• Title/Summary/Keyword: SPS

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Fabrication of TiAl Alloys by Mechanical Milling and Spark Plasma Sintering (기계적 분쇄화 및 스파크 플라즈마 소결에 의한 TiAl 합금의 제조)

  • Kim, M.S.;Kim, J.S.;Hwang, S.J.;Hong, Y.H.;Oh, M.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.1
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    • pp.17-22
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    • 2004
  • In the present study, newly developed spark plasma sintering(SPS) technique was introduced to refine the grain size of ${\gamma}$-based TiAl intermetallic compounds. Ti-46Al-1.5Mo and Ti-46Al-1.5Mo-0.2C(at%) prealloyed powders were produced by mechanical milling(MM) in high-energy attritor. The mechanically milled powders were characterized by XRD and SEM for the microstructural evolution as a function of milling time. And then, the MMed powders were sintered by both spark plasma sintering and hot pressing in vacuum (HP). After the sintering process, MM-SPSed specimens were heat-treated in a vacuum furnace (SPS-VHT) and in the SPS equipment(MM-SPS) for microstructural control. It was found from microstrutural observation that the microstructure consisting of equiaxed ${\gamma}$-TiAl with a few hundred nanometer in average size and ${\alpha}_2-Ti_3Al$ particles were formed after both sintering processes. It was also revealed from hardness test and three-point bending test that the effect of grain refinement on the hardness and bending strength is much higher than that of carbon addition. The fully lamellar microstructures, which is less than $80{\mu}m$ in average grain size was obtained by SPS-VHT process, and the fully lamellar microstructure which is less than $100{\mu}m$ in average grain size was obtained by MM-SPS for a relatively shorter heat-treatment time.

Preparation of β-FeSi2 Thermoelectric Materials by MA/SPS Process -Formation ofβ-FeSi2Phase- (MA/SPS 공정에 의한 β-FeSi2 열전재료의 제조(I) -β-FeSi2상의 형성-)

  • Kim, Hwan-Tae;Gwon, Yeong-Sun;Lee, Chung-Hyo
    • Korean Journal of Materials Research
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    • v.12 no.3
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    • pp.176-181
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    • 2002
  • Fabrication of ${\beta}-FeSi_2$ was attempted by making use of the combined process of mechanical alloying (MA) and spark plasma sintering (SPS). MA was performed under the Ar gas atmosphere using mixed powders of pure iron and silicon having the mole fraction of 1:2. SPS process was performed at 800-85$0^{\circ}C$ with the applied pressure of 50MPa and the holding time was ranging from 0 to 30min. The mechanically alloyed powder by cyclic operation of rotor for 15hrs consisted of $\varepsilon$-FeSi and Si phases. When this mechanically alloyed powder was sintered by SPS process above 85$0^{\circ}C$, $\varepsilon$-FeSi and ${\alpha}-Fe_2Si_5$ phase were formed. Bulk product sintered at 82$0^{\circ}C$ for 30min consisted of ${beta}-FeSi_2$ phase with a small fraction of $\varepsilon$-FeSi and the density of sintered specimen was 75.3% theoretical density. It was considered that the MA/SPS combined process was effective for the preparation of ${\beta}-FeSi_2$ without heat treatment process after sintering.

An Empirical Relation between the Plating Process and Accelerator Coverage in Cu Superfilling

  • Cho, Sung-Ki;Kim, Myung-Jun;Koo, Hyo-Chol;Kim, Soo-Kil;Kim, Jae-Jeong
    • Bulletin of the Korean Chemical Society
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    • v.33 no.5
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    • pp.1603-1607
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    • 2012
  • The effects of plating process on the surface coverage of the accelerator were investigated in terms of Cu superfilling for device metallization. When a substrate having 500 nm-wide trench patterns on it was immersed in an electrolyte containing poly (ethylene glycol) (PEG)-chloride ion ($Cl^-$)-bis(3-sulfopropyl) disulfide (SPS) additives without applying deposition potential for such a time of about 100s, voids were generated inside of the electrodeposit. In time-evolved electrochemical analyses, it was observed that the process (immersion without applying potential) in the electrolyte led to the build-up of high initial coverage of SPS-Cl on the surface, resulting in the fast saturation of the coverage. Repeated experiments suggested that the fast saturation of SPS-Cl failed in superfilling while a gradual increase in the SPS-Cl coverage through competition with initially adsorbed PEG-Cl enabled it. Consequently, superfilling was achievable only in the case of applying the plating potential as soon as the substrate is dipped in an electrolyte to prevent rapid accumulation of SPS-Cl on the surface.

