• Title/Summary/Keyword: Sub-division method

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Fabrication of 4.25 Co0.53Fe0.47-Al2O3 Composite by High Frequency Induction Heated Combustion Synthesis (고주파유도가열 연소합성에 의한 4.25 Co0.53Fe0.47-Al2O3 복합재료 제조)

  • Park, Na-Ra;NamKung, Hoon;Ko, In-Yong;Shon, In-Jin
    • Journal of Powder Materials
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    • v.16 no.2
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    • pp.91-97
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    • 2009
  • Nanopowders of $Co_3O_4$ and FeAl were fabricated by high energy ball milling. Dense 4.25 $Co_{0.53}Fe_{0.47}-Al_2O_3$ composite was simultaneously synthesized and consolidated by high frequency induction heated combustion method within 2 min from mechanically activated powders. Consolidation was accomplished under the combined effects of a induced current and mechanical pressure of 80 MPa.

Properties and Fabrication of 5Cu0.6Fe0.4-Al2O3 Composite by High Frequency Induction Heated Sintering (고주파유도가열 소결에 의한 5Cu0.6Fe0.4-Al2O3 복합재료제조 및 기계적 성질)

  • Lee, Dong-Mok;Song, Jun-Young;Park, Na-Ra;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.47 no.11
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    • pp.754-758
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    • 2009
  • Dense $5Cu_{0.6}Fe_{0.4}-Al_{2}O_{3}$ composite was consolidated from mechanically synthesized powders by high frequency induction heating method within 2 min. Consolidation was accomplished under the combined effects of a induced current and mechanical pressure. Dense $5Cu_{0.6}Fe_{0.4}-Al_{2}O_{3}$ with relative density of up to 95% was produced under simultaneous application of a 80 MPa pressure and the pulsed current. Fracture toughness and hardness of the composite are $7.6MPa{\cdot}m^{1/2}$ and $844kg/mm^{2}$ respectively.

Development of thermal conductivity model with use of a thermal resistance circuit for metallic UO2 microcell nuclear fuel pellets

  • Heung Soo Lee;Dong Seok Kim;Dong-Joo Kim;Jae Ho Yang;Ji-Hae Yoon;Ji Hwan Lee
    • Nuclear Engineering and Technology
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    • v.55 no.10
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    • pp.3860-3865
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    • 2023
  • A metallic microcell UO2 pellet has a microstructure where a metal wall is connected to overcome the low thermal conductivity of the UO2 fuel pellet. It has been verified that metallic microcell fuel pellets provide an impressive reduction of the fuel centerline temperature through a Halden irradiation test. However, it is difficult to predict the effective thermal conductivity of these pellets and researchers have had to rely on measurement and use of the finite element method. In this study, we designed a unit microcell model using a thermal resistance circuit to calculate the effective thermal conductivity on the basis of the microstructure characteristics by using the aspect ratio and compared the results with those of reported metallic UO2 microcell pellets. In particular, using the thermal conductivity calculated by our model, the fuel centerline temperature of Cr microcell pellets on the 5th day of the Halden irradiation test was predicted within 6% error from the measured value.

Reference evapotranspiration estimates based on meteorological variables over Korean agro-climatic zones for rice field (남한지역의 논 농업기후지대에 대한 기상자료 기반의 기준 증발산량 추정)

  • Jung, Myung-Pyo;Hur, Jina;Shim, Kyo-Moon;Kim, Yongseok;Kang, Kee-Kyung;Choi, Soon-Kun;Lee, Byeong-Tae
    • Korean Journal of Agricultural and Forest Meteorology
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    • v.21 no.4
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    • pp.229-237
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    • 2019
  • This study was conducted to estimate annual reference evapotranspiration (ET0) for the agro-climatic zones for rice paddy fields in South Korea between 1980 and 2015. The daily ET0 was estimated by applying the Penman-Monteith method to meteorological data from 61 weather stations provided by Korean Meteorological Administration (KMA). The average of annual ET0 from 1980 to 2015 was 1334.1±33.89 mm. The ET0 was the highest at the Southern Coastal Zone due to their higher air temperature and lower relative humidity. The ET0 had significantly increased with 2.81 mm/yr for the whole zones over 36 years. However, the change rate of it was different among agro-climatic zones. The annual ET0 highly increased in central zones and eastern coastal zones. In terms of correlation coefficient, the temporal change of the annual ET0 was closely related to variations of four meteorological factors (i.e., mean, minimum temperatures, sunshine duration, and relative humidity). The results demonstrated that whole Korean agro-climatic zones have been undergoing a significant change in the annual ET0 for the last 36 years. Understanding the spatial pattern and the long-term variation of the annual ET0 associated with global warming would be useful to improve crop and water resource managements at each agro-climatic zone of South Korea.

