• Title/Summary/Keyword: Standard Method

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Accurate Measurement of Arsenic in Laver by Gravimetric Standard Addition Method Combined with High Resolution Inductively Coupled Plasma Mass Spectrometry

  • Lee, Kyoung-Seok;Kim, Hyeon-Ji;Yim, Yong-Hyeon;Kim, Jeongkwon;Hwang, Euijin
    • Mass Spectrometry Letters
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    • 제5권2호
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    • pp.57-61
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    • 2014
  • A gravimetric standard addition method combined with internal standard calibration has been successfully developed for the accurate analysis of total arsenic in a laver candidate reference material. A model equation for the gravimetric standard addition approach using an internal standard was derived to determine arsenic content in samples. Handlings of samples, As standard and internal standard were carried out gravimetrically to avoid larger uncertainty and variability involved in the volumetric preparation. Germanium was selected as the internal standard because of its close mass to the arsenic to minimize mass-dependent bias in mass spectrometer. The ion signal ratios of $^{75}As^+$ to $^{72}Ge^+$ (or $^{73}Ge^+$) were measured in high resolution mode ($R{\geq}10,000$) to separate potential isobaric interferences by high resolution ICP/MS. For method validation, the developed method was applied to the analysis of arsenic content in the NMIJ 7402-a codfish certified reference material (CRM) and the result was $37.07mg{\cdot}kg^{-1}{\pm}0.45mg{\cdot}kg^{-1}$ which is in good agreement with the certified value, $36.7mg{\cdot}kg^{-1}{\pm}1.8mg{\cdot}kg^{-1}$. Finally, the certified value of the total arsenic in the candidate laver CRM was determined to be $47.15mg{\cdot}kg^{-1}{\pm}1.32mg{\cdot}kg^{-1}$ (k = 2.8 for 95% confidence level) which is an excellent result for arsenic measurement with only 2.8 % of relative expanded uncertainty.

한국적 CALS 표준화 구축방안 (Construction of Korean Korea CALS Standardization)

  • 김철환;김규수;신영인
    • 한국전자거래학회지
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    • 제1권1호
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    • pp.117-140
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    • 1996
  • CALS is recognized as a national response to the new chapter of information society. It is essential that the standardization in Korea should be constructed compatible with not only domestic but also international standardization trend. This study aims to propose a proper direction of CALS standardization in Korea, based on the international CALS standardization movement. This paper classifies standard into five types and provides a proper direction and guidance far each standard. As a trend of CALS standard, all ten data files are converted using SGML standard far the interchangeability of data among heterogenous systems. CAD and Graphic data arc also moving toward to the STEP as their standard. In this regard, this paper discusses how to implement SGML and STEP Model. Finally, this paper proposes a method how to construct an EDI system with CALS standard and how to establish a standard authorization institute which will be responsible far the standard authorization. Furthermore, this paper also proposes the CALS Test Network (CTN) as its experimental method.

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국내 토양오염 공정시험방법의 용출법 사용시 용출액의 pH의 변화가 토양 오염 평가에 미치는 문제점 (The controversial points for the assessment of soil contamination related to the change of pH of extraction solution in using partial extraction in standard method in Korea)

  • 오창환;유연희;이평구;이영엽
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2000년도 추계학술대회
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    • pp.294-297
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    • 2000
  • Heavy metals are extracted from Chonju stream sediment, roadside soils and sediments along Honam expressway, soils and tailings from mining area using partial ectraction in Standard Method, partial ectraction method with maintaining 0.1N of extraction solution and acid digestion. In samples having buffer capacity against acid, 0.1N of extraction solution can not be maintained and pH of extraction solution increases up to 8.0 when partial extraction in Standard Method is used. The averages and ranges of (heavy metals extracted using partial extraction in standard method, HPE)/(heavy metals extracted using partial extraction method with maintaining 0.1N of extraction solution, HPEM) values are 0.506 and 0.145~1.126 in Cd, 0.534~ and 0.078~0.928 in Zn, 0.461 and 0.041~1.715 in Mn, 0.359 and 0.011~0.874 in Cu, 0.195 and 0.018~1.785 in Cr, 0.710 and 0.003~3.075 in Pb, and 0.088 and 1.73$\times$10$^{-5}$ ~0.303 in Fe. These data indicate that the difference between HPE and HPEM is big in the order of Fe, Cr, Cu, Mn, Cd, Zn and Pb. It is quite possible that the partial extraction method in Standard Method of soil in Korea is not adequate for an assessment of contamination in area where buffer capacity of soil will be decreased or lost after a long term exposure of soils to environmental damage.

