• 제목/요약/키워드: Separation Ability

검색결과 211건 처리시간 0.026초

고성능 액체 크로마토그래피에서 키랄 크라운 에테르로부터 유도된 키랄 고정상을 이용한 광학분리의 비교 (Comparative Enantiomer Separation on Chiral Stationary Phases Derived from Chiral Crown Ether by HPLC)

  • 황호;전소희;김지연;이원재
    • KSBB Journal
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    • 제27권4호
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    • pp.232-236
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    • 2012
  • Comparative liquid chromatographic enantiomer separation of ${\alpha}$-amino acids, their esters and primary amino compounds was performed using two chiral stationary phases (CSPs) prepared by covalently bonding (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid (18-C-6-TA) of the same chiral selector. In general, the separation factors and resolution factors for these analytes on CSP 1 were greater than on CSP 2, while these capacity factors on CSP 2 were quite greater than on CSP 1. Except for leucine methyl ester and phenylalanine methyl ester, the elution orders of all analytes including ${\alpha}$-amino ${\alpha}$-alkyl acids and phenylglycine alkyl esters on CSP 1 are identical to those on CSP 2. This study showed that different connecting structures for these two CSPs might influence their ability to resolve the analytes depending on their structures related to the chiral recognition mechanism.

와이어메쉬 절연계의 파이로 충격 절연 성능 시험 (Pyroshock Isolation Performance Test using Wiremesh Isolators)

  • 윤세현;장영순;한재홍
    • 한국항공우주학회지
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    • 제36권9호
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    • pp.923-928
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    • 2008
  • 파이로 충격은 고주파 영역까지 큰 가속도가 유발되는 천이 진동 현상으로 발사체에서는 주로 화약에 의한 분리 장치의 작동에 의해 발생하게 된다. 일반적인 발사체의 경우 단 분리, 페어링 분리, 위성 분리 이벤트에서 파이로 충격이 발생하게 되는데 이에 의해 위성 또는 발사체의 전자 장비가 비정상적인 기능을 보이거나 작동 불능 상태가 될 수 있다. 본 논문에서는 이러한 파이로 충격의 절연을 위해 와이어메쉬 절연계를 소개하였고 동일 단면을 기준으로 밀도와 높이를 다르게 9 종류를 제작하였다. 와이어메쉬 절연계의 전형적인 특성을 살펴보기 위해 기본적인 압축 시험을 수행하였고 더미 질량을 이용하여 파이로 충격 시험을 수행, 충격 절연 효과가 뛰어남을 검증하였다.

상 분리에 의한 콜레스테릭 액정의 피치 변화 (Pitch Variations in Cholesteric Liquid Crystals by Phase Separation)

  • 박한수;김범경;김환기;김인선;송기국
    • 폴리머
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    • 제30권2호
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    • pp.182-186
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    • 2006
  • CLC는 주기적인 나선구조 때문에 빛을 선택적으로 반사하는 특성을 보이는데, 반사 파장대역이 넓은 CLC를 광반응에 의한 상 분리 현상을 이용하여 제조하였다. CLC 액정 셀에 의하여 반사되는 빛의 파장은 노광하는 빛의 세기가 작을수록 그리고 UV 흡수 dye의 양이 증가할수록 범위가 증가하여 초기 50 nm의 반사 파장대역을 300 nm까지 넓힐 수 있었다. 광경화된 CLC 액정 셀 내에 상 분리에 의하여 형성된 다양한 CLC 피치 분포를 SEM으로 관찰하였고, ATR-IR 실험을 이용하여 CLC피치 분포가 넓어지는 것이 상 분리에 의한 것임을 확인하였다.

소형화된 듀얼 주파수 FM 송신기 개발 (Development of miniaturized dual-frequency FM transmitter)

  • 류정탁
    • 한국산업정보학회논문지
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    • 제16권5호
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    • pp.31-35
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    • 2011
  • 본 논문에서는 소형화된 듀얼 주파수 FM 송신기의 개발과 현장에서의 실험 결과를 보여주고 있다. 개발된 시스템의 크기는 2.6 cm ${\times}$ 2.6 cm ${\times}$ 2.6 cm 이다. 사용주파수는 88.1 MHz 과 88.3 MHz를 사용하였다. 시스템의 동작 전원은 3.7 V로 전원 공급은 한번 충전에 7시간 사용할 수 있는 내장 밧데리를 사용하였다. 전송 주파수의 채널 분리도는 40dB이다. 현장에서의 실험 결과 3m 이내의 공간에서 전파 특성이 안정적이며 이는 개발 제품이 원하는 사용 범위에 속한다.

