• Title/Summary/Keyword: Thin section

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Effect of rock mineralogy on mortar expansion

  • Karaman, Kadir;Bakhytzhan, Aknur
    • Geomechanics and Engineering
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    • v.20 no.3
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    • pp.233-241
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    • 2020
  • Alkali-silica reaction (ASR) is among one of the most important damaging mechanisms in concrete, depending primarily on aggregates which contain reactive minerals. However, expansion in concrete may not directly relate to the reactive minerals. This study aims to investigate the influence of ASR and the expansion of mortar bars depending on aggregate type containing various components such as quartz, clay minerals (montmorillonite and kaolinite) and micas (muscovite and biotite). In this study, the accelerated mortar bar tests (AMBT) were performed in two conditions (mortar bars in the same and sole NaOH solutions). Petrographic thin section studies, X-ray diffraction (XRD) analysis (Rietveld method), scanning electron microscopy (SEM) and chemical analyses were carried out. This study showed that quartzite bars led to increase in expansion values of mortar bars in diabase-1 and andesite when these were in the same NaOH solution. However, three samples (basalt, quartzite and claystone) were found having ASR expansion based on the AMBT when the special molds were used for each sample. SEM study revealed that samples which exhibit highest expansions according to AMBT had a generally rough surface and acicular microstructures in or around the micro-cracks. Basalt and quartzite showed more variable in major oxides than those of other samples based on the chemical analyses, SEM studies and AMBT. This study revealed that the highest expansions were observed to source not only from reactive aggregates but also from alteration products (silicification, chloritization, sericitization and argillisation), phyllosilicates (muscovite, biotite and vermiculite) and clays (montmorillonite and kaolinite).

A Study on the Si-SiO$_2$Interface State Characteristics of Nonvolatile SNOS FET Memories using The Charge Pumping Method (Charge Pumping 방법을 이용한 비휘발성 SNOS FET기억소자의 Si-SiO$_2$계면상태 특성에 관한 연구)

  • 조성두;이상배;문동찬;서광열
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1992.05a
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    • pp.82-85
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    • 1992
  • In this study, charge pumping method was used to investigate the Si-SiO$_2$interface characteristics of the nonvolatile SNOSFET memory devices, fabricated using the CMOS 1 Mbit processes (1.2$\mu\textrm{m}$ design rule), with thin oxide layer of 30${\AA}$ thick and nitride layer of 525${\AA}$ thick on the n-type silicon substrate (p-channel). Charge pumping current characteristics with the pulse base level were measured for various frequencies, falling times and rising times. By means of the charge dynamics in a non-steady state, the average Si-SiO$_2$interface state density and capture cross section were determined to be 3.565${\times}$10$\^$11/cm$\^$-2/eV$\^$-1/ and 4.834${\times}$10$\^$-16/$\textrm{cm}^2$, respectively. However Si-SiO$_2$ interface state densities were disributed 2.8${\times}$10$\^$-11/~5.6${\times}$10$\^$11/cm$\^$-2/~6${\times}$10$\^$11/cm$\^$-2/eV$\^$-1/ in the lover half of energy gap.

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A Behavior of the Wet Etching of CoNbZr/Cu/CoNbZr Multi-Layer Films (CoNbZr/Cu/CoNbZr 다층막의 습식 식각 거동)

  • 김현식;이영생;송재성;오영두;윤재홍
    • Electrical & Electronic Materials
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    • v.10 no.7
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    • pp.645-650
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    • 1997
  • We manufactured CoNbZr/Cu/CoNbZr multi-layer films by rf magnetron sputtering methods and formed the patterns on the deposited multi-layer films. In this study, we fabricated a new etchant for forming the patterns by the wet etching with etchant and we searched for the best etching conditions and the etchant composition. Cu was etched selectively independent on the concentration of iron chloride solution, but amorphous CoNbZr thin film did not. The etchant was achieved by iron chloride solution(17.5 mol%) mixed with HF (20 mol%) during 150 sec, which etched CoNbZr/Cu/CoNbZr multi-layer films at the same time. Also, the etchant etched CoNbZr/Cu/CoNbZr multi-layer films by the three-step. It was shown that the cross-section had the isotropic structure and excellent etching characteristics with the above etchant.

