• 약학회지
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• 제33권4호
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• pp.241-245
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• 1989

A new application of high performance liquid chromatography for the determination of capsaicin and dihydrocapsaicin in cataplasma preparation was investigated. Optimum conditions for a good separation and detection were determined; 0.93 volt, acetonitrile: $H_3PO_4$ sol (pH 2.8), sample size; $7\;{\mu}l$. Recovery rates of capsaicin and dihydrocapsaicin from mixed artificial preparations were 99.9% and 98.4% respectively. Also reproducibility tests showed that the coefficient of variation was 1.59% for capsaicin and 1.14% for dihydrocapsaicin. There was no interference with cataplasma preparation containing thymol, dl-camphor and the commonly encountered excipients or additives such as gelatine, glycerine. This method was rapid, accurate and it gave higher sensitivity than other method.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 춘계학술대회
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• pp.1442-1446
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• 2004

The heat (mass) transfer characteristics on the blade surface of a first-stage turbine rotor cascade has been investigated by employing the naphthalene sublimation technique. A four-axis profile measurement system is employed for the measurements of the local heat (mass) transfer coefficient on the curved blade surface. The experiments are carried out for two free-stream turbulence intensities of 1.2% and 14.7%. The high free-stream turbulence results in more uniform distributions of heat load on the both pressure and suction surfaces and in an early boundary-layer separation on the suction surface. The heat (mass) transfer enhancement on the suction surface due to the endwall vortices is found to be relatively small under the high free-stream turbulence.

• International Journal of Naval Architecture and Ocean Engineering
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• 제7권4호
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• pp.655-669
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• 2015

The Overall Motion Sickness Incidence is applied to the hull form optimization of a wave piercing high-speed catamaran vessel. Parametric hull modelling is applied to generate two families of derived hull forms, the former varying the prismatic coefficient and the position of longitudinal centre of buoyancy, the latter instead the demi-hull separation. Several heading angles are analysed in a seaway, considering all combinations of significant wave height and zero-crossing period under two operating scenarios. The optimum hull is generated and vertical accelerations at some critical points on main deck are compared with the parent ones. Finally a comparative analysis with the results obtained for a similarly sized monohull passenger ship is carried out, in order to quantify, by the OMSI, the relative goodness in terms of wellness onboard of monohulls and catamarans, as a function of sea states and operating scenarios.

• Macromolecular Research
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• 제11권1호
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• pp.53-61
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• 2003

A molecular-thermodynamic model is developed for the salt-induced protein precipitation. The protein molecules interact through four intermolecular potentials. An equation of state is derived based on the statistical mechanical perturbation theory with the modified Chiew's equation for the fluid phase, Young's equation for the solid phase as the reference system and a perturbation based on the protein-protein effective two body potential. The equation of state provides an expression for the chemical potential of the protein. In a single protein system, the phase separation is represented by fluid-fluid equilibria. The precipitation behaviors are simulated with the partition coefficient at various salt concentrations and degree of pre-aggregation effect for the protein particles. In a binary protein system, we regard the system as a fluid-solid phase equilibrium. At equilibrium, we compute the reduced osmotic pressure-composition diagram in the diverse protein size difference and salt concentrations.

• Korean Journal of Hydrosciences
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• 제7권
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• pp.77-86
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• 1996

An air chamber is design to keep the pressure from exceeding a predetermined value, or to prevent low pressures and colum separation. Therefore, it can be used to protect against rapid transients in a pipe system following abrupt pump stoppage. In this research, an air chmber was applied to a hypthetical pipe system to analyze attenuation effect of pressure head for different air volumes, locations, chamber areas, coefficients of orifice loss and pollytropic exponents. With an increase of air volume, the maximum pressure head at pump site is decreased and the minimum pressure head is imcreased. For different locations and areas of the chamber, the attenuation effects do not show much difference. Also, as the orifice loss coefficient increases, the maximum pressure head is decreased. For different polytropic exponents, isothermal process shows lower maximum pressure head than that of the adiabatic process.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2004년도 추계학술대회논문집
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• pp.596-599
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• 2004