Treatment of Rolled Steel Coolant Wastewater by Superconducting High Gradient Magnetic Separation

  • Kim, Tea-Hyung;Ha, Dong-Woo;Oh, Sang-Soo;Kim, Ho-Sup;Ko, Rock-Kil;Lee, Nam-Jin;Kwon, Jun-Mo;Kim, Young-Hun;Kung, Chae-Hun;Ha, Tae-Wook
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 하계학술대회 논문집
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    • pp.354-354
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    • 2009
  • We have developed the prototypes of superconducting magnetic separation system with high temperature superconductor wire. This separation filter system consist of magnetized matrix SUS430 wire and acrylic frame. This study introduced rolled steel process coolant wastewater applied superconductor HGMS(High Gradient Magnetic Separation). HGMS treatment have acted high efficient method for various wastewater. We have surveyed superconducting magnetic separation technology and reviewed the status of related industries using applied superconductivity. In our basic preliminary experiment using HGMS, it was made clear that the fine para-magnetic particles in the wastewater obtained from rolling process of steel can be separated with high efficiency. We investigated the ability of magnetic flock formation, which used inorganic materials and polymer coagulants. We had a purpose to remove SS of coolant at steel factory. Maximum coagulation remove rate of SS 98%. Removing ratio of $Fe_3O_4$ fine particles in wastewater showed over than 99% in the wastewater containing magnetic fines after four times of repetition of separation.

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EGR Cooler 대체용 Vortex Tube의 에너지 분리 현상에 관한 실험적 연구 (Experimental Study on the Energy Separation of the Vortex Tube for EGR Cooler)

  • 김창수;박성영
    • 한국산학기술학회논문지
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    • 제11권1호
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    • pp.55-60
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    • 2010
  • 고압의 가스를 이용하여 고온 가스와 저온 가스를 분리하거나 입자상 물질의 분리에 사용 할 수 있는 장치인 볼텍스 튜브의 에너지 분리 특성을 적용하여 자동차의 EGR Cooler 대체장치의 기본 설계 자료를 구축하기 위하여 실험을 수행하였다. 설계를 위한 기초 자료를 확보하기 위하여, 볼텍스 튜브의 입구 압력, 저온출구 및 고온출구압력 변화에 따른 에너지 분리 특성을 분석하였다. 공급압력이 상승할수록 에너지 분리 효과가 상승하였으며, 최고온도는 저온유량비가 약 0.85 에서, 최저온도는 저온유량비가 약 0.35 에서 발생하였다. 볼텍스 튜브의 고온측 출구온도는 고온측 및 저온측 출구압력에 영향을 받으며, 저온측 출구온도는 출구압력 변화에 독립적인 온도변화 특성을 나타내었다. 본 연구의 결과는 자동차의 EGR Cooler 대체장치의 기본 설계 자료로 응용될 수 있을 것이다.

관절염환자(關節炎患者)의 특성(特性)에 대한 조사(調査) 연구(硏究) (A Research in the Characteristic of Arthritis Patienth)