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Electron Microscopic Studies on Cellular Characteristics and Transport Systems in Tight Epithelia (Tight epithelia의 세포특성과 수송체계에 관한 전자현미경적 연구)

  • Jeon, Jin-Seok
    • Applied Microscopy
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    • v.26 no.1
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    • pp.47-57
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    • 1996
  • This study analysed the transport properties of bladder mucosa known as the typical system of 'tight epithelia' by using TEM observation with both rapid freeze-fracture electron microscopy and thin-section method and mainly analysed the cellular characteristics of turtle bladder epithelial cells. The bladder epithelium, like other tight epithelia, consists of a heterogenous population of cells. The majority of the mucosal cells are the granular cells and may function primarily in the process of active $Na^+$ reabsorption in turtle bladder. The remaining two types of cells are rich in mitochondria and is believed to be res-ponsible for a single major transport system, namely, $H^+$ transport by A-type of cell and urinary $HCO_{3}^-$ secretion by B-type of cell. As viewed in freeze-fracture electron micrograph, the tight junctions form a continuous tight seal around the epithelial cells, thus restricting diffusion in tight epithelia. In addition, the apical surface membranes have a population of rod-shaped intramembranous particles (IMPs). It is believed that these IMPs probably represent the components of the proton pump. However, it is likely that these characteristics of the apical transporter remain to be clarified in tight epithelial cells.

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FCCL 제작 시 Cu Sputter 조건에 따른 Through Hole 특성 연구

  • Kim, Sang-Ho;Yun, Yeo-Wan
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2008.11a
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    • pp.15-16
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    • 2008
  • In case manufacturing COF, through hole should be made to be used for a pathway connecting the conductive layers of its both faces. In case Cu-plating inside of through hole with electroless plating way, contact between Cu and PI film gets bad to be fell apart from PI by the impact of applying to the electric devices. Therefore, after sputtering is applying on inner through hole, then a method to perform electroplating process. In this study, after changing sputtering condition to manufacture FCCL, we looked the changeability of the upper PI and inner hole Cu layers. Making use of RF Magnetron sputtering equipment, we coated Cu thin film and Cu-plated on it through electroplating. After cold-mounting the completed FCCL, we examined hole section through an optical microscope. From the result of test, with parameters deposition pressure and deposition time, both the thickness of the hole plated layer and PI plated upper layer increased at regular rate, increasing the thickness of Cu sputter layer. However, from the result of test in increasing RF-power, we could know the increment rate of hole plated layer is considerably greater than that of PI plated upper layer. Therefore, we finally acquired good result; if you want only to increase the plated layer of inner hole, it's much better to increase RF-power.

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Heat Resistance Properties of Thin Section HiSiMo Ductile Iron for Exhaust Manifold (배기 매니폴드용 박육 고규소 구상흑연주철의 내열 특성)

  • Lee, Do-Kyung;Kim, Sung-Gyu;Lee, Byung-Woo
    • Journal of Power System Engineering
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    • v.17 no.4
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    • pp.109-114
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    • 2013
  • In this study, the microstructure, mechanical properties and high temperature oxidation characteristics of HiSiMo and HiSiMoM ductile iron for exhaust manifold were investigated. The HiSiMoM ductile iron was developed by optimization of alloying element addition and casting design. The exhaust manifold prototype was fabricated using the HiSiMoM iron and this resulted in the weight saving of 0.73kg. The microstructures of the HiSiMo and HiSiMoM irons were similar each other and graphite nodularity was 89% and 93% respectively. Tensile strengths of them were 663.5 and 674.4 MPa and Brinell hardness were 235.3 and 243.9 respectively. Both irons showed parabolic weight gain behavior in high temperature oxidation atmosphere. Oxidation layer was divided into external and internal layers. The weight gain of the HiSiMoM iron was lower than that of the HiSiMo iron after isothermal oxidation test at $900^{\circ}C$. This should be rationalized by higher Si enrichment at the interface of the matrix and internal layer of the HiSiMoM iron.

A Study on Sound Radition from the Periodic Structure depend on Symmetrical beam space Using FEM (FEM을 이용한 대칭형 보강재에 보강된 평판의 음향방사에 관한 연구)

  • Kim J.T.;Kim T.H.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.10a
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    • pp.732-739
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    • 2005
  • The determination of sound pressure radiated from periodic plate structures is fundamental in the estimation of noise level in aircraft fuselages or ship hull structures. As a robust approach to this problem, here a very general and comprehensive analytical model is developed for predicting the sound radiated by a vibrating plate stiffened by periodically spaced orthogonal symmetrical beams subjected to a sinusoidally time varying point load. In this these, we experiment with the numerical analysis using the space harmonic series and the SYSNOISE for measuring the vibration mode and character of response caused by sound radiation with adding the harmonic point force in the thin isotropic plate supported by the rectangular lattice reinforcement. We used the reinforcements, beams of open type section like the style of 'ㄷ' letter; the space of the beams were chosen to be 0.2m, 0.3m, 0.4m. We studied the behavior of sound pressure levels, analysis of vibration mode between support points, connection between frequency function and sound pressure levels, and connection between position function and sound pressure levels.

