• 한국자기공명학회논문지
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• 제17권2호
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• pp.81-85
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• 2013

Various fluorine-containing materials are used in electronic devices like LCD display panels and Li-ion batteries. The structural conformation of fluorine in fluorinated materials is an important contributing factor that influences the chemical and physical properties. The conformation can be changed by heat and stress during manufacture or use. Understanding the conformational changes is critical for understanding the performance and durability of electronic devices. Solid-state NMR spectroscopy could be widely used for the analysis of various fluorine-containing materials for electronic devices. However, conventional CPMAS probes cannot be used for in-situ analysis of fluorine-containing electronic devices like LCD panels and Li-ion batteries. In this paper, we show the design, construction, and optimization of a $^{19}F-^{13}C$ double-resonance solid-state NMR probe for a 400MHz wide-bore magnet with a flat square coil for in-situ analysis of fluorine-containing electronic devices without observing fluorine background signals. This custom-built probe does not show any fluorine background signals, and can have higher efficiency for lossy samples.

• Journal of Power Electronics
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• 제17권6호
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• pp.1694-1706
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• 2017

Models and experiments for magnetic resonance coupling wireless power transmission (MRC-WPT) topologies such as the chain topology and branch topology are studied in this paper. Coupling mode theory based energy resonance models are built for the two topologies. Complete energy resonance models including input items, loss coefficients, and coupling coefficients are built for the two topologies. The storage and the oscillation model of the resonant energy are built in the time domain. The effect of the excitation item, loss item, and coupling coefficients on MRC systems are provided in detail. By solving the energy oscillation time domain model, distance enhancing models are established for the chain topology, and energy relocating models are established for the branch topology. Under the assumption that there are no couplings between every other coil or between loads, the maximum transmission capacity conditions are found for the chain topology, and energy distribution models are established for the branch topology. A MRC-WPT experiment was carried out for the verification of the above model. The maximum transmission distance enhancement condition for the chain topology, and the energy allocation model for the branch topology were verified by experiments.

• 한국자기공명학회논문지
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• 제23권1호
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• pp.12-19
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• 2019

A former study has shown that the spin-lattice relaxation time ($T_1$) in cancerous prostate tissue had enhanced contrast at an ultra-low magnetic field, $132{\mu}T$. To study the field dependence and the origin of the contrast we measured $T_1$ in pairs of ex-vivo prostate tissues at the Earth's magnetic field. A portable and coil-based nuclear magnetic resonance (NMR) system was adopted for $T_1$ measurements at $40{\mu}T$. The $T_1$ contrast, ${\delta}=1-T_1$ (more cancer)/$T_1$(less cancer), was calculated from each pair. Additionally, we performed pathological examinations such as Gleason's score, cell proliferation index, and micro-vessel density (MVD), to quantify correlations between the pathological parameters and $T_1$ of the cancerous prostate tissues.

• 한국의학물리학회지:의학물리
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• 제31권4호
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• pp.189-193
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• 2020

An MR-based attenuation correction (MRAC) map plays an important role in quantitative positron emission tomography (PET) image evaluation in PET/magnetic resonance imaging (MRI) systems. However, the MRAC map is affected by the magnetic field inhomogeneity of MRIs. This study aims to evaluate the characteristics of MRAC maps of physical phantoms on PET/MRI images. Phantom measurements were performed using the Siemens Biograph mMR. The modular type physical phantoms that provide assembly versatility for phantom construction were scanned in a four-channel Body Matrix coil. The MRAC map was generated using the two-point Dixon-based segmentation method for whole-body imaging. The modular phantoms were scanned in compact and non-compact assembly configurations. In addition, the phantoms were scanned repeatedly to generate MRAC maps. The acquired MRAC maps show differently assigned values for void areas. An incorrect assignment of a void area was shown on a locally compact space between phantoms. The assigned MRAC values were distorted using a wide field-of-view (FOV). The MRAC values also differed after repeated scans. However, the erroneous MRAC values appeared outside of phantom, except for a large FOV. The MRAC map of the phantom was affected by phantom configuration and the number of scans. A quantitative study using a phantom in a PET/MRI system should be performed after evaluation of the MRAC map characteristics.

• 융복합기술연구소 논문집
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• 제12권1호
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• pp.13-18
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• 2022

Polyacrylonitrile was synthesized through suspension polymerization and then sieved to obtain spherical beads with a size of 200~510 ㎛. PAN was copolymerized with 2 mol% MMA monomer which is known to promote cyclization and crosslinking of nitrile group. The resonance cyclization reaction of the nitrile group in the synthesized PAN beads was observed near 170℃ with thermal analysis and FT-IR. The reaction conversion of the nitrile group in spherical beads was 23% during heat treatment, which was lower than that of the well-oriented PAN fiber used as a precursor of carbon fiber. This is because the stereo-regularity of molecular chains in the form of a random coil (spherical bead) is much lower than that of PAN fiber. It was confirmed that the compressive strength of the spherical PAN bead was greatly improved through the resonance cyclization and shrinkage according to the heat treatment, and it was also observed that the pores in PAN beads were formed after the heat treatment.

• 한국자기공명학회논문지
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• 제26권4호
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• pp.51-58
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• 2022

The baseline flattened NMR spectrum has been achieved by several methodologies including pulse manipulation with a series of phase cycling. The background signal inherent in the probe is also main source of baseline distortion both in solution and solid NMR. The simple direct polarization with 90° pulse flipping the magnetization from the z-axis onto the receiver coil requires the strong rf pulse enough to encompass the wide frequency range to excite the resonance of interest nuclei. Albeit the perfect polarization 90° pulse, the signal from the unwanted magnetic fields such as background signal can not be completely suppressed by suitable phase cycling. Moreover, slowly baseline wiggling signal from the low 𝛾 nuclei is not easy to eliminate with multiple pulse manipulation. So there is still need to contrive the new scheme for that purpose in an adroit manner. In this article new triple pulse excitation schemes for TIP and modified DEPTH pulse sequence are analytically examined in terms of arbitrary phase and flip angle of pulse. The suitable phase cycling for these pulse trains is necessary for the good sensitivity and resolution of the spectrum. It is observed that the ¹³C sensitivity TIP experiment is almost equal to the CP/MAS with modified DEPTH sequence, both of which are applicable to both solid and solution state NMR.