MEAC Method for Analysis of Power System Stability Improving Effect Considering Run-up SPS Function of HVDC (MEAC를 적용한 HVDC Run-up SPS의 안정도향상 효과분석)

  • Lee, Jae-Gul;Song, Ji-Young;Jang, Gil-Soo
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.66 no.10
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    • pp.1454-1459
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    • 2017
  • In spite of continuous increase of electric power demand and new generation plants, it is very difficult to install new transmission line. Therefore, it comes to be difficult to operate the power system stable, so it is required to find another way to get new transmission capacity. Because HVDC transmission system installation is the one of the best option for us, we have undertake the HVDC project in mainland. Buckdangjin-Goduck HVDC project(500kV, 3GW) is currently under construction and Eastern Power HVDC project(500kV, 8GW) is under the study for technical specification. Both of them have the Run-up SPS function for taking action of 765kV Transmission line fault. The Run-up SPS function increases the active power output of the HVDC rapidly when the transmission line between the power plant and network is tripped, thereby preventing the generator from overspeed and improving the power system stability. In this paper, we propose MEAC(Modified Equal Area Criteria) method based on traditional EAC method to quantitatively evaluate the effect of the HVDC run-up SPS function on the power system stability improvement.

Password System Enhancing the Security agains (타인의 관찰에서 안전한 패스워드 시스템)

  • Park Jong-Min;Kim Yong-Hun;Cho Beom-Joon
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.8 no.8
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    • pp.1790-1795
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    • 2004
  • In this paper, the new password system called SPS(Secure Password System) in order to enhance the security of the system as well as to improve the weakness of the password which is very easy to be disclosed by other people, improving the methods which is identifying the users' legality using the computer system in the multi-users computer. SPS is adopting several strong points such as Easy Embodiment, Low Cost, and most of the good points of the traditional password system. In addition, it makes an easy introduction from the traditional password system. Above SPS has the high stable security in the practical experiments about both the literal attack of the online intruders and the exposure of Clients' password.

Effect of Growth Temperature on the Luminescence Properties of InP/GaP Short-Period Superlattice Structures

  • Byun, Hye Ryoung;Ryu, Mee-Yi;Song, Jin Dong;Lee, Chang Lyul
    • Applied Science and Convergence Technology
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    • v.24 no.1
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    • pp.22-26
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    • 2015
  • The optical properties of InP/GaP short-period superlattice (SPS) structures grown at various temperatures from $400^{\circ}C$ to $490^{\circ}C$ have been investigated by using temperature-dependent photoluminescence (PL) and emission wavelength-dependent time-resolved PL measurements. The PL peak energy for SPS samples decreases as the growth temperature increases. The decreased PL energy of ~10 meV for the sample grown at $425^{\circ}C$ compared to that for $400^{\circ}C$-grown sample is due to the CuPt-B type ordering, while the SPS samples grown at $460^{\circ}C$ and $490^{\circ}C$ exhibit the significant reduction of the PL peak energies due to the combined effects of the formation of lateral composition modulation (LCM) and CuPt-B type ordering. The SPS samples with LCM structure show the enhanced carrier lifetime due to the spatial separation of carriers. This study represents that the bandgap energy of InP/GaP SPS structures can be controlled by varying growth temperature, leading to LCM formation and CuPt-B type ordering.

