• Title/Summary/Keyword: Scale-up process

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Comparison of EG/AD/S and EG/AD model ice properties

  • Kim, Jung-Hyun;Choi, Kyung-Sik
    • International Journal of Ocean System Engineering
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    • v.1 no.1
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    • pp.32-36
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    • 2011
  • EG/AD/S type model ice was originally selected as the primary model ice material for the MOERI ice tank in Korea. The existence of a sugar component in the EG/AD/S mixture may cause a serious maintenance problem. In order to understand the influence of sugar in the original model ice, a series of tests with EG/AD/S and EG/AD model ices were performed, and their material properties compared. Because the target strength of model ice in the full-scale MOERI ice tank is expensive and difficult to control, tests were performed under cold room conditions using a miniature ice tank. This paper describes the material properties of EG/AD/S and EG/AD model ices, such as flexural strength, compressive strength and elastic modulus. In order to obtain the desired strength and stiffness levels for the model ice, a warm-up process was introduced.

Development and Validation of the Empowerment Scale for Woman with Breast Cancer (유방암여성 임파워먼트 측정도구 개발 및 타당화)

  • Shin, Sun Hwa;Park, Hyojung
    • Journal of Korean Academy of Nursing
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    • v.45 no.4
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    • pp.613-624
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    • 2015
  • Purpose: The purpose of this study was to develop a scale to evaluate empowerment in woman with breast cancer and to examine the validity and reliability of the scale. Methods: The development process for the initial items included a literature review, interviews, and construction of a conceptual framework. The identified items were evaluated for content validity by experts, resulting in 3 factors and 48 preliminary items. Participants were 319 women with breast cancer recruited to test reliability and validity of the preliminary scale. Data were analyzed using item analysis, confirmatory factor analysis, criterion related validity, internal consistency and test-retest reliability. Results: The final scale consisted of 30 items and 3 factors. Factors, including 'intrapersonal factor' (14 items), 'interactional factor' (8 items), and 'behavioral factor' (8 items), were drawn up after confirmatory factor analysis. Goodness of fit of the final research model was very appropriate as shown by ${\chi}^2/df=1.86$, TLI=.90, CFI=.92, SRMR=.06, and RMSEA=.05. Criterion validity was evaluated by total correlation with the Cancer Empowerment Questionnaire .78. Cronbach's alpha for total items was .93 and test-retest reliability was .69. Conclusion: Findings from this study indicate that the scale can be used in the development of nursing interventions to promote the empowerment of women having breast cancer.

Performance of Pilot-Scale Biodiesel Production System (파일럿 규모의 바이오디젤 생산공정의 실증연구)

  • Jeong, Gwi-Taek;Park, Jae-Hee;Park, Seok-Hwan;Park, Don-Hee
    • KSBB Journal
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    • v.24 no.1
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    • pp.89-95
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    • 2009
  • Biodiesel (fatty acid alkyl esters), which is produced from sustainable resources such as vegetable oil, animal fat and waste oils, have used to as substitutes for petro-diesel. In this study, we investigate the performance of 30 L and 300 L pilot-scale biodiesel production system using alkali-catalyst transesterification from soybean oil and rapeseed oil produced at Jeju island in Korea. The 30 L-scale biodiesel production was performed to in the condition of reaction temperature $65^{\circ}C$, catalyst amount 1% (w/w) and oil to methanol molar ratio 1 : 8. At that reaction condition, the fatty acid methyl ester contents of product are above 98% within reaction time 30 min. Also, the conversion yield of over 98% was obtained in 300 L-scale biodiesel production system using rapeseed oil and soybean oil. The quality of biodiesel produced from reaction system was satisfied to recommended quality standard of Korea. Our results may provide useful information with regard to the scale-up of more economic and efficient biodiesel production process.

