• Macromolecular Research
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• 제11권4호
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• pp.224-230
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• 2003

The blends of polypropylene (PP) with glass filled thermotropic liquid crystalline polymer (LCP-g) have been prepared by melt mixing techniques at different blend ratios. The thermal, dynamic mechanical, crystalline and morphological characteristics of these blends were investigated. Higher percent crystallinity was observed for 10% level of LCP-g in the blend in comparison to that of other blend ratios. The thermal stability increased with LCP-g concentration in the blend with PP. The variation of storage modulus, stiffness and loss modulus as a function of blend ratios suggested the phase inversion at the 50% level of LCP-g in the blend. The scanning electron microscopy (SEM) photographs showed the creation of voids and destruction of the fiber structures during the dynamic mechanical measurements. Processing behavior of the blends depended on the fiber forming characteristics of LCP-g, which again varied with the molding temperatures.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2020년도 봄 학술논문 발표대회
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• pp.66-67
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• 2020

The synthesis of stearic acid composite phase change material (PCM) was investigated and the samples produced were characterized for use in latent heat storage, using a simple chemical sol-gel process. The PCM was encapsulated to tetraethyl orthosilicate by various preparation ratios of stearic acid (5, 10, 15, 20, 30 and 50%). Fourier transformation infrared spectroscope (FT-IR) and X-Ray diffraction (XRD) were performed to determine the chemical structure and crystalloid phase of the microencapsulated PCM. SATEOS1 (5%) shows the best proportion for the PCM. With the presence of stearic acid as core materials and SiO2 as the supporting materials, it does not show any chemical reaction between both of them. SATEOS1 shows promising potential for thermal energy storage as it shows a better encapsulation efficiency and good thermal stability.

• 대한원격탐사학회:학술대회논문집
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• 대한원격탐사학회 2004년도 Proceedings of ISRS 2004
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• pp.452-455
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• 2004

MSC (Multi-Spectral Camera) system is a remote sensing instrument to obtain high resolution ground image. EOS (Electro-Optic System) for MSC mainly consists of PMA (Primary Mirror Assembly), SMA (Secondary Mirror Assembly), HSTS (High Stability Telescope Structure) and DFPA (Detector Focal Plane Assembly). High performance of EOS makes it possible for MSC system to provide high resolution and high quality ground images. Temperature of the EOS needs to be controlled to be in a specific range in order not to have any thermal distortion which can cause performance degradation. It is controlled by full redundant CPU based electronics. The validity of thermistor readings can be checked because a few thermistors are installed on each control point on EOS. Various kinds of thermal control logics are used to prevent 'Single Point Failure'. Control logic has a few set of database in order not to be corrupted by SEU (Single Event Upset). Even though the thermal control logic is working automatically, it can also be monitored and controlled by ground-station operator. In this paper, various ways of thermal control logic for EOS in MSC will be presented, which include thermal control mode and logic, redundancy design and status monitoring and reporting scheme.

• 전기학회논문지
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• 제57권5호
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• pp.803-807
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• 2008

A making process of DSC(dye sensitized solar cell) was presented. In general, Photo electrodes of DSC was made by using colloid paste of nano $TiO_2$ and processing of Doctor-blade printing and high temperature sintering for porous structure. These methods lead to cracks on $TiO_2$ surface and ununiform of $TiO_2$ thickness. This phenomenon is one factor that makes low efficiency to cells. After $TiO_2$ printing on TCO glass, a physical vibration was adapted for reducing ununiform of $TiO_2$ thickness. And a thermal treatment at low temperature(under $75^{\circ}C$) was adapted for reducing cracks on $TiO_2$ surface. In this paper, we have designed and manufactured an ultrasonic circuit (100W, frequency and duty variable) and a thermal equipment. Then, we have optimized forcing time, frequency and duty of ultrasonic irradiation and thermal heating for surface treatment of photo-electrode of DSC. In I-V characteristic test of DSC, ultrasonic and thermal treated DSC shows 19% improved its efficiency against monolithic DSC. And it shows stability of light-harvesting from drastically change of light irradiation test.

• Tribology and Lubricants
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• 제1권1호
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• pp.80-87
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• 1985

고온에서 화학적역안정성 및 기계적안정성의 섬유구조를 갖기 위해 lithim complex gellant로 정한 지방산과 $LiOH\cdot H_2O$ 및 boric acid의 이차연속검화반응으로 lithium dual complex 그리이스를 합성하였다. complex gellant의 양은 14%(NLGI 2호)가 적정량이었으며, 특히 castor wax를 1.5% 첨가했을때 이상적인 성능을 나타냈다. 이렇게 합성한 그리이스의 유분리성, 산화안정성, 내수성, 혼화안정성, 극압 및 내마모성은 ASTM 및 KS 방법에 준해 시험하였으며, 매우 우수한 특성을 지녔음을 알았다.