Korean and English affricates in bilingual children

  • Yu, Hye Jeong
    • Phonetics and Speech Sciences
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    • v.9 no.3
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    • pp.1-6
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    • 2017
  • This study examined how early bilingual children produce sounds in their two languages articulated with the same manner of articulation but at different places of articulation. English affricates are palato-alveolar and Korean affricates are alveolar. This study analyzed the frequencies of center of gravity (COG), spectral peak (SP), and the second formant (F2) of word-initial affricates in English and Korean produced by twenty-four early Korean-English bilingual children (aged 4 to 7), and compared them with those of monolingual counterparts in the two languages. If early Korean-English bilingual children produce palato-alveolar affricates in English and alveolar affricates in Korean, they may produce Korean affricates with higher COGs, SPs, and F2s than English affricates. The early Korean-English bilingual children at the age of 4 produced English and Korean affricates with similar COGs, SPs, and F2s, and the COGs, SPs, and F2s of their Korean affricates were similar to those of the Korean monolingual counterparts. However, the early bilingual children at the age of 5 to 7 had lower COGs and SPs for English affricates with higher F2s compared to Korean affricates, and the COGs, SPs, and F2s of their English affricates were similar to those of the English monolingual counterparts.

Development of Auto-navigation System having Automatically Changeable Function for Main Navigation Equipments (주요 항해장비의 자동대체기능을 가지는 항해자동화 시스템의 개발)

  • 이정우;이덕상;김득태;정일영;심탁섭;이성신;배진호
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2001.05a
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    • pp.737-740
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    • 2001
  • We develope the PC based SPS to improve safety at sea, save fuel and time during a voyage and makes mariner's work more efficient and comfortable in ship navigation, who propose the auto-navigation system with SPS as basic main system. Developed SPS operate the function to monitor navigational equipment and to substitute a broken main navigational equipment such as CIS, ECDIS, or Radar/ARPA, automatically. These can be improve more efficient and comfortable ship navigation and reduce these traffic accident. The SPS has the function as DB and network server, additionally.

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Ductile Fracture Behaviour of SPS Specimen Under Pure Mode II Loading (순수 모드 II하중 하에서의 SPS 시험편의 연성파괴 특성에 관한 연구)

  • O, Dong-Jun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.2
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    • pp.289-295
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    • 2001
  • The aim of this study is to investigate the ductile fracture behaviour under pure Mode II loading using A533B pressure vessel steel. Single punch shear(SPS) test was performed to obtain the J-R curve under pure Mode II loading which was compared with that of the Model I loading. Simulation using Rousellier Ductile Damage Theory(RDDT) was carried out with 4-node quadrilateral element(L(sub)c=0.25mm). For the crack advance, the failed element removal technique was adopted with a $\beta$ criterion. Through the $\beta$ value tuning-up procedures, $\beta$(sub)crit(sup)II was determined as 1.5 in contrast with $\beta$(sub)crit(sup)I=5.5. In conclusion, it was found that the J-R curve under Mode II loading was located at lower part than that under Mode I loading obtained from the previous study and that the $\beta$ values strongly depended on the loading type. In addition, the predicted result using RDDT showed a good agreement with the SPS experimental one under pure Mode II loading.

Statistical Image Feature Based Block Motion Estimation for Video Sequences (비디오 영상에서 통계적 영상특징에 의한 블록 모션 측정)

  • Bae, Young-Lae;Cho, Dong-Uk;Chun, Byung-Tae
    • The Journal of the Korea Contents Association
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    • v.3 no.1
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    • pp.9-13
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    • 2003
  • We propose a block motion estimation algorithm based on a statistical image feature for video sequences. The statistical feature of the reference block is obtained, then applied to select the candidate starting points (SPs) in the regular starting points pattern (SPP) by comparing the statistical feature of reference block with that of blocks which are spread ower regular SPP. The final SPs are obtained by their Mean Absolute Difference(MAD) value among the candidate SPs. Finally, one of conventional fast search algorithms, such as BRGDS, DS, and three-step search (TSS), has been applied to generate the motion vector of reference block using the final SPs as its starting points. The experimental results showed that the starting points from fine SPs were as dose as to the global minimum as we expected.

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