• Title/Summary/Keyword: Reflection Spectra

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Attenuated total reflection Fourier transform infrared as a primary screening method for cancer in canine serum

  • Macotpet, Arayaporn;Pattarapanwichien, Ekkachai;Chio-Srichan, Sirinart;Daduang, Jureerut;Boonsiri, Patcharee
    • Journal of Veterinary Science
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    • v.21 no.1
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    • pp.16.1-16.10
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    • 2020
  • Cancer is a major cause of death in dogs worldwide, and the incidence of cancer in dogs is increasing. The attenuated total reflection Fourier transform infrared spectroscopic (ATR-FTIR) technique is a powerful tool for the diagnosis of several diseases. This method enables samples to be examined directly without pre-preparation. In this study, we evaluated the diagnostic value of ATR-FTIR for the detection of cancer in dogs. Cancer-bearing dogs (n = 30) diagnosed by pathologists and clinically healthy dogs (n = 40) were enrolled in this study. Peripheral blood was collected for clinicopathological diagnosis. ATR-FTIR spectra were acquired, and principal component analysis was performed on the full wave number spectra (4,000-650 cm-1). The leave-one-out cross validation technique and partial least squares regression analysis were used to predict normal and cancer spectra. Red blood cell counts, hemoglobin levels and white blood cell counts were significantly lower in cancer-bearing dogs than in clinically healthy dogs (p < 0.01, p < 0.01 and p = 0.03, respectively). ATR-FTIR spectra showed significant differences between the clinically healthy and cancer-bearing groups. This finding demonstrates that ATR-FTIR can be applied as a screening technique to distinguish between cancer-bearing dogs and healthy dogs.

Optical Characteristics of Nanocone-patterned c-Si Wafers Coated with Dielectric Thin Films (유전박막이 도포된 나노원뿔 패턴된 단결정 Si 기판의 광특성)

  • Kim, Eunah;Park, Jimin;Ko, Eun-Ji;Kim, Dong-Wook
    • Current Photovoltaic Research
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    • v.5 no.2
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    • pp.55-58
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    • 2017
  • We investigated the influences of dielectric thin film coating on the optical characteristics of c-Si wafers with nanocone (NC) arrays using finite-difference time-domain (FDTD) simulations. Dielectric thin films on high-refractive-index surface can lower optical reflection and reflection dips appear at the wavelengths where destructive interference occurs. The optical reflection of the NC arrays was lower than that of the dielectric-coated planar wafer in broad wavelength range. Remarkable antireflection effects of the NC array could be attributed to beneficial roles of the NCs, including the graded refractive index, multiple reflection, diffraction, and Mie resonance. Dielectric thin films modified the optical reflection spectra of the NC arrays, which could not be explained by the interference alone. The optical properties of the dielectric-coated NC arrays were determined by the inherent optical characteristics of the NC arrays.

Measurement of Milling Ratio using the Visible and the Near-Infrared Rays Spectrum (가시광선 및 근적외선 스펙트럼을 이용한 도정비율 측정)

  • 이용국;이재현
    • Journal of Biosystems Engineering
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    • v.24 no.3
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    • pp.259-266
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    • 1999
  • This research was carried out to investigate the possibility of real time rice milling ratio measurement using the spectral reflection characteristics. In this study, various methods were compared such as \circled1 using the whiteness meter, \circled2 using the colorimeter, \circled3 using the Visible and the NIR reflection spectrum. The samples were milled in the domain of 84~96% by 0.5% interval classified by milling ratio. The NMG treatment method required about 20 minutes to determine the milled ratio and r2 was 0.0028 to 0.7959 that was very low. In case of whiteness meter, r2 was high but speed of measurement was 5 minutes that was very low. Measurement with the colorimeter required about 5 minutes and r2 was 0.60 to 0.85 that was low. The reflection spectrum were measured in the range of 400~2,500nm with 2nm interval and the MLR model with six-wavelength obtained from first derivative of spectra gave the best results(r2 = 0.967, SEP = 0.729%)