Process Balance of Natural Indigo Production based on Traditional Niram Method

  • Shin, Younsook;Yoo, Dong Il;Kim, Kangwha
    • Textile Coloration and Finishing
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    • v.24 no.4
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    • pp.253-259
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    • 2012
  • In this work, the natural indigo production process from Polygonum tinctorium was balanced based on the traditional Niram method in Korea. A standard procedure was determined considering the conditions of indican extraction from plant material, the amount of alkali for precipitation, storage of extract, etc. The effect of experimental conditions on the yield of crude dye was investigated. The contents of indigo and indirubin of the crude dyes were analyzed by HPLC. Increase of the amount of crude dye was observed within 1-2.5 days of extraction time. Longer extraction beyond 2.5 days resulted in a slight decrease in the amount of crude dye. There was no consistency in terms of indigo content depending on extraction pH. We found that the storage of extract or harvested plants affected adversely to dye yield and dye quality. Based on the lab scale extraction, large scale extraction was performed for 2-2.5 days in water and 2.0-2.5 g/L of $Ca(OH)_2$ was applied for precipitation of indigo dye. We obtained natural indigo dye containing about 15% of pure indigo in scale-up production using whole plant except root.

Optimization for Small-scale Process of Swine Wastewater Treatment Using Rhodopseudomonas palustris KK14 (Rhodopseudomonas palustris KK14를 이용한 소규모 돈분폐수처리공정의 최적화)

  • Kim, Han-Soo;Oh, Chun-Hyun;Kim, Hyuk-Il;Cho, Hong-Yon;Yang, Han-Chul
    • Applied Biological Chemistry
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    • v.37 no.4
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    • pp.303-309
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    • 1994
  • To develop the treatment process of swine wastewater using Rhodopseudomonas palustris KK14 with high utilizable ability of organic acids, some operating conditions were investigated and optimized in flask-scale and laboratory-scale reactors. The optimal operating conditions in photosynthetic bacteria (PSB) reactor of semi-continuous type were obtained at HRT 6 day, 5% (v/v/day) seeding rate of PSB sludge and 10% (v/v/day) returning rate of PSB return sludge. Under the above operating condition, COD level of the wastewater (initial COD: 10 g/l) was reduced to about 1.7 g/l after 4 days treatment and MLSS was held constant at $4{\sim}5\;g$ per liter. In laboratory-scale process consisted of 5.2 l anaearobic digestion reactor and 15 l PSB reactor, the total removal rates of COD and BOD were increased to 95% and 96% by the continuous operation for 5.36 days, respectively, showing $3kg\;COD/m^3/day$ COD loading rate and 1.1 Kg COD/Kg MLSS/day sludge loading rate in PSB reactor. The offensive odor was considerably removed through the treatment process of swine wastewater.

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Characteristics of Preparative Liquid Chromatography (제조용 액체 크로마토그래피의 특성)

  • Row, Kyung-Ho;Jin, Yin-Zhe
    • KSBB Journal
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    • v.20 no.3
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    • pp.149-163
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    • 2005
  • Recently preparative liquid chromatography (PLC) has been used more frequently to separate drugs and natural substances. This modern separation methodologies require reliable tools that perform on a high level in terms of efficiency and reproducibility. However, large-scale PLC easily tends to reduce the yield and purity of the product. To promote the separation efficiency of PLC, we need to properly understand the controlling effects of the process, which may enable to predict the process and to improve the design and operation of PLC. Progress in computer technology allows the use of sophisticated models, provided their parameters can be measured. Some hardwares as well as softwares for PLC were already commercially available. In this work, the separation characteristic of PLC will be reviewed and compared on both the software and the hardware.

