• Korean Journal of Metals and Materials
• /
• v.49 no.10
• /
• pp.811-817
• /
• 2011

In this study, we have investigated the role of a metal oxide hole injection layer (HIL) between an Indium Tin Oxide (ITO) electrode and an organic hole transporting layer (HTL) in organic light emitting diodes (OLEDs). Nickel Oxide films were deposited at different deposition times of 0 to 60 seconds, thus leading to a thickness from 0 to 15 nm on ITO/glass substrates. To study the influence of NiO film thickness on the properties of OLEDs, the relationships between NiO/ITO morphology and surface properties have been studied by UV-visible spectroscopy measurements and AFM microscopy. The dependences of the I-V-L properties on the thickness of the NiO layers were examined. Comparing these with devices without an NiO buffer layer, turn-on voltage and luminance have been obviously improved by using the NiO buffer layer with a thickness smaller than 10 nm in OLEDs. Moreover, the efficiency of the device ITO/NiO (< 5 nm)/NPB/$Alq_3$/ LiF/Al has increased two times at the same operation voltage (8V). Insertion of a thin NiO layer between the ITO and HTL enhances the hole injection, which can increase the device efficiency and decrease the turn-on voltage, while also decreasing the interface roughness.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2009.11a
• /
• pp.146-146
• /
• 2009

최근에 광도전체와 형광체를 기반으로 평판형 디지털 방사선 검출기의 상업적 발전가능성에 많은 관심을 가지고 있다. 본 연구는 기존의 직접변환방식에 널리 사용되었던 비정질 셀레늄 (amorphous selenium) 기반의 디지털 방사선 검출기보다 높은 전기적신호 및 동작특성을 가지는 물질층을 제작하기 위해 High Purity (99.99%)의 상용화된 $PbI_2$를 특수용매에 담가두었다가 약 1시간동안 Biology 초음파 처리한 후 농축기를 사용하여 건조된 $PbI_2$를 3Roll-milling을 사용하여 미세크기의 Powder를 얻어내었다. 합성된 $PbI_2$ Powder를 PIB(Particle-in-Binder)법을 이용하여 전도성을 가진 ITO(Indium-tin-oxide)코팅된 유리판에 제작된 필름의 상부에 Magnetron sputtering system 을 사용하여 전극을 $1cm{\times}1cm$의 크기로 증착하였다. I-V 테스트를 통하여 X선 조사시 $PbI_2$필름의 Sensitivity, Dark current, SNR(signal-to-noise ratio)을 측정하여 필름의 전기적 검출 특성을 정량적으로 평가하였고 SEM(scanning electron microscope)을 통하여 입자의 크기를 관찰하였다.

• Journal of Powder Materials
• /
• v.16 no.4
• /
• pp.268-274
• /
• 2009

For the purpose of obtaining basic information on the development of lead-free materials, a high density composites (a) W-Cu, (b) W-Sn (c)W-Cu-Sn and (d) W-Cu-Ni were fabricated by the P/M method. The particle size of used metal powders were under 325 mesh, inner size of compaction mould was $\phi8$ mm, and compaction pressure was 400 MPa. A High density composite samples were sintered at a temperature between $140^{\circ}C$ and $1050^{\circ}C$ for 1 hour under Ar atmosphere. The microstructure, phase transformation and physical properties of the sintered samples were investigated. As the results, the highest relative density of 95.86% (10.87 g/$cm^3$) was obtained particularly in the sintered W-Cu-Sn ternary system sample sintered at 450 for 1hr. And, Rockwell hardness (HRB) of 70.0 was obtained in this system.

• Journal of Powder Materials
• /
• v.19 no.4
• /
• pp.271-277
• /
• 2012

$SnO_2$ nanotubes were successfully synthesized using an electrospinning technique followed by calcination in air. The nanotubes were the single phase nature of $SnO_2$ and consisted of approximately 14 nm nanocrystals. SEM and TEM characterizations demonstrated that uniform hollow fibers with an average outer diameter of around 124 nm and wall thickness of around 25 nm were successfully obtained. As anode materials for lithium ion batteries, the $SnO_2$ nanotubes exhibited excellent cyclability and reversible capacity of $580mAhg^{-1}$ up to 25 cycles at $100mAg^{-1}$ as compared to $SnO_2$ nanoparticles with a capacity of ${\sim}200mAhg^{-1}$. Such excellent performance of the $SnO_2$ nanotube was related to the one-dimensional hollow structure which acted as a buffer zone during the volume contraction and expansion of Sn.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2000.01a
• /
• pp.145-146
• /
• 2000