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Characterization of thin film properties of Copper(II)-Phthalocyanine using a near-field scanning microwave microscope (근접장 마이크로파 현미경을 이용한 Copper(II)-phthalocyanine 박막의 특성 연구)

  • Park, Mie-Hwa;Lee, Kie-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.460-463
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    • 2003
  • We report the microwave reflection coefficient $S_{11}$ of copper(II)-phthalocyanine(CuPc) using a near-field microwave microscope(NSMM) in order to understand the intrinsic electromagnetic properties of organic materials. For a NSMM system, a high-quility microstip resonator coupled with a dielectric resonator was used. The reflection coefficient $S_{11}$ was changed by the preparation conditions of CuPc thin films. We compared the reflection coefficient with crystal phase, surface morphology, UV absorption spectra and x-ray diffraction results.

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An optical channel-switching transmission filter using the segmented chirped fiber Bragg grating (영역이 분리된 첩 광섬유 격자를 이용한 광 채널 스위칭용 투과 필터의 설계)

  • 박세강;박진우;구현덕;이상배
    • Korean Journal of Optics and Photonics
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    • v.12 no.5
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    • pp.401-405
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    • 2001
  • We propose a novel channel-switching transmission filter using segmented chirped fiber Bragg gratings (CFBG's) each of which has separate transmission bands in the reflection spectrum of the CFBG. The segmented CFBG's are made by using specially designed slits. The separated reflection spectral bands of the segmented CFBG's are controlled by the attached fiber stretchers, and the controlled reflection bands are used to choose the channels independently. Tunability of the transmission spectra is experimentally demonstrated in WDM transmission experiments.

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An analytical model for displacement response spectrum considering the soil-resonance effect

  • Zhang, Haizhong;Zhao, Yan-Gang
    • Earthquakes and Structures
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    • v.22 no.4
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    • pp.373-386
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    • 2022
  • The development of performance-based design methodologies requires a reasonable definition of a displacement-response spectrum. Although ground motions are known to be significantly affected by the resonant-like amplification behavior caused by multiple wave reflections within the surface soil, such a soil-resonance effect is seldom explicitly considered in current-displacement spectral models. In this study, an analytical approach is developed for the construction of displacement-response spectra by considering the soil-resonance effect. For this purpose, a simple and rational equation is proposed for the response spectral ratio at the site fundamental period (SRTg) to represent the soil-resonance effect based on wave multiple reflection theory. In addition, a bilinear model is adopted to construct the soil displacement-response spectra. The proposed model is verified by comparing its results with those obtained from actual observations and SHAKE analyses. The results show that the proposed model can lead to very good estimations of SRTg for harmonic incident seismic waves and lead to reasonable estimations of SRTg and soil displacement-response spectra for earthquakes with a relatively large magnitude, which are generally considered for seismic design, particularly in high-seismicity regions.

Corrosion and Photo-Reflection Behavior of Aluminum and Stainless Steel During Immersion Test in Salt Solution (3 wt% NaCl 수용액에서 알루미늄과 스테인리스강의 부식에 따른 광 반사 거동)

  • Cho, Soo Yeon;Na, Hyeon Gyu;Cho, Hye Ri;Moon, Jong Ju;Ahn, Tae-Jung;Jang, HeeJin
    • Corrosion Science and Technology
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    • v.19 no.3
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    • pp.109-114
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    • 2020
  • The photo-reflectance of aluminum and AISI 304 stainless steel during cyclic immersion test in 3 wt% NaCl solution was examined in this study. Overall, corrosion was not recognized by a visual inspection or weight measurement up to 310 h. When evaluated, it was noted that the roughness of the specimens did not change significantly. However, localized corrosion, which is located at the vicinity of intermetallic precipitation of aluminum or at the grain boundary of stainless steel, was confirmed by the use of an optical microscope and scanning electron microscopy after tens of hours of utilizing the corrosion test. In this respect, an increase of the peak intensity for metallic Al after 90 h of test, and for metallic Fe after 153 h was detected from the X-ray photoelectron spectra. In this context, it was shown that from the photo-reflectance spectra, the reflection of the visible light from the tested samples was changed noticeably over the test duration. As a result, the intensity of reflected light was decreased up to 90 h ~ 153 h, and thereafter was shown to increase higher than the initial intensity before the corrosion test.