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Capabilities of 1D CUF-based models to analyse metallic/composite rotors

  • Filippi, Matteo;Carrera, Erasmo
    • Advances in aircraft and spacecraft science
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    • v.3 no.1
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    • pp.1-14
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    • 2016
  • The Carrera Unified Formulation (CUF) is here extended to perform free-vibrational analyses of rotating structures. CUF is a hierarchical formulation, which enables one to obtain refined structural theories by writing the unknown displacement variables using generic functions of the cross-section coordinates (x, z). In this work, Taylor-like expansions are used. The increase of the theory order leads to three-dimensional solutions while, the classical beam models can be obtained as particular cases of the linear theory. The Finite Element technique is used to solve the weak form of the three-dimensional differential equations of motion in terms of "fundamental nuclei", whose forms do not depend on the adopted approximation. Including both gyroscopic and stiffening contributions, structures rotating about either transversal or longitudinal axis can be considered. In particular, the dynamic characteristics of thin-walled cylinders and composite blades are investigated to predict the frequency variations with the rotational speed. The results reveal that the present one-dimensional approach combines a significant accuracy with a very low computational cost compared with 2D and 3D solutions. The advantages are especially evident when deformable and composite structures are analyzed.

Dynamic Characteristics of Thermal Stratification Build-up by Unsteady Natural Convection (비정상 자연대류에 의한 온도성층화의 동특성에 관한 연구)

  • Kang, B.S.;Lee, J.S.;Lee, T.S.;Ro, S.T.
    • The Magazine of the Society of Air-Conditioning and Refrigerating Engineers of Korea
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    • v.17 no.4
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    • pp.382-394
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    • 1988
  • Dynamic characteristics of thermally-forced stratification process in a square enclosure with a linear temperature profile at the side walls have been investigated through flow visualization experiment and numerical analysis. The experiment was performed on air with the Rayleigh numbers of order $10^5$. A particle tracer method is used for the flow visualization and to obtain a sudden linear temperature profile at the side walls copper blocks which already have a linear temperature profile are come into contact with the thin copper plates of the test section. Immediately a meridional circulation is developed and heat transfer takes place from the wall to the interior region by circulation of fluid and finally a thermal stratification is achieved. In the numerical study, QUICK scheme for convective terms, SIMPLE algorithm for pressure correction, and the implicit method for the time marching are adopted for the integration of conservation equations. Comparison of flow visualization and numerical results shows that the developing flow patterns are very similar in dynamic nature even though there is a time lag due to the inevitable time delay in setting up a linear temperature profile. For high Rayleigh numbers, the oscillatory motion is likely to take place and stratified region is extended. However, initial temperature adjustment process is much slower than that for low Rayleigh numbers.

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Experimental Study on the Shear Capacity of Continuous Cap-Type Shear Connector (연속 캡 형상 전단연결재의 전단 내력에 관한 실험 연구)

  • Oh, Myoung Ho;Kim, Young Ho;Jeong, Sug Chang;Kim, Myeong Han
    • Journal of Korean Association for Spatial Structures
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    • v.19 no.2
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    • pp.91-99
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    • 2019
  • The push-out tests have been conducted on the specimens which consist of the steel beam with U-shape section and the continuous cap-type shear connector. Existing formulas for the elevation of shear connector capacity were investigated on the basis of test results. The shear capacities of continuous cap-type shear connectors distinctly declined as the diameters of side-hole in the shear connector increased. The rebars through side-hole for the transverse reinforcement improved the shear capacity of continuous cap-type connector by 20 to 30 percent. It was not feasible to obtain the appropriate capacity values of continuous cap-type shear connectors made of thin steel plate like those of in this study, using the existing formulas. The new formula for reflecting the shear strength of penetrative bars was proposed based on the shear equation of Eurocode 4. The slip capacities of continuous cap-type shear connectors were shown to exceed the limit value of 6mm for the sufficiently ductile behavior.