Thermal Stability Improvement of Ni-Silicide using Ni-Co alloy for Nano-scale CMOSFET (나노급 CMOSFET을 위한 니켈-코발트 합금을 이용한 니켈-실리사이드의 열안정성 개선)

  • Park, Kee-Young;Jung, Soon-Yen;Han, In-Shik;Zhang, Ying-Ying;Zhong, Zhun;Li, Shi-Guang;Lee, Ga-Won;Wang, Jin-Suk;Lee, Hi-Deok
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.1
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    • pp.18-22
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    • 2008
  • In this paper, the Ni-Co alloy was used for thermal stability estimation comparison with Ni structure. The proposed Ni/Ni-Co structure exhibited wider range of rapid thermal process windows, lower sheet resistance in spite of high temperature annealing up to $700^{\circ}C$ for 30 min, more uniform interface via FE-SEM analysis, NiSi phase peak. Therefore, The proposed Ni/Ni-Co structure is highly promising for highly thermal immune Ni-silicide for nano-scale MOSFET technology.

High performance ultrafine-grained Ti-Fe-based alloys with multiple length-scale phases

  • Zhang, Lai-Chang
    • Advances in materials Research
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    • v.1 no.1
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    • pp.13-29
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    • 2012
  • In order to simultaneously enhance the strength and plasticity in nanostructured / ultrafine-grained alloys, a strategy of introducing multiple length scales into microstructure (or called bimodal composite microstructure) has been developed recently. This paper presents a brief overview of the alloy developement and the mechanical behavior of ultrafine-grained Ti-Fe-based alloys with different length-scale phases, i.e., micrometer-sized primary phases (dendrites or eutectic) embedded in an ultrafine-grained eutectic matrix. These ultrafine-grained titanium bimodal composites could be directly obtained through a simple single-step solidification process. The as-prepared composites exhibit superior mechanical properties, including high strength of 2000-2700 MPa, large plasticity up to 15-20% and high specific strength. Plastic deformation of the ultrafine-grained titanium bimodal composites occurs through a combination of dislocation-based slip in the nano-/ultrafine scale matrix and constraint multiple shear banding around the micrometer-sized primary phase. The microstructural charactersitcs associated to the mechanical behaivor have been detailed discussed.

A Study on Gas-Liquid Reaction Intensification by Using Rotating Flow (회전유동을 이용한 기체-액체 반응 촉진 기술 연구)

  • Jun Sang Park
    • Journal of the Korean Society of Visualization
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    • v.21 no.2
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    • pp.45-54
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    • 2023
  • In the present study, we propose new type of a spinning disk reactor(SDR) with high performance and very convenient structure to make a large scale equipment from lab-scale than the conventional one. A split-disk experimental equipment, based on new type of spinning disk reactor, has been developed to generate an energy to break a bulk of injected gas into smaller gas bubble. Several cases of an experimental observation make it to confirm that a bulk of injecting gas could be continuously break into smaller bubbles. It shows the feasibility to make a scale-up of SDR by using the characteristic of Taylor-Proudman column in rotating flow. A theoretical study on single phase liquid flow is given to predict a liquid induced shear stress, which make the present study to be self-containment.

Non-Thermal Plasma Technique for Removing $SO_2$ and $NO_x$ from Combustion Flue Gas (연소가스내 탈황탈질처리를 위한 저온 플라즈마 기술)

  • Song, Yeong-Hun;Sin, Wan-Ho;Kim, Seok-Jun;Jang, Gil-Hong
    • 한국연소학회:학술대회논문집
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    • 1997.06a
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    • pp.69-76
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    • 1997
  • Industrial-scale pulse corona process to remove $SO_2$ and $NO_x$ simultaneously from combustion flue gas has been studied. The pilot plant built in the present study treats 2,000 $Nm^3$/hr of flue gas from a boiler. The geometry of the pulse corona reactor is similar to that of an electrostatic precipitator commonly used in industry, A thyratron switch and magnetic pulse compressors, which can generate up to 130 kV of peak pulse voltage and up to 30 kW of average pulse power, have been used to produce pulsed corona. The removal efficiencies of $S0_2$ and $NO_x$ with the present process are maximum of 95 % and 85 %, respectively. Electrical power consumption to produce the pulsed corona, which has been one of the major difficulties to apply this process to industry, has been evaluated in the present study. The results showed that the power consumption can be reduced significantly by simultaneous addition of hydrocarbon injection and heterogeneous phase reactions to the process.

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