Radiographic changes of mandibular cortical bone in bisphosphonate drug holiday

  • Lee, Dae-Hoon;Seo, Ja-In;Song, Seung-Il;Lee, Jeong-Keun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.48 no.4
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    • pp.219-224
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    • 2022
  • Objectives: There have been few studies to date on the residual effect of bisphosphonate. This study investigated the radiographic changes of mandibular cortical thickness upon bisphosphonate drug holiday. Materials and Methods: This retrospective study includes 36 patients diagnosed with MRONJ (medication-related osteonecrosis of the jaw) at Ajou University Dental Hospital in 2010-2021. All patients stopped taking bisphosphonate under consultation with the prescribing physicians. Panoramic radiographs were taken at the start of discontinuation (T0), 12 months after (T1), and 18 months after (T2) discontinuation of bisphosphonate, respectively. Mental index and panoramic mandibular index were calculated using Ledgerton's method. Paired t-tests were used to analyze differences over time. Results: The difference in indices (mental index and panoramic mandibular index) between T0 and T1 was not statistically significant (paired t-test, P>0.05). However, the difference in these indices between T1 and T2 was statistically significant (paired t-test, P<0.05). Conclusion: The cortical thickness of the mandible decreased in the late stage (after 18 months) as observed by panoramic radiograph.

Monitoring of Veterinary Antibiotics in Agricultural Soils using Liquid Chromatography Coupled with Tandem Mass Spectrometry (LC-MS/MS를 이용한 농경지 토양 중 항생제 모니터링)

  • Lee, Young-Jun;Choi, Jeong-Heui;Chung, Hyung Suk;Lee, Han Sol;Park, Byung-Jun;Kim, Jang-Eok;Shim, Jae-Han
    • Korean Journal of Environmental Agriculture
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    • v.35 no.3
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    • pp.166-174
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    • 2016
  • BACKGROUND: The current study developed a monitoring method of 6 veterinary antibiotics (amoxicillin, ampicillin, enrofloxacin, tetracycline, chlortetracycline, oxytetracycline) in agricultural soils using liquid chromatography-tandem mass spectrometry (LC-MS/MS) in positive electrospray ionization mode.METHODS AND RESULTS: Sample preparation was carried out using acidic acetonitrile and citrate salts followed by purification with dispersive solid phase extraction (d-SPE). Separation on Eclipse Plus C18 column was conducted in gradient of the mobile phase, 0.1% formic acid and 5 mM ammonium formate in methanol (A) and 0.1% formic acid and 5 mM ammonium formate in distilled water (B). The linearity of the matrix-matched calibrations expressed as the coefficient of determination was good with R2≥0.9900. The limit of quantifications (LOQs) ranged from 0.5 to 10 μg/kg for all analytes. Analysis of 51 agricultural soil samples taken in the Republic of Korea revealed concentrations less than 1.9 μg/kg for enrofloxacin, 75.5 μg/kg for chlortetracycline.CONCLUSION: The method was successfully applied to monitor 6 veterinary antibiotics from 51 field incurred agricultural soil samples in 17 provincial areas throughout the Republic of Korea. The developed method was simple, easy, and versatile and can be used for monitoring various veterinary antibiotics in soil.

The Synthesis of Na0.6Li0.6[Mn0.72Ni0.18Co0.10]O2 and its Electrochemical Performance as Cathode Materials for Li ion Batteries

  • Choi, Mansoo;Jo, In-Ho;Lee, Sang-Hun;Jung, Yang-Il;Moon, Jei-Kwon;Choi, Wang-Kyu
    • Journal of Electrochemical Science and Technology
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    • v.7 no.4
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    • pp.245-250
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    • 2016
  • The layered $Na_{0.6}Li_{0.6}[Mn_{0.72}Ni_{0.18}Co_{0.10}]O_2$ composite with well crystalized and high specific capacity is prepared by molten-salt method and using the substitution of Na for Li-ion battery. The effects of annealing temperature, time, Na contents, and electrochemical performance are investigated. In XRD analysis, the substitution of Na-ion resulted in the P2-$Na_{2/3}MO_2$ structure ($Na_{0.70}MO_{2.05}$), which co-exists in the $Na_{0.6}Li_{0.6}[Mn_{0.72}Ni_{0.18}Co_{0.10}]O_2$ composites. The discharge capacities of cathode materials exhibited $284mAhg^{-1}$ with higher initial coulombic efficiency.

