to better remove debris. Through these methods, a $1000\;{\mu}m$ thick stainless steel plate was machined by using a $73\;{\mu}m$ diameter electrode. The diameters of the hole entrance and exit were $96\;{\mu}m$ and $88\;{\mu}m$, respectively. It took only 351s to completely drill one hole.

유도초음파를 이용한 장거리 배관 탐상기법 (Long Range Ultrasonic Guided Wave Techniques for Inspection of Pipes)

  • 박익근;김용권;김현묵;송원준;조용상;안연식
    • Journal of Welding and Joining
    • /
    • 제23권5호
    • /
    • pp.43-48
    • /
    • 2005
  • Conventional non-destructive techniques for inspection of the weld in pipelines require significant test time and high cost. Ultrasonic guided waves have been widely studied and successfully applied to various non-destructive tests with advantage of the long-range inspection. In this paper, a study on the application of ultrasonic guided waves to the long-range inspection of the pipeline is presented using a long-range guided wave inspection system, Wavemaker SE16, GUL. The characteristics and setup of the long-range guided wave inspection system and experimental results in pipes of with various diameter are introduced. The experimental results in mock-up pipes with cluster type detects show that the minimum detectable wall thickness reduction with this guided wave system is $2\~3\%$ in the pipe cross section area. And the wall thickness reduction of $5\%$ in cross section area can be detected when actual detection level is used. Therefore, the applicability of the guided wave systeme to long-range inspection of wall thickness reduction in pipes is verified.