• 치과방사선
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• 제22권1호
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• pp.29-37
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• 1992

The temporomandibular joint was evaluated using magnetic resonance imaging using a urface coil in 11 patients having reciprocal clicking or locking and compared with the normal joint in five subjects. Serial multisection 3㎜-thick parasagittal, paracoronal, and axial image on both closing and opening mouth were obtained with a 1.5 Tesla MR system and surface coil using CSMEMP, GRASS, MPGR, powerful extensions of fast imaging that is currently under clinical evaluation. MR images obtained were analized correlating with the theory of internal derangement. The obtained results were as follows: 1. The serial findings of structures in joint were determined on the serially sectioned images of joint with reciprocal clicking or locking by CSMEMP and MPGR on closing mouth. 2. The delta shaped white images of synovial fluid in the glenoid fossa and on the posterior surface of condyle were revealed on the parasagittal images by MPGR on opening mouth as in the normal joints. 3. The white image of joint fluid surrounding meniscus was recognized on the paracoronal image by GRASS on opening mouth as in the normal joints. 4. In joints having temporomandibular dysfunction the smooth image of displaced meniscus was recognized, but otherwise in the normal joints the image of muscle was noted on the paracoronal image sectioned at the anterior portion of condyle by GRASS. 5. The more thickened fascial plane between superior and inferior belly of lateral pterygoid muscle was not recognizable in joints having temporomandibular dysfunction than in the normal joints.

• 전자공학회논문지
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• 제53권8호
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• pp.119-126
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• 2016

본 논문에서는 의복용 무선전력전송 시스템을 구축을 위한 평면형 직물공진기를 제안하고, 공진기에 사용된 의복용 직물기판의 재질별 특성을 분석하였다. 평면형 직물공진기는 공진주파수가 1-10 MHz가 되도록 직물기판 위에 전도성 물질로 루프 및 코일을 평면 설계하였다. 의복용으로 많이 사용되고 있는 폴리에스테르 섬유와 면을 직물기판으로 사용하였으며, 평면 루프와 코일은 동테이프(copper tape)와 실버페이스트(silver paste)로 설계하였다. 자기공진형 무선전력전송 시스템에 적용된 직물의 재질별 특성을 분석하기 위해 송신부와 수신부를 대칭으로 설계하였다. 실험 결과, 낮은 유전상수 및 비교적 두꺼운 두께를 가진 직물기판과 표면저항이 작은 도체성 재질의 패턴(루프 및 코일)으로 제작되었을 때, 의복용 무선전력전송 시스템이 높은 전송효율을 보였다. 본 연구를 통해 제안된 평면형 직물 공진기는 무선전력전송 기술의 영역을 의복용으로 넓힐 수 있는 가능성을 보여주었다.

• 한국자기학회지
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• 제22권6호
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• pp.200-203
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• 2012

원통형 페라이트 코어와 검출 코일을 이용하여서 직교형 플럭스게이트 센서를 제작하고, 구동주파수가 출력 감도에 미치는 영향에 대해서 조사하였다. 외부 자계에 대한 플럭스게이트 센서의 출력은 코어의 단면적, 권선수, 구동주파수 등에 비례한다. 따라서, 센서를 소형화시키면서 출력(감도)를 저하시키는 것을 방지하기 위해서는 구동주파수를 높이는 것이 필요하다. 그러나, 구동주파수는 자성체 코어의 주파수특성, 구동회로의 성능, 검출 코일의 주파수특성 등 다양한 요인으로 제한 된다. 본 연구에서는 원통형 페라이트 코어와 검출 코일을 이용하여 제작한 직교형 플럭스게이트 센서에 있어서 센서 출력의 주파수특성과 검출 코일의 인덕턴스와 캐패시턴스를 측정하여서 상호 연관성에 대해서 살펴보았다. 그 결과 외부 자계에 대한 센서의 출력은 검출 코일의 임피던스에 의존한다는 것을 알 수 있었고, 검출 코일의 LC공진주파수에서 높은 출력(감도)을 얻을 수 있었다.

• 한국자기학회지
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• 제8권4호
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• pp.241-248
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• 1998

본 연구에서는 micro magnetic device의 제작과 특성 분석을 위하여 고주파수 대역에서 사용가능한 자성체의 개발과 meander형 마이크로 코일의 가공 기술 확립에 그 목적을 두었다. 자성체로서는 DC magnetron reactive sputtering system에 의해 제조된 초 미세결정구조를 갖는 FeTaC, FeTaN막을 사용하였으며, 그 자기적 특성은 다음과 같다. Bs:13~17kG, Hc:0.1~0.2Oe, $\mu$':2000~4000. 전기 도금법에 의해 제작된 Cu코일은 2$\mu$$\Omega$-cm의 비저항을 나타내었으며, 공심형 5turn 언덕터의 경우에는 50nH의 인덕턴스와 700MHz의 공진 주파수 그리고 200MHz에서 30의 성능 지수를 보였다. 또한 meandergudxo의 폐자로 인덕터에서 인덕턴스는 150nH, 공진 주파수는 100MHz, 그리고 성능지수는 10~30 MHz에서 4의 값을 나타내었다.