The media transport systems, such as printers, copiers, facsimile, ATMs, cameras, etc., have been widely used and being developed rapidly. In the development of those systems, the media feeding mechanism is an important key technology for the design and development of the media transport systems. In this paper, a multi-degree of freedom sheet model with dynamic contact conditions is presented to understand the mechanism of sticking and jamming. A sheet is modelled as a cantilever beam and the feeding velocity is assumed to be constant. The relation between the feeding velocity and the coefficient of friction for guaranteeing stable feeding is presented. Simulations are performed for a horizontal linear guide and a oblique linear guide, calculating the contact force and contact states of mass points.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2004년도 추계학술대회논문집
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• pp.600-605
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• 2004

In many machines handling lightweight and flexible media such as magnetic tape drives, xerographic copiers and sewing machines, the media must transit an open space. It is important to predict the static and dynamic behavior of the sheets with a high degree of reliability. The nonlinear theory of the dynamic elastica has often been used to a nonlinear dynamic deflection model. In this paper, the governing equation is derived and simulated by the finite differential method. The parametric cubic curve is applied for defining the guide shape. The dynamic contact conditions suggested by Klarbring is used to predict the direction of the flexible media according to the initial velocity and the friction coefficient. The analysis is also compared to the conventional model, showing that after contacting a $45^{\circ}$ wall, the directions of flexible media of two models are different.

• Computers and Concrete
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• 제10권3호
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• pp.219-229
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• 2012

Carbonation is a widespread degradation of concrete and may be coupled with more severe degradations. An experimental investigation was carried out to study the effect of carbonation on chloride ion diffusion of concrete. The characteristic of concrete after carbonation was measured, such as carbonation depth, strength and pore structure. Results indicated that carbonation depth has a good linear relation with square root of carbonate time, and carbonation can improve compressive strength, but lower flexural strength. Results about pore structure of concrete before and after carbonation have shown that carbonation could cause a redistribution of the pore sizes and increase the proportion of small pores. It also can decrease porosities, most probable pore size and average pore diameters. Chloride ion diffusion of concrete after carbonation was studied through natural diffusion method and steady state migration testing method respectively. It is supposed that the chloride ion concentration of carbonation region is higher than that of the sound region because of the separation of fixed salts, and chloride ion diffusion coefficient was increased due to carbonation action evidently.

• 약학회지
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• 제24권2호
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• pp.117-122
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• 1980

A new application of high pressure liquid chromatography for the determination of fenitrothion and cis- and trans-neopynamin in insecticidal preparations was investigated. Optimum conditions for a good separation and determination were determined; solvent system: dichloromethane + n-hexane = 17 + 83; Bow rate: 0.5ml/min; column: u-porasil ($4mm{\times}3Ocm$); absorbance wavelength: 254nm; 0.05 AUFS and sample size: 30 ul. Recovery of fenicrothion, cis- and trans-neopynamin from mixed artificial preparations was 99.6%, 99.7% and 99.8% respectively. Also reproducibility tests showed that the coefficient of variation was 0.89% for fenitrothion, 0.74% cis-neopynamin and 1.1% for trans-neopynamin. There was no interference with insecticidal preparation containing DDVP, allethrin, S-421 and kerosene. HPLC method was rapid, accurate and it gave better reproducibility and higher sensitivity than any other analytical method. It was considered that HPLC could be greatly applied to the analysis of fenitrothion and neopynamin in insecticidal preparations.

• 한국해양공학회지
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• 제35권2호
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• pp.113-120
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• 2021

In order to perform a precise wave tank experiment, it is necessary to maintain the incident wave generated by the wavemaker in a steady state and to effectively remove the reflected waves. In this paper, a combined sloping-wall-type punching plate wave absorber was proposed to attenuate reflected waves effectively in a two-dimensional mini wave tank. Using the four-point reflection separation method, the reflected waves were measured to determine the reflection coefficients. Experiments were conducted under various punching plate porosities, sloping plate angles, and incident wave conditions to evaluate the performance of the combined punching plate wave absorber. The most effective wave absorbing performance was achieved when the porosity was 10% and the inclination angle of the punching plate was 18.6° under the present condition. It was also found that the installation of the sloping plate could improve the wave attenuation performance by generating the shoaling effect of the incident wave.