  • 강점덕;남철현;김기열
    • 대한예방한의학회지
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    • 제1권1호
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    • pp.149-165
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    • 1997
  • In order that, investigating the feature of patients suffering arthritis, analysing its contents, and grasping a Primary factor affecting it, I might offerbasic datas which could help to plan and perform healthy affairs to thake precautions beforehand, I have investigated, analysed, and studied a total of 320 patients suffering arthritis, who have received physiotherapy in hospital located in Teaegu area for five months, from November 1 1995 to March 30 1996, of which summary and conclusion is this. 1. The general feature of patients in investigative objects In the distribution of the distinction of sex, men accounted for 26.9% and women, for 73.1%, and, in the fistribution of age, 60-year-old or more, most for 27.2% and from 20 to 29 years old, least for 14.0%. In the distinction of a vocation, housewives most accounted for 34.7% and students(jobless men), least for 19.3%. In the distinction of a matrimonial state, married persons most accounted for 76.7% and people living alone(divorce, separation by death, separation), least for 11.4%. In the distinction of an economic state, the middle classes most accounted for 73.5% and the upper classes, least for 2.9%. In the distinction of their academic careers, graduates of a primary school most accounted for 26.9% and graduates of university, for 14.1%, of which patients, having the ability to decode the national language, reached to 11.3%. In the distinction of the house form, people living in independent houses most accounted for 76.4% and residents in apartment(having an elevator), least for 9.4%. 2. In the distribution of the recurring state in the distinction of the feature, the recurring group was more than the group of patients falling that ill at first as 62.2% and in the distinction of the feature of the recurring group, the recurring group turned high in case of men being from 50s to 60s years old or more, people living alone (divorce, separation by death, separation), students (joblessmen), people working in farming, stockbeeding, forestry, fisheries, a simple labour, graduates of a primary school I having the ability to decode the national language, the upper classes, people part two years since they begined to suffer arthritis, people who had members having ever experienced arthritis among families. 3. In the distribution of arthritis on the distinction of bodily pars, a knee articulation most accounted for 50.2% and the articulation of fingers, for 8.8%, wile the simultaneous, several parts (multiple) accounted for 35.1%. In the distinction of the feature, arthritis of a knee turned high in case of men being from 20s to 30s years old, unmarried persons, people having academic careers of university, the middle classes, residents in apartment (having stairs). In the dictnction of a feature the case of several parts (multiple) turned high in case of women being from 50s to 60s years old or more, people living alone (divorce, separation by death, separation), people having the ability to decode th. national language, the graduates of a primary school, the upper classes, residents in apartment (having elevator). 4. In the distribution of arthritis on e distinction of a contracting term, two years or more most accounted for 51.6% and the case of contacting from one year to two years, for 15.3%. Analysing the distinction of the feature, the case of two years or more turned high in case of women being from 50s to 60s years old or more, people living alone (divorce separation by death, separation), the upper classes, people having the ability to decode the national language, residents in apartment (having elevator). 5. In the distribution of an treatment institution before patients came to help, their not curing most accounted for 39.1%, general, orthopedic, neurological surgery (physical therapy), for. 20.0%, and th. therapy of Chinese medicine (acupuncture, moxacautery, Chinese medicine), for 17.5%, and a pharmacy (medical therapy), for 13.4%. The case of patients not curing, in the distinction of a feature, turned high in case of men 20s years old, unmarried, the lower classes, people having academic careers of university, residents in apartment (having elevator). 6. In e distribution of the extent of satisfaction with treatment, common most accounted for 54.4% and some satisfaction, for 32.8%. The case of common, in the distinction of a feature, turned high, in case of men living alone from 50s to 60s years old (divorce, separation by death, separation), married persons, the upper classes, people having academic careers of university, residents in independent house, residents in apartment (having elevator), 7. In the distribution of the degree of knowledge of the cause of arthritis, patients knowing that the cause is to use very much a articulation in normal times most accounts for 60.1%, and patients knowing the state of short nutrition as a cause, for 2.5%. The case of patients knowing that the cause is to use very much in normal times, in the distinction of a feature, turned high in·case of ment being 20s and 60s years old or more, unmarried persons, e lower classes, people having the ability to decode. the national language, people having academic careers of university, residents in apartment (having stairs), 8. In the distribution of the state of physical exercise before arthritis contracted, patients exercising very much on the whole most accpimend for 40.3%, and patients not exercising, for 34.7%. The case of patients exercising very much on the whole, in the distinction of the feature, turned high in case of men being from 50s to 60s years old or more, people living alone(divorce, separation by death, separation), the lower classes, people having the ability to decode the national language, graduates of a primary school, residents in apartment (having elevator). 9. In the taste of patients suffering from arthritis, while the group of patients falling that ill at first and the recurring group didn't smoke cigarets, during alcohol and coffee on the whole, and the group of patients falling once again that ill drank a cup of distilled linquor and three cup of coffee or more on the whole per one day, and the group of patients falling that ill at first liked sort of vegetables and the recurring group liked very much sons of vegetables and fresh and meat in their loving food normal times. 10. Analysing the distribution on the dining table used by patients and the structure of a powder room, at first, in the structure of a powder room, the group of patients filling that ill have a toilet stool using as their sits, and a Bush toilet on the whole, and the recurring group, a toilet stool using as their sits and conventional type, and in the structure of a dinning table, the group of patients falling that ill at first and the recurring group turned high, each as 66.9% and 6.3%, who have a dining table carring here and there. 11. In the distribution of patients of arthritis in relation to stress, the case that they feeled severly symptoms of arthritis when thay got stress, turned high, each, as 78.6% in the recurring poop, and the case not knowing, as 61.5% in the first group. In the extent of stress normal times, the case that they got much stress on the whole turned high, each, as 72.4% in e recurring group, and the care that got less stress on the whole, as 60.0%. 12. In the distribution on the distinction of symptoms and impedimental extent, the recurring group turned high in each variable. Analysing the feature of the recurring group, in the distinction of symptoms, the case that they fooled much that the node of an articulation is stiff, turned high, as 71.6, and in the distinction of treatment before. patients came to helpk, the theraphy of Chinese medicine (physical theraphy), as 84.4%, the theraphy of Chinese medicine (acupuncture, moxacautery, Chinese medicine), as 73.2%, and in the distinction of the satisfing extent on treatment, the case of comman, as 72.3%, and in the cause of arthritis, the case not recruiting their health after a birth, as 68.5%, and the case not recovering wholely an articulation having got hurt, as 62.8%, and in the state of physical exercise before they begined suffering from arthritis, the case exercising very much on the whole, (as 74.2%), and in the extent of subjective impediment, the case of not being able to act almost, as 66.7%, the case of acting but feeling some hard, as 66.3%. 13. The correlation in variables in relation to arthritis Analysing realted variables, the recurring frequency showed correlation with such as the extent that patients got stress normal times, and the exercising state before suffering arthritis, and showed contra-correlation with academic careers, the wights, coffee. The cigaret, e loving food of taste, showed corralation with the weight, stature, alcohole as the loving food of taste. On the basis of this result medical members of heal, who are related to the regular education, public education or development of this program, should be concerned to prevent orthris.

