• Journal of the Korean Ceramic Society
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• v.53 no.5
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• pp.529-534
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• 2016

Nanocrystalline powder of zirconia stabilized with 8 mol% yttria (YSZ) has been synthesized through oxalate process using $ZrOCl_2{\cdot}8H_2O$ and $Y(NO_3)_3{\cdot}6H_2O$ as starting materials. Understanding of the characteristic changes of YSZ powder as a function of processing conditions is crucial in developing dense and porous microstructures required for fuel cell applications. In this research, microstructure change, surface area, particle shape and particle size were measured as a function of different processing conditions such as calcination temperature, stirring speed and concentration of starting materials. The resultant crystallite sizes were calculated by XRD-LB (X-Ray Diffraction Line-Broadening) method, BET method, and morphology of the crystal was observed in TEM and FE-SEM. The TEM examination showed that the powder synthesized with 0.7 M of YSZ concentration had a spherical morphology with sizes ranging from 20 to 40 nm. However, the powder was gradually aggregated above 1.0 M of YSZ concentration with the aggregation being intensified as the YSZ concentration was increased.

• Transactions of the KSME C: Technology and Education
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• v.3 no.2
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• pp.97-106
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• 2015

Flexible structures are often important components of mechanical assemblies in motion. A flexible structure sometimes must go through assembly steps that cause it to be in a pre-stressed condition when in the starting position for operation. A virtual prototype of the assembly must also bring the model of the flexible structure into the same pre-stressed condition in order to obtain accurate simulation results. This case study is presented regarding the simulation of a constant velocity joint, with a focus on the flexible boot. The case study demonstrates that careful definition of the initial conditions of the boot and flexible body contacts yields high-fidelity simulation results.

• Proceedings of the KSME Conference
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• 2001.06d
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• pp.955-960
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• 2001

In order to develop an efficient turbine for wave energy conversion suitable for actual ocean conditions, a new type of the air turbine with staggered blades has been investigated experimentally. Experiments have been carried out under steady flow conditions. Both the running and starting characteristics under sinusoidally oscillating flow conditions are simulated by a CFD method using a quasi-steady analysis. It is known that the air turbine with staggered blades gives a better performance compared with conventional Wells turbine, and a proper design factor of the air turbine is discussed for the setting angle of the rotor.

• The Korean Journal of Ceramics
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• v.3 no.3
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• pp.191-194
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• 1997

Epitaxial Pb(Zr, Ti)O3(PZT) thin films were prepared on MgO(100) substrates by dipping-pyrolysis (DP) process using metal naphthenates as starting materials, and effects of pyrolysis and final heat-treatment conditions on the film's orientation were investigated. Solid-state epitaxial growth of PZT proceeds at lower temperature around 650℃ from the precursor pyrolyzed at 350 and 500℃. The in-plane alignment of the PZT films depends not only on the final heat-treatment temperature but on the pyrolysis conditions; the films, pyrolyzed at a higher temperature for a short time, i.e., at 500℃ for 10 min, exhibited stronger orientation after the same final heat treatment at 650°∼750℃. The PZT films with the strongest orientation were prepared by pyrolysis under the above conditions followed by final heat treatment at 750℃.

• BMB Reports
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• v.37 no.4
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• pp.503-506
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• 2004

Glucose-1-phosphate uridylyltransferase from E. coli K12 was used to convert uridine-5'-triphosphate and glucose-1-phosphate to UDP-D-glucose. The conversion was efficient and completed within 5 minutes under the employed conditions. In addition, thymidine-5'-monophosphate kinase and acetate kinase were proven to be non-specific, converting udridine-5'-monophosphate to uridine-5'-triphosphate with 55% conversion after 6 h, which was much slower than the production of TTP under the same conditions (complete conversion within one hour). Since these two reactions could proceed under the same conditions, a one-pot synthesis of UDP-D-glucose with ATP regeneration was designed from easily available starting materials, and conversion up to 40% by HPLC peak integration was achieved given a reaction time of 4 h.