Primary emphasis was placed on the electrophoretic deposition of low voltage phosphor to indium-tin oxide-coated glass for the application of field emission display. The phosphor deposited by various parameters, such as deposition time and applied voltages was examined in detail. In addition, a comparison was made by analyzing luminance properties of the phosphor mixed with and without conducting $In_2O_3$ powder of less than 1um size. The measurement was performed as a function of $In_2O_3$ concentration from 3% to 15% by weight. The enhanced impact of indium powder mixing on the phosphor was clearly demonstrated by aging performance curve at 1000V excitation voltages with a current density of $1\;mA/cm^2$

• Journal of Powder Materials
• /
• v.28 no.6
• /
• pp.455-461
• /
• 2021

In this study, multilayered SnO nanoparticles are prepared using oleylamine as a surfactant at 165℃. The physical and chemical properties of the multilayered SnO nanoparticles are determined by transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). Interestingly, when the multilayered SnO nanoparticles are heated at 400℃ under argon for 2 h, they become more efficient anode materials, maintaining their morphology. Heat treatment of the multilayered SnO nanoparticles results in enhanced discharge capacities of up to 584 mAh/g in 70 cycles and cycle stability. These materials exhibit better coulombic efficiencies. Therefore, we believe that the heat treatment of multilayered SnO nanoparticles is a suitable approach to enable their application as anode materials for lithium-ion batteries.

• Proceedings of the Korean Vacuum Society Conference
• /
• 2012.08a
• /
• pp.415-415
• /
• 2012

ICP (RF) 열 플라즈마 분말 합성법은 초고온 열플라즈마(~10,000 K) 속으로 원료물질을 투입한 뒤, 용융, 기화 및 재합성의 과정을 거쳐 초미분(<1 ${\mu}s$)을 합성하는 방법으로 고출력 시스템의 경우 고온/고 엔탈피 열 유동을 통한 고융점 및 저융점 복합물질의 동시 기화에 의한 물질 조성이 제어된 나노 복합체의 대량 합성이 가능할 것으로 기대되고 있다. 본 연구에서는 전북대학교 고온플라즈마 응용연구센터의 60&200 kW의 고출력 ICP (RF) 열 플라즈마 시스템을 이용하여 LTO (Lithium Titanium Oxide)와 IZTO (Indium Zinc Tin Oxide), Barium Borosilicate Glass (K2O-BaO-B2O3-SiO2)의 다성분계 나노 복합체를 합성하였으며, FE-SEM, TEM, XRD, ICP-OES를 이용하여 그 특성을 분석하였다.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2002.07b
• /
• pp.988-991
• /
• 2002

ITO (Indium Tin Oxide) powder was synthesized by precipitation method. ITO colloidal solutions for coating on glass were fabricated by ball milling method. ITO colloidal solution with variation of concentration from 2% to 15% were fabricated ITO thin film measured sheet resistance and transmittance. In the result, 15% sol showed the lowest value of sheet resistance, 2% sol showed the highest value of transmittance. In addition, effect of annealing temperature and $SiO_2$ film were investigated.

• Journal of environmental and Sanitary engineering
• /
• v.19 no.1
• /
• pp.42-49
• /
• 2004

The study was carried out in order to improve the quality of fermented soybean, that is, Doenjang with strain ,mold and bactea, added mulberry leaves powder were investigated and analyzed as follows. 1. The water content of samples was 38.51-50.10%, pH value 5.44-6.21 and total acidity, 2.42-3.13 2. The reducing sugar of content for samples was 7.01-7.24% on contrast mulberry added sample was 8.34-12.11%, Amino-N as contrast 5.96-7.63% mulberry added, 8.34-12.11% 3. In sensory evaluation test, excellent results was 2% added sample than others. 4. The heaby metals analyzed form samples cans, iron, tin and lead content of samples were 5.63-6.03 ppm, 31.70-35.53 ppm and trace.

• Journal of the Korean Electrochemical Society
• /
• v.10 no.2
• /
• pp.88-93
• /
• 2007

Nano-sized Sn particles were coated with Ni-P layer using an electroless deposition method and their anodic performance was tested for lithium secondary batteries. Uniform coating layers were obtained, of which the thickness was controlled by varying the $Ni^{2+}$ concentration in the plating bath. It was found that the Ni-P layer plays two important roles in improving the anodic performance of Sn powder electrode. First, it prevents the inter-particle aggregation between Sn particles during the charge/discharge process. Second, it provides an electrical conduction pathway to the Sn particles, which allows an electrode fabrication without an addition of conductive carbon. A pseudo-optimized sample showed a good cyclability and high capacity ($>400mAh\;g^{-1}$) even without conductive carbon loading.