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6-sigma 방법론을 적용한 종합설계 교육모델 개발 (Development of Capstone Design Education Model Using 6-sigma Methodology)

  • 유경현
    • 공학교육연구
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    • 제23권4호
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    • pp.28-36
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    • 2020
  • Capstone design education is essential in the engineering design process according to the certification standards of ABEEK. Capstone design process should be properly trained in undergraduate courses in order to increase the design ability of systems, components and processes within realistic constraints. In this study, a modified design model as a capstone design education model was proposed to reduce the separation between the design process at industrial sites and the design process at university education. The modified design model based on 6-sigma methodology is composed of 6 design steps such as define, measure, analyse, design, verify, and report. Each step has appropriated design contents and tools, and is configured to generate design results. The proposed design model was directly applied to the capstone design class for automotive engineering in Kunsan National University, and it was confirmed that the proposed DMADVR methodology was a very useful design education model to enhance the design ability, teamwork ability and communication skills required by ABEEK.

Separation of Calcium-binding Protein Derived from Enzymatic Hydrolysates of Cheese Whey Protein

  • Kim, S.B.;Shin, H.S.;Lim, J.W.
    • Asian-Australasian Journal of Animal Sciences
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    • 제17권5호
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    • pp.712-718
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    • 2004
  • This study was carried out to separate the calcium-binding protein derived from enzymatic hydrolysates of cheese whey protein. CWPs (cheese whey protein) heated for 10 min at $100^{\circ}C$ were hydrolyzed by trypsin, papain W-40, protease S, neutrase 1.5 and pepsin, and then properties of hydrolysates, separation of calcium-binding protein and analysis of calcium-binding ability were investigated. The DH (degree of hydrolysis) and NPN (non protein nitrogen) of heated-CWP hydrolysates by commercial enzymes were higher in trypsin than those of other commercial enzymes. In the result of SDS-PAGE (sodium dodecyl sulphate polyacrylamide gel electrophoresis), $\beta$-LG and $\alpha$-LA in trypsin hydrolysates were almost eliminated and the molecular weight of peptides derived from trypsin hydrolysates were smaller than 7 kDa. In the RP-HPLC (reverse phase HPLC) analysis, $\alpha$-LA was mostly eliminated, but $\beta$-LG was not affected by heat treatment and the RP-HPLC patterns of trypsin hydrolysates were similar to those of SDS-PAGE. In ion exchange chromatography, trypsin hydrolysates were shown to peak from 0.25 M NaCl and 0.5 M NaCl, and calcium-binding ability is associated with the large peak, which was eluted at a 0.25 M NaCl gradient concentration. Based on the results of this experiment, heated-CWP hydrolysates by trypsin were shown to have calcium-binding ability.

용매추출에 의한 코발트 분리 기술 (Extraction/Separation of Cobalt by Solvent Extraction: A Review)

  • ;조성수;이계호;이찬기;엄성현
    • 공업화학
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    • 제26권6호
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    • pp.631-639
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    • 2015
  • 용매추출에 의한 코발트 분리 기술에 대해 리뷰하였고 특히 다양한 시약을 사용한 코발트의 분리 및 상용 추출용제를 사용하여 스크랩으로부터의 코발트 회수기술에 대하여 분석하였다. 코발트 분리 능력은 phosphinic > phosphonic > phosphoric acid 순으로 정리되며, 이것은 유기상내에 추출용제와 존재하는 코발트의 사면체 배위 화합물의 안정성이 증가하기 때문이다. 용매의 조성에 따라 달라지지만 주로 Cyanex 272, D2EPHA 및 PC 88A와 같은 상용 추출용제 등이 상용 추출 공정에서 우선적으로 사용되어야 하며, 다양한 조합을 효과적으로 관리한다면 코발트 함유 스크랩과 관련한 다양한 분리기술 문제점들을 해결할 수 있을 것이다.