• Mass Spectrometry Letters
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• v.7 no.2
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• pp.50-54
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• 2016

Multi-collector inductively coupled plasma mass spectrometry (MC-ICP-MS) is currently used in our laboratory for isotopic and quantitative analyses of nuclear materials at ultra-trace levels in environmental swipe samples, which is a very useful for monitoring undeclared nuclear activities. In this study, to improve measurement precisions of uranium isotopes at ultratrace levels, we adopted a desolvating nebulizer system (Aridus-II, CETAC., USA), which can improve signal sensitivity and reduce formation of uranium hydride. A peristaltic pump was combined with Aridus-II in the sample introduction system of MC-ICP-MS to reduce long-term signal fluctuations by maintaining a constant flow rate of the sample solution. The signal sensitivity in the presence of Aridus-II was improved more than 10-fold and the formation ratio of UH/U decreased by 16- to 17- fold compared to a normal spray chamber. Long-term signal fluctuations were significantly reduced by using the peristaltic pump. Detailed optimizations and evaluations with uranium standards are also discussed in this paper.

• Journal of the Korean Society for Nondestructive Testing
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• v.27 no.2
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• pp.183-189
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• 2007

Ultra precise processed parts are required together with the development of optoelectronics industry. As important parts of optoelectronics industry, there are ferrule of optical connector and lens for optical devices. In particular, the lens requires high reliability with high precision without including flaws. These optical modules need ultra precise processing in order to reduce the loss of light sources and various nondestructive inspections are carried out in the finishing stage to separate good and bad quality products. Therefore, it was analyzed through the characteristics of response of amplitude and resonant frequency according to the mass variations of aspheric lens that is used currently in laser printers.

• Journal of Satellite, Information and Communications
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• v.11 no.4
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• pp.81-88
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• 2016

In this paper, we propose an adaptive multi-target estimation algorithm using the characteristics of signals in the IR-UWB(Impulse-Radio Ultra Wideband) radar system, which is attracting attention because it has good transparency, robustness to the indoor environment, and high precision positioning of tens of centimeters. We proposed an algorithm that estimates multiple peaks with the characteristic that the signal reflected by the target has a peak. To verify the performance of these algorithms, multiple targets were placed in front of the radar and the existing technique and the multi - target estimation algorithm were compared. The location of the targets is estimated in real time with one transmitting antenna and one receiving antenna. The number of estimates can be increased compared with the existing peak signal derivation method, and multiple targets can be derived. The conventional technique estimates only one target, which results in a mean square error of 1 while a multi - target estimation algorithm yields a result of about 0.05. The proposed method is expected to be able to apply multiple targets to the estimation and application in one IR-UWB module environment.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.20 no.11
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• pp.1178-1185
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• 2009

In this paper, a wideband ultra-high speed & high purity discrete frequency synthesizer having minimum 2.5 MHz step size was proposed. To achieve fast and wideband operation, discrete frequencies were synthesized by mixing of 3 different pre-synthesized 16 frequencies made from fixed PLL and frequency dividers. Frequencies with discrete 2.5 MHz step were produced in 710~1,610 MHz. The measured hopping response time was 350 nsec average, output level was 21.5 dBm average with 2.65 dB flatness, spurious and harmonics level were suppressed below -60 dBc, and phase noise was -94 dBc/Hz@100 Hz. Also, a new measurement method for synthesizer response time was described.

• Korean Journal of Veterinary Service
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• v.39 no.2
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• pp.81-86
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• 2016

Honeybee venom (BV) from Apis mellifera L. has been used as natural antimicrobial compounds in pigs, cows, dairy cattle and chicken farms in Korea. The purpose of this study was conducted to confirm homogeneity and stability of BV dissolved with distilled water or saline solution. Melittin was analyzed with ultra-high performance liquid chromatography (UPLC) for BV to secure the validation of analysis. BV at concentration of 1 mg/mL was dissolved with distilled water or saline solution at room temperature. Homogeneity of BV dissolved with distilled water or saline solution at upper, milddle, and lower layers all satisfied the accuracy and precision criteria. Stability of BV dissolved with distilled water or saline solution for 7 days all satisfied the criterion both light and dark storage condition. BV has satisfied with homogeneity and stability in distilled water or saline solution at room temperature under light or dark condition. The results of this study suggest that BV has a possibility as the substitute of natural antimicrobial agents for the animal drugs and feed additives.

• Korean Journal of Optics and Photonics
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• v.24 no.2
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• pp.77-85
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• 2013

The precision of retardation measurement has been improved upto $3{\sigma}$ <0.005 nm after improvements are made to the conventional transmission ellipsometer. Improvements are made such that, i) the polarizer module instead of the sample stage is rotated, ii) the light source is replaced, iii) the starting points of two rotating modules are accurately synchronized, and iv) the fine background retardation is compensated. Together with the newly introduced RVD (Retardation Vector Difference) method, the improved instrument is successfully applied to characterize the ultra small optical birefringence of the rubbed polyimide alignment layer, after the residual retardation due to glass substrate whose magnitude is about 1.0 nm is properly subtracted. It is verified that the net retardation of the alignment layer ranges from 0.05 nm to 0.15 nm.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.08a
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• pp.255-255
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• 2010