Effect of Halal and Conventional Slaughtering Method with CO2 and N2 Gas Stunning on Physicochemical Traits of Chicken Breast Muscle and Small Intestine (도계 중 할랄방법에 CO2와 N2 가스기절처리가 닭 가슴살과 내장의 물리화학적 특성에 미치는 영향)

  • Song, Dong-Heon;Alam, Shahbubul Muhammad;Lee, Jeong-Ah;Hoa, Van Ba;Kang, Sun Moon;Kim, Hyoun Wook;Jeon, JinJoo;Kang, Hwan Ku;Cho, Soo-Hyun;Seol, Kuk-Hwan
    • Korean Journal of Poultry Science
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    • v.49 no.1
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    • pp.1-8
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    • 2022
  • We investigated the effects of stunning methods and gas treatments during slaughter on the quality characteristics of chicken breast and small intestine. Broilers (Ross 308) were stunned and slaughtered using halal, CO2, or N2 gas stunning methods (for 10 birds). After slaughter, the pH, proximate composition, color, water-holding capacity, cooking loss, and shear force of chicken breast muscle and small intestine were determined. Compared with the halal treatment, CO2 treatment resulted in higher pH and lower cooking loss (P<0.05), and the pH, color, and shear force of chicken breast muscle with N2 treatment were similar to those of the halal treatment (P>0.05). Compared with the halal treatment, the gas treatments resulted in lower pH and lightness and higher redness, yellowness, thickness, and shear force of the small intestine (P<0.05). However, compared with the CO2 treatment, the N2 treatment resulted in lower pH, redness, and yellowness, and higher lightness, thickness, and shear force. Overall, compared with the halal method, our results suggest that the use of N2 gas suppresses the discoloration and deterioration of the texture of chicken meat and small intestine caused by CO2 gas treatment in the gas stunning method.

Response Characteristics of Electrochemical Non-enzyme Immunosensor using Fe3O4 Nanoparticle (Fe3O4 나노분말을 이용한 전기화학적 비효소 면역센서 응답특성)

  • Kim, Chang-Kyu;Lee, Gyoung-Ja;Uhm, Young-Rang;Lee, Min-Ku;Rhee, Chang-Kyu
    • Journal of Powder Materials
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    • v.16 no.3
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    • pp.180-184
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    • 2009
  • In this paper, the electrochemical non-enzyme immunosensor has been developed for the determination of salmonella antigen, using inverse voltammetry. For the estimation of salmonella antigen concentration, the $Fe_3O_4$ nanoparticles synthesized by microemulsion method were conjugated with salmonella antigen. Then, the immunocomplex between antibody immobilized on the transducer surface and antigen containing a magnetic nanoparticles was formed. From the linear relationship between the reduction peak current of Fe(III) and salmonella antigen concentration, it is suggested that the electrochemical non-enzyme biosensor is applicable to detect salmonella antigen in the concentration range of $10^1-10^5$ CFU/ml.

Estimation of radionuclides leaching characteristics in different sized geopolymer waste forms with simulated spent ion-exchange resin

  • Younglim Shin;Byoungkwan Kim;Jaehyuk Kang;Hyun-min Ma;Wooyong Um
    • Nuclear Engineering and Technology
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    • v.55 no.10
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    • pp.3617-3627
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    • 2023
  • This study presents a method to solidify spent ion-exchange resin (IER) in a metakaolin-based geopolymer and shows results of mechanical strength, immersion, leaching, irradiation, and thermal cycling tests for waste acceptance criteria (WAC) to repository. The geopolymer waste form with 20 wt% of simulated spent IER met the WAC in South Korea (ROK), and the leaching tests of various sized-waste forms up to 15.0 × 30.0 cm and waste loadings up to 20 wt% for 1-5 d and 1-90 d achieved a leachability index, Li > 6. In a leaching test for 5 d, the cumulative fraction leached (CFL) for Cs, which leached the most, was linearly correlated with the square root of leaching time for all waste forms, and Li increased as the size of the waste form increased. The CFL was also correlated with elapsed time in the 90 d leaching test. The correlations among CFL, time, and volume-to-surface area ratio of waste forms used to estimate the Li of Cs of a 200-L sized geopolymer with 15 wt% IER showed the Li values as 14.73 (5 d) and 17.71 (90 d), respectively, indicating that the large-sized geopolymer waste form met the WAC.