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수질공정시험법과 Standard Method의 총질소 분석방법비교 (Comparison of the Total Nitrogen Determination Methods by UV spectrophotometric method and Standard method)

  • 박상찬;박종호;강병욱;이성희;장인수;조중식
    • 한국산학기술학회:학술대회논문집
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    • 한국산학기술학회 2010년도 추계학술발표논문집 1부
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    • pp.291-293
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    • 2010
  • 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 수중의 총질소를 간편하면서도 신속하고 정확하게 분석할 수 있는 방법으로 각각의 질소성분을 standard method에 의해 분석한 후 이들을 합산하는 방법보다 회수율이 좋게 나타났다. 자외선 흡광광도법을 이용할 경우 Cr(VI)이온과 Br이온에 의해 방해를 받으므로, Br이온을 다량 함유하는 해수의 총질소 분석방법으로는 적합하지 않은 것으로 관찰되었다. 전처리를 한 후 220 nm에서 흡광도를 측정하기 위해서는 탄산염의 방해를 방지하기 위해 pH를 2~3으로 조절한 후 분석해야만 하고, 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 총질소를 분석하는 방법으로 우수성이 입증되었으나 각 형태별 질소의 농도를 측정할 수 없는 단점이 있으므로 각 형태별 질소의 농도를 측정하기 위해서는 standard method를 이용해야 된다. 본 연구에서 알카리성 과황산칼륨을 이용한 자외선 흡광광도법은 총질소를 분석하는데 있어서 standard method에 의한 합산법보다 시간과 노력을 절약할 수 있는 것으로 검토되었다.

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DEVELOPMENT OF A NON-STANDARD FINITE DIFFERENCE METHOD FOR SOLVING A FRACTIONAL DECAY MODEL

  • SAID AL KATHIRI;EIHAB BASHIER;NUR NADIAH ABD HAMID;NORSHAFIRA RAMLI
    • Journal of applied mathematics & informatics
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    • 제42권3호
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    • pp.695-708
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    • 2024
  • In this paper we present a non-standard finite difference method for solving a fractional decay model. The proposed NSFDM is constructed by incorporating a non-standard denominator function, resulting in an explicit numerical scheme as easy as the conventional Euler method, but it provides very accurate solutions and has unconditional stability. Two examples from the literature are presented to demonstrate the performance of the proposed numerical scheme, which is compared to three methods from the literature. It is found that the method's estimated errors are extremely minimal, such as within the machine precision.

Design standard for fairway in next generation

  • Ohtsu, Kohei;Yoshimura, Yasuo;Hirano, Masayoshi;Takahashi, Hironao;Tsugane, Masanori;Ohtsu, Kohei
    • 한국항해항만학회:학술대회논문집
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    • 한국항해항만학회 2006년도 Asia Navigation Conference
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    • pp.230-239
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    • 2006
  • The depth, width and alignment of fairway that are main port water facilities should be designed considering the various elements including particulars of design ships, weather and sea conditions around fairway and method of ship-handling. However not only the existing Japanese design standard for fairway and also those of other countries do not take into consideration of such kind of elements and no design standard is made by quantitative analysis. In this circumstance the new design standard (Approach Channels, A Guide for Design) depending on classified various elements and quantitative analysis was proposed in 1997 by PIANC and IAPH. But it was proved that calculated values according to this standard were unfounded and had some problems to output the discontinuous value by small difference of calculation condition because the each value fur each element was simply added. And also it is hard to apply this standard to the design of port water facilities in Japan because this [A Guide for Design] is the design standard for long channels in European port. The proposal of more reasonable Japanese standard will be expected by applying the study result of naval architecture and navigation and by the cooperation of ship operators to use fairway, naval architects to built ships and civil engineers to dredge fairway. The concept of a fairway in 'Design standard fur fairway in next generation' is defined as passage for approach channel) and traffic lane designated by light buoys as navigable water for safe navigation. In 'Design standard for fairway in next generation' depth, width and alignment are picked up among many design elements of a fairway. Design method for those elements is shown based on design ships and navigational environments. This standard shows the method of design for each dimension depending on characteristic on design ship and weather and sea condition. On the other hand, in case of existing fairway, it is possible to decide the size of ship and navigation criteria by opposite analysis.