Recently, nonvolatile memories (NVM) of various types have been researched to improve the electrical performance such as program/erase voltages, speed and retention times. Also, the charge trap memory is a strong candidate to realize the ultra dense 20-nm scale NVM. Furthermore, the high charge efficiency and the thermal stability of SiC nanocrystals NVM with single $SiO_2$ tunnel barrier have been reported. [1-2] In this study, the SiC charge trap NVM was fabricated and electrical properties were characterized. The 100-nm thick Poly-Si layer was deposited to confined source/drain region by using low-pressure chemical vapor deposition (LP-CVD). After etching and lithography process for fabricate the gate region, the $Si_3N_4/SiO_2/Si_3N_4$ (NON) and $SiO_2/Si_3N_4/SiO_2$ (ONO) barrier engineered tunnel layer were deposited by using LP-CVD. The equivalent oxide thickness of NON and ONO tunnel layer are 5.2 nm and 5.6 nm, respectively. By using ultra-high vacuum magnetron sputtering with base pressure 3x10-10 Torr, the 2-nm SiC and 20-nm $SiO_2$ were successively deposited on ONO and NON tunnel layers. Finally, after deposited 200-nm thick Al layer, the source, drain and gate areas were defined by using reactive-ion etching and photolithography. The lengths of squire gate are $2\;{\mu}m$, $5\;{\mu}m$ and $10\;{\mu}m$. The electrical properties of devices were measured by using a HP 4156A precision semiconductor parameter analyzer, E4980A LCR capacitor meter and an Agilent 81104A pulse pattern generator system. The electrical characteristics such as the memory effect, program/erase speeds, operation voltages, and retention time of SiC charge trap memory device with barrier engineered tunnel layer will be discussed.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.3
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• pp.31-40
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• 2017

This paper deals with the high precision of GPS measurement reduction and its implementation on near real-time and kinematic mode for those applications requiring centimeter-level precision of the estimated coordinates, even if target stations are a few hundred kilometers away from their references. We designed the system architecture, data streaming and processing scheme. Intensive investigation was performed to determine the characteristics of the GPS medium-range functional model, IGS infrastructure and some exemplary systems. The designed system consisted of streaming and processing units; the former automatically collects GPS data through Ntrip and IGS ultra-rapid products by FTP connection, whereas the latter handles the reduction of GPS observables on static and kinematic mode to a time series of the target stations' 3D coordinates. The data streaming unit was realized by a DOS batch file, perl script and BKG's BNC program, whereas the processing unit was implemented by definition of a process control file of BPE. To assess the functionality and precision of the positional solutions, an experiment was carried out against a network comprising seven GPS stations with baselines ranging from a few hundred up to a thousand kilometers. The results confirmed that the function of the whole system properly operated as designed, with a precision better than ${\pm}1cm$ in each of the positional component with 95% confidence level.

• Journal of Broadcast Engineering
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• v.26 no.4
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• pp.409-418
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• 2021

Conformal coating is a technology that protects PCB(Printed Circuit Board) and minimizes PCB failures. Since the defects in the coating are linked to failure of the PCB, the coating surface is examined for air bubbles to satisfy the successful conditions of the conformal coating. In this paper, we propose an algorithm for detecting problematic bubbles in high-risk groups by applying image signal processing. The algorithm consists of finding candidates for problematic bubbles and verifying candidates. Bubbles do not appear in visible light images, but can be visually distinguished from UV(Ultra Violet) light sources. In particular the center of the problematic bubble is dark in brightness and the border is high in brightness. In the paper, these brightness characteristics are called valley and mountain features, and the areas where both characteristics appear at the same time are candidates for problematic bubbles. However, it is necessary to verify candidates because there may be candidates who are not bubbles. In the candidate verification phase, we used convolutional neural network models, and ResNet performed best compared to other models. The algorithms presented in this paper showed the performance of precision 0.805, recall 0.763, and f1-score 0.767, and these results show sufficient potential for bubble test automation.

• Journal of the Korean Wood Science and Technology
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• v.44 no.3
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• pp.337-349
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• 2016

In this study, an analytical method to evaluate the quality of isoflavonoid compounds purified and isolated from the fruits of Cudrania tricuspidata was developed and validated using Ultra Performance Liquid Chromatography (UPLC). The fruits of C. tricuspidata were extracted with methanol and further fractioned with n-hexane, ethyl acetate and water. The resulting ethyl acetate extract separated into four isoflavonoid compounds by a combination of silica gel and sephadex LH-20 column chromatography. The structures of the compounds were elucidated as alpinumisoflavone, 6,8-diprenyl genistein, 6,8-diprenyl orobol, 4'-O-methylalpinumisoflavone by various techniques such as UV-Vis, ESI-MS, $^1H\;NMR$ and $^{13}C\;NMR$ spectroscopy. Finally, a method to characterize the compounds was developed by using the UPLC equipped with a $C_{18}$ column and a gradient mobile phase system consisting of 2% acetic acid in water (solvent A) and 2% acetic acid in methanol (solvent B). The developed method was validated with the parameters such as selectivity, linearity, limit of detection, limit of quantitation, accuracy, and precision, which are defined by the ICH (International Conference on Harmonization). Using the validated method, the compounds in the fruits harvested in different months were also quantitatively analyzed. We propose this approach this approach can readily be utilized as an efficient evaluation method to quantify the extracts of C. tricuspidata.