• Journal of Powder Materials
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• v.26 no.3
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• pp.195-200
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• 2019

Whisker-type magnesium hydroxide sulfate hydrate ($5Mg(OH)_2{\cdot}MgSO_4{\cdot}3H_2O$, abbreviated 513 MHSH), is used in filler and flame-retardant composites based on its hydrate phase and its ability to undergo endothermic dehydration in fire conditions, respectively. In general, the length of whiskers is determined according to various synthetic conditions in a hydrothermal reaction with high temperature (${\sim}180^{\circ}C$). In this work, high-quality 513 MHSH whiskers are synthesized by controlling the concentration of the raw material in ambient conditions without high pressure. Particularly, the concentration of the starting material is closely related to the length, width, and purity of MHSH. In addition, a ceramic-coating system is adopted to enhance the mechanical properties and thermal stability of the MHSH whiskers. The physical properties of the silica-coated MHSH are characterized by an abrasion test, thermogravimetric analysis, and transmission electron microscopy.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.11a
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• pp.221-223
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• 1999

In this work, samples were manufactured variously by changing conventional calcining and sintering conditions and we tried the utilization by making the heat treatment time, which is demanded to high-Tc phase formation, much shorter. We found out optimal heat treatment conditions with the analysis on formation process at superconducting phase in term of the change of calcining and sintering time and then, examined X-ray diffraction(XRD) patterns, scanning electron microscope(SEM) measurement and energy dispersive X-ray spectrometer(EDX) of the samples manufactured under heat treatment conditions which we suggest here. As a result, 2223 high-$T_c$, phase of (Bi,Pb)SrCaCuO superconductor starting with ($Bi_l$ xPbx,)$_2$$Sr_2$$Ca_2$$Cu_3$$O_y$, composition was formed from 1 hr sintering sample at temperature nearby melting point and also the completed sample with calcining and sintering time of 9 hr was formed high-$T_c$.low-$T_c$ phase appearing in sight above the critical temperature of liquid $N_2$.

• Geomechanics and Engineering
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• v.30 no.3
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• pp.219-231
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• 2022

Geotechnical materials such as silt, fine sand, or coarse granular soils may be unstable under undrained shearing or during rainfall infiltration starting an unsaturated state. Some researches are available describing the instability of coarse granular soils in drained or undrained conditions. However, there is a need to investigate the instability mechanism of unsaturated silty soil considering the effect of degree of compaction and net confining stress under partially and fully drained conditions. The specimens in the current study are compacted at 65%, 75%, & 85% degree of compaction, confined at pressures of 60, 80 & 120 kPa, and tested in partially and fully drained conditions. The tests have been performed in two steps. In Step-I, the specimens were sheared in constant water content conditions (a type of partially drained test) to the maximum shear stress. In Step-II, shearing was carried in constant suction conditions (a type of fully undrained test) by keeping shear stress constant. At the start of Step-II, PWP was increased in steps to decrease matric suction (which was then kept constant) and start water infiltration. The test results showed that soil instability is affected much by variation in the degree of compaction and confining stresses. It is also observed that loose and medium dense soils are vulnerable to pre-failure instability i.e., instability occurs before reaching the failure state, whereas, instability in dense soils instigates together with the failure i.e., failure line (FL) and instability line (IL) are found to be unique.

• 제어로봇시스템학회:학술대회논문집
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• 1992.10b
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• pp.208-213
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• 1992

In this paper we are concerned with optimal control problems whose costs am quadratic and whose states are governed by linear delay equations and general boundary conditions. The basic new idea of this paper is to Introduce a new class of linear operators in such a way that the state equation subject to a starting function can be viewed as an inhomogeneous boundary value problem in the new linear operator equation. In this way we avoid the usual semigroup theory treatment to the problem and use only linear operator theory.

• Journal of the Korean Institute of Telematics and Electronics
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• v.13 no.4
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• pp.18-23
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• 1976

We have obtained the solution of van der Pol's equation characterized by an arctangent nonlinearity, using the perturbation method by writing periodicity conditions: $$X^{(n)}(2{\pi})-X^{(n)}(0)=0$$ $$X^{(n)'}(2{\pi})-X^{(n)'}(0)=0 (n=0,1,2......)$$ together with the starting condition: $$X^{(n)}(\frac{\pi}{2})=0,\;X^{(n)}'(\frac{\pi}{2})=-R^{(n)}$$. Our results agree with Liapunov's theorem and our calculated value is more similar to Murata's measured value than Murata's calculated value.