• 대한화학회지
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• 제68권2호
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• pp.87-92
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• 2024

The commercialization of rechargeable metal-air batteries is extremely desirable but designing stable oxygen reduction reaction (ORR) catalysts with non-noble metal still has faced challenges to replace platinum-based catalysts. The nonnoble metal catalysts for ORR were prepared to improve the catalytic performance and stability by the thermal decomposition of ZIF-8 with optimum cobalt loading. The porous carbon was obtained by the calcination of ZIF-8 and different loading amounts of Co nanoparticles were anchored onto porous carbon forming a Co/PC catalyst. Co/PC composite shows a significant increase in the ORR value of current and stability (500 h) due to the good electronic conductive PCN support and optimum cobalt metal loading. The significantly improved catalytic performance is ascribed to the chemical structure, synergistic effects, porous carbon networks, and rich active sites. This method develops a new pathway for a highly active and advantageous catalyst for electrochemical devices.

• Composites Research
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• 제33권5호
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• pp.309-314
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• 2020

우주 발사체용 극저온 추진제 탱크 경량화를 위한 고분자복합재료의 적용은 방향성을 가지는 복합재의 특성으로 인해 기체 투과도 성능 규명이 선행되어야 한다. 이러한 특성은 탱크 안정성 및 탑재 연료량 산정과 같은 성능 및 경제성과 직결된 지표다. 본 연구에서는 구조해석을 통해 도출된 극저온 추진제 탱크의 구조에 대하여 2가지 두께에 대한 투과도를 실험적으로 평가하였으며, 나아가 극저온-상온 환경에 노출된 열충격 횟수에 따른 시편의 비가역적 특성에 대한 투과도 분석 결과를 포함한다. 연구에 사용된 복합재는 두께에 반비례하며 열충격 횟수에 비례하는 투과도 특성을 보였으며, 우주 발사체용 극저온 추진제 탱크 소재로 적절한 투과도 성능을 가지는 것을 검증하였다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.289.2-289.2
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• 2016

In-Ga-Zn-O(IGZO) receive great attention as a channel material for thin film transistors(TFTs) as next-generation display panel backplanes due to its superior electrical and physical properties such as a high mobility, low off-current, high sub-threshold slope, flexibility, and optical transparency. For the purpose of fabricating high performance IGZO TFTs, a thermal recovery process above a temperature of $300^{\circ}C$ is required for recovery or rearrangement of the ionic bonding structure. However diffused metal atoms from source/drain(S/D) electrodes increase the channel conductivity through the oxidation of diffused atoms and reduction of $In_2O_3$ during the thermal recovery process. Threshold voltage ($V_{TH}$) shift, one of the electrical instability, restricts actual applications of IGZO TFTs. Therefore, additional investigation of the electrical stability of IGZO TFTs is required. In this paper, we demonstrate the effect of Ti diffusion and modulation of interface traps by carrying out an annealing process on IGZO. In order to investigate the effect of diffused Ti atoms from the S/D electrode, we use secondary ion mass spectroscopy (SIMS), X-ray photoelectron spectroscopy, HSC chemistry simulation, and electrical measurements. By thermal annealing process, we demonstrate VTH shift as a function of the channel length and the gate stress. Furthermore, we enhance the electrical stability of the IGZO TFTs through a second thermal annealing process performed at temperature $50^{\circ}C$ lower than the first annealing step to diffuse Ti atoms in the lateral direction with minimal effects on the channel conductivity.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2005년도 추계종합학술대회
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• pp.603-606
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• 2005

In this paper, the formation and thermal stability of Ni-silicide using Ni-Pd alloys is studied for ultra shallow S/D junction of nano-scale CMOSFETs. There are no different effects when Ni-Pd is used in single structure and TiN capping structure. But, in case of Cobalt interlayer structure, it was found that Pure Ni had lower sheet resistance than Ni-Pd, because of a thick silicide. Also, Ni-Pd has merits that surface of silicide and interface between silicide and silicon have a good morphology characteristics. As a result, Ni-Pd is an optimal candidate for shallow S/D junction when cobalt is used for thermal stability.

• Composites Research
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• 제17권6호
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• pp.37-43
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• 2004

경화제의 사슬길이와 화학구조 차이가 반응특성, 열적, 기계적특성에 미치는 영향을 조사하기 위하여 선형구조를 가지고 양쪽 막단기에 에폭시기를 갖는 범용 에폭시수지인 DCEBF를 양쪽 관능기가 동일하고 주쇄의 사슬길이가 서로 다른 선형아민 경화제인 EDA와 HMDA로 각자 1:1 당량비로 혼합하여 예비 및 후 경화조건으로 경화하였다. 그 결과, 수지 경화물의 특성은 경화제 주쇄의 탄소원자수에 따라 큰 영향을 받는 것으로 밝혀졌다. 즉, 주쇄의 길이가 짧은 EDA 경화계는 길이가 긴 HMDA 경화계보다 열안정성, 밀도, 부피수축(%), 유리전이온도, 인장탄성률 및 인장강도, 굴곡탄성률 및 굴곡강도의 값이 높게 나타났고, 반면에 최대발열온도, 에폭시기의 전환률, 선팽창계수의 값은 낮게 나타났다. 이는 주쇄의 탄소원자수 2개를 가지는 EDA가 3차원 망목상 공간구조 형성과정에서 packing capability가 우수하여 rigid한 특성을 가지기 때문이다. 굴곡 파단 특성은 굴곡탄성률과 굴곡강도와 밀접한 관계를 나타내었다.