• Title/Summary/Keyword: Taylor cone

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Dual Nano-Electrospray and Mixing in the Taylor Cone

  • Radionova, Anna;Greenwood, David R.;Willmott, Geoff R.;Derrick, Peter J.
    • Mass Spectrometry Letters
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    • v.7 no.1
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    • pp.21-25
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    • 2016
  • Dual-channel nano-electrospray has recently become an ionization technique of great promise especially in biological mass spectrometry. This unique approach takes advantage of the mixing processes that occurs during electrospray. Understanding in more detail the fundamental principles influencing spray formation further study of the origins of the mixing processes: (1) in a Taylor cone region, (2) in charged droplets or (3) in both environments. The dual-channel emitters were made from borosilicate theta-shape glass tubes (O.D. 1.2 mm) and had a tip diameters of less than 4 μm. Electrical contact was achived by deposition of a thin film of an appropriate metal onto the surface of the emitter. The experimental investigation of the Taylor cone formation in a dual-channel electrospray emitter has been carried out by injection of polystyrene beads (diameter 3 μm) at very low concentrations into one of the channels of the non-tapered theta-glass tubes. High-speed camera experiments were set up to visualize the mixing processes in Taylor cone regions for dual-channel emitters. Mass spectra from dual nano-electrospray are presented.

Reduction of Height of Taylor Cone Caused by Water Surface Discharge and Its Ozone Generation Characteristics (수표면방전의 방전 수돌기의 높이제한과 오존발생특성)

  • Park, Seung-Lok;Kim, Jin-Gyu;Kim, Ju-Yong;Lee, Dae-Hee;Moon, Jae-Duk
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.50 no.7
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    • pp.334-339
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    • 2001
  • A silent type ozone generator using water surface has been studied and improved its ozone generation characteristics by the controlling the height of Taylor cone by installing a mesh electrode, a dielectric bed of glass beads in the just under th surface of the water. The current-voltage characteristics and characteristics of ozone generation quantity of the test system were investigated and discharge current oscillograms of the each cases of the mesh electrode and the beds were observed and compared each other to analyze the discharge conditions. The Taylor cone height could be the cause of the discharge bridge to decrease the ozone generation on the discharge spacing. In this study, the hight of Taylor cone could be reduced greatly by installing the mesh and the glass beads bed just under the water surface. Therefore a higher ozone generation also could be obtained.

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Experimental study on CIS thin film deposition via electrostatic spray technique (정전기 스프레이 기술을 이용한 CIS 박막코팅에 관한 실험적 연구)

  • Yoon, Hyun;Yoon, Sukgoo;Kim, Hoyoung
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.11a
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    • pp.37.2-37.2
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    • 2010
  • Electrostatic spray deposition is an innovative coating technique that produces fine, uniform, self-dispersive (due to the Coulombic repulsion), and highly wettable, atomized drops. Copper-indium salts are dissolved in an alcohol-based solvent, which is then electrostatically sprayed onto a moderately heated, molybdenum-coated substrate. Solvent flowrates range from 0.02 to 5 ml/hr under applied voltages of 1 to 20 kV yielding drop sizes around a few hundred nanometers. By comparing the scanning electron miscrscope images of coated samples, the substrate temperature, applied voltage, solvent flowrate, and nozzle-substrate distance are demonstrated to be the primary parameters controlling coating quality. Also, the most stable electrostatic spray mode that reliably produces uniform and fine drops is the cone-jet mode with a Taylor cone issuing from the nozzle.

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Visualization of surface structures coated by electrospun polymers (고분자 용액이 전기방사된 표면의 구조 가시화)

  • Lee, Saebom;Lee, Minki;Yang, Sanghyeok;Kim, Seunghyun;Kim, HyeongJin;Sung, Seokwon;Lee, Minseong;Lee, Jinkee
    • Journal of the Korean Society of Visualization
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    • v.16 no.3
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    • pp.40-46
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    • 2018
  • The surface structure of the electrospun polymer fibers depends on the polymer concentration, the type of solvent used, applied voltage and so on. To make a desired surface, it is important to understand the effects of the physicochemical properties to form a stable Taylor cone and jet dispensation. We observed the formation of Taylor cone and a consequent structure of fiber by controlling the parameters of applied voltage, solution concentration, solvent and collector effectively. Once the surfaces were fabricated, the structures were analyzed using optical imaging technologies. As the solution concentration was increased, the smooth fibers were formed. In addition, different solvent ratios determined the viscosity and the surface tension of solutions. As a result, with decreased viscosity and increased surface tension, thin fibers were obtained by electrospinning. Furthermore the aligned nanofiber was successfully created by using drum collector.

Discharge and Ozone Generation Characteristics by Permittivity of Dielectric Material installed in Water Surface Discharge (수표면 방전에 투입된 유전체의 유전율에 따른 방전 및 오존발생특성)

  • 박승록;김진규;김형표
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.17 no.3
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    • pp.56-63
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    • 2003
  • A silent type ozone generator using water surface has been studied and improved its ozone generation characteristics by installing dielectric heads in the just under the surface of the wale- At this time, different permittivitis of dielectric beads were used to change the discharge condition of water surface. The current-voltage characteristics and characteristics of ozone generation quantity of the test system were investigated and discharge photos of glass beads were observed The height of Taylor cone may be the cause of the discharge bridge to decrease the ozone generation on the discharge spacing. In this study, the hight of Taylor cone could be controlled greatly by installing dielectric beads just under the water surface. Therefore a higher ozone generation also could be obtained. As the permittivity of dielectric material increased. discharge starting voltage was advanced and maximum 110 ppmy of ozone was generated by using the ferroelectric ball.