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GIS감리절차 확립을 위한 감리방법론(GASP)엔 관한 연구 (A Study for GASP(GIS Audit Standard Procedure) methodology to set up the GIS Audit process)

  • 신동빈;맹홍주;전성자
    • Spatial Information Research
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    • 제10권1호
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    • pp.29-43
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    • 2002
  • 이 연구는 GIS감리의 특성을 파악하고 기존의 GIS사업에 적용된 감리사례를 분석 하여 실제 적용할 수 있는 GIS감리기준, 지침 및 수행절차와 활동의 정의를 토대로 GIS사업을 효율적으로 추진할 누 있는 표준절차 정의를 통한 GIS감리방법론을 확립 하는데 목적을 두고 있다. 이에 본 인구는 감리수행을 위하며 GIS사업의 표준절차를 정의하고, 이러한 방법론을 준수했는지의 여부를 점검하는 과정을 골격으로 하고 있다. 이를 표준절차 정의에 의한 감리방법이라 하며, GASP(GIS Audit Standard Procedure)방법론이라 한다. GASP방법론이란 GIS감리를 효과적으로 수행하기 위하여 감리대상 사업의 전 공정과 예측되는 대상업무를 도출하기 위한 시범작업(Pilot project)을 수행한 후, 업무에 내한 표준절차를 사전에 정의(Prototype)하여 준수 여부를 감리하는 것을 말한다. 이는 GIS사업의 특성. 범위, 내용을 분석하여 모든 과정의 활동은 평가할 수 있는 보나 발전된 감리방법론이다.

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직접 비교법을 이용한 W-Band 밀리미터파 전력 표준 전달 시스템 (A W-Band Millimeter-Wave Power Standard Transfer System Using the Direct Comparison Method)

  • 권재용;강태원;강진섭;이동준
    • 한국전자파학회논문지
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    • 제24권1호
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    • pp.47-54
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    • 2013
  • 본 연구는 국내 최초로 개발된 직접 비교법을 이용한 W-band 밀리미터파 전력 표준 전달 시스템에 대한 것이다. 이 시스템은 75~110 GHz 대역에서 W-band 도파관형 전력감지기의 실효 효율과 교정 인자를 측정하기 위하여 개발되었다. 전력 표준 전달 시스템 구성의 핵심 요소인 방향성 결합기의 반사 특성 평가 기법을 소개하고 실험 결과를 보인다. 구현된 시스템을 이용하여 측정하고자 하는 전력감지기의 교정 인자 측정 결과를 보이고, 불확도 요인에 대하여 고찰한다. 측정 결과를 기준값과 비교하여 W-band 밀리미터파 전력 표준 전달 시스템에 의한 측정의 유효성을 검증한다.

정보통신시설공사 수량산출기준에 관한 연구 (A Study on the Standard Method of Measurement Information Communication Field Contractors)

  • 설동화;이광희
    • 정보통신설비학회논문지
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    • 제2권4호
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    • pp.52-63
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    • 2003
  • This study proposes a change from the currentexpected price integrated system, which is based on the standard of estimated unit manpower and material, to a new actual construction cost integrated system. In order to implement it, the standard method of measurement organization system as well as the communication area standard of estimated unit manpower and material should be changed Moreover, the work breakdown structure and itemized structure should be assorted.

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