The effect of vibration of the water surface for hydrogen gas generation by plasma electrical discharge (비열플라즈마에 의한 수소가스발생에 미치는 수표면 진통효과)

  • Kim, Jong-Seog;Park, Jae-Yoon;Jung, Jang-Gun;Kim, Tae-Yong;Lee, Jae-Dong;Koh, Hee-Seog;Lee, Hyun-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.05b
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    • pp.115-119
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    • 2004
  • This paper is investigated about the effect of vibration of the water surface for hydrogen gas generation by non-thermal plasma. The vibration of the water surface is more powerful with increasing applied voltage. In this experimental reactor which is made of multi-needle and plate, the maximum acquired hydrogen production rate is about 6.8[ml/sec]. Although the generation of hydrogen gas is increased with elevating time, it is saturated after specific time due to the volume of reactor and the saturation of taylor cone.

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Elastically-influenced instabilities in Taylor-Couette and other flows with curved streamlines: a review

  • Muller, Susan J.
    • Korea-Australia Rheology Journal
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    • v.20 no.3
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    • pp.117-125
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    • 2008
  • Viscoelastic instabilities are of fundamental importance to understanding the physics of complex fluids and of practical importance to materials processing and fluid characterization. Significant progress has been made over the past 15 years in understanding instabilities in viscoelastic flows with curved streamlines and is reviewed here. Taylor-Couette flow, torsional flow between a cone and plate, and torsional flow between parallel plates have received special attention due to both the basic significance of these flows and their critical role in rheometry. First, we review the criteria for determining when these flows become unstable due to elasticity in the absence of inertia, and discuss the generalization of these criteria to more complex flows with curved streamlines. Then, focusing on experiments and simulations in the Taylor-Couette problem, we review how thermal sensitivity (i.e., the dependence of fluid viscosity and elasticity on temperature) and inertia affect the stability of viscoelastic flows. Finally, we conclude with some general thoughts on unresolved issues and remaining challenges related to viscoelastic instabilities.

Mode Change from Cone-jet to Dripping in Electrospraying (전기분무 콘제트-드리핑 모드 변환)

  • Park, Kun-Joong;Kim, Ho-Young;Song, Seung-Jin
    • Proceedings of the KSME Conference
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    • 2007.05b
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    • pp.2971-2976
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    • 2007
  • The mode change from Taylor cone-jet to dripping in electrospraying has been analytically investigated. The change has been predicted by the dynamic behavior of a liquid drop at the tip of the cone-jet. Conservation laws are applied to determine the upward motion of the drop, and an instability model of electrified jets is used to determine the jet breakup. Finally, for the first time, the analysis enables prediction of the transition in terms of the Weber number and electric Bond number. The predictions are in good agreement with experimental data.

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High Speed and Continuous Electrospinning Printing Using Polymer Ink (고분자 폴리머 잉크를 이용한 고속 연속 전기 방사 프린팅)

  • Zhang, Da-Hai;Kwon, Kye-Si
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.39 no.4
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    • pp.379-384
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    • 2015
  • Electrospinning has recently been used for micropatterning. The electrospinning method as a patterning tool has the advantage of a rapid patterning speed because it is based on a continuous printing mode rather than a drop-on-demand mode. To obtain stable continuous printing, a high molecular weight polymer must be mixed with functional materials for patterning. In this paper, polyethylene oxide (PEO) was used. The effect of polymer on viscosity and formation of a Taylor cone jet from the electrospinning nozzle was investigated. Finally, the electrospinning patterning results of a silver paste ink on a glass substrate were investigated.

An Experimental Study on Characteristics of Droplet Generation by Electrospraying for Highly Viscous Liquids (정전분무에 의한 고점성 액체의 액적 생성 특성에 관한 실험적 연구)

  • Kim, Sang-Su;Gu, Bon-Gi
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.26 no.4
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    • pp.604-613
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    • 2002
  • Generation characteristics of electrospray droplets for highly viscous liquid have been investigated by measuring size distributions of droplets emitted from the Taylor cone using glycerol solutions with various conductivities. Because of very small volatility of glycerol, droplet sizes can be measured by an aerodynamic size spectrometer (TSI Aerosizer DSP) with negligible evaporation of droplets. For highly conducting and viscous liquid, the sizes of the droplets electrosprayed from the Taylor cone are found to be relatively insensitive to applied voltages and the electrosprays assisted by the corona discharge call produce monodisperse droplets as long as the corona intensity is not too high. Near the minimum flow rate where a liquid cone is stable, the spray tends to consist of a one -peak monodisperse distribution of drop lets. However, at high flow rates, the spray bifurcates into bimodal distributions, which are consistent with the result of the previous study for less viscous liquids than our liquids. For liquid flow rates (Q) below 1 nl/s, the measured droplet diameters by the aerosizer are in the range of 0.30 to 1.2 ${\mu}{\textrm}{m}$ for the glycerol solutions. The diameters of monodisperse droplets scale approximately with $r^*=Q_$\tau$(Q$\tau$){^1/3}$ where $r^*$ is a characteristic length and $\tau$is the electrical relaxation time of the fluid. However, when compared with several represe ntative scaling laws, the droplet diameters are two to six factors greater than those predicted by the scaling laws. This may be closely related to the combined effect of the much higher viscosity and the electrical charge on the jet breakup of glycerol so solution.