Optical Characterization of Sensory Rhodopsin II Thin Films using a Near-field Scanning Microwave Microscope (근접장 마이크로파 현미경을 이용한 로돕신의 광학적 특성 연구)

  • Yu, Kyung-Son;Kim, Song-Hui;Yoon, Young-Woon;Lee, Kie-Jin;Lee, Jung-Ha;Choi, Ah-Reum;Jung, Kwang-Hwan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.1
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    • pp.80-85
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    • 2007
  • We report the electro-optical properties of the sensory rhodopsin II using a near-field scanning microwave microscope(NSMM). Rhodopsin was known as a photoreceptor pigment with a retinal as a chromophore via a protonated Schiff base and consists of seven ${\alpha}-helical$ transmembrane segments. The sensory rhodopsin II, expressing E. coli UT5600 with endogenous retinal biosynthesis system and purified with $Ni^{-2}-NTA$ affinity chromatography in the presence of 0.02 % DM (Dodecyl Maltoside) from Natronomonas pharaonis. We measured the absorption spectra and the transients difference of sensory rhodopsin II from Natronomonas pharaonis using a UV/VIS spectrophotometer with Nd-Yag Laser (532 nm). The absorption spectra of NpSR II showed a typical rhodopsin spectrum with a left shoulder region and the photointermediates spectra of NpSR II-ground state (${\lambda}max=498\;nm$), NpSR II-M state (${\lambda}max=390\;nm$), and NpSR II-O state (${\lambda}max=550\;nm$) during the photocycle. The observed photocycle reaction was confirmed by measuring the microwave reflection coefficient $S_{11}$ at an operating frequency of f=3.93-3.95 GHz and compared with the results of a photocycle of NpSR II.

Electromagnetic wave absorption characteristics in Ni-Mn-Zn Ferrite with varying Mn content and applied magnetic field (Ni-Mn-Zn ferrite의 합성과 Mn의 치환량 및 인가자장에 따른 전자기파 흡수 특성 연구)

  • Ji-Hye Lee;Sang-Min Lee;Young-Min Kang
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.33 no.6
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    • pp.294-302
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    • 2023
  • Ni-Mn-Zn ferrite, Ni0.5-xMnxZn0.5Fe2O4 (0 ≤ x ≤ 0.5), was synthesized using the sol-gel method to investigate the crystal structure, microstructure, magnetic properties, high-frequency characteristics, and electromagnetic (EM) wave absorption characteristics as a function of Mn substitution. As the Mn content increased, a continuous decrease in saturation magnetization (MS) was observed with little change in coercivity (HC). Samples for each composition (x) exhibited strong EM wave absorption performance with first and second strong EM wave absorption regions satisfying minimum reflection loss, RLmin < -40 dB in the 1.5~2.5, 6~11 GHz range, respectively. The EM wave absorption in Ni-Mn-Zn ferrite depends on magnetic loss, and adjusting µ' and µ'' spectra by Mn substitution or H field allows control of the EM wave absorption frequency.

Conductivity of copper(II)-phthalocyanine thin films due to a grain growth (결정 성장 조건에 따른 copper(II)-phthalocyanine 박막의 전기전도도 특성)

  • Park, Mie-Hwa;Yoo, Hyun-Jun;Lee, Kie-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.05a
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    • pp.132-136
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    • 2004
  • 열 증착 방법을 이용하여 copper(II)-phthalocyanine(CuPc) 박막을 glass 기판 위에 제작하였다. 열처리 조건은 $150^{\circ}C$에서 후열(annealing) 처리 하는 방식과 예열하는 두 가지 방식으로 달리하였다. 제작된 박막의 전기전도도를 평가하기 위해 마이크로웨이브 근접장 효과를 이용한 근접장 현미경(near-field scanning microwave microscope)을 이용하여 비파괴적인 방식으로 CuPc 박막의 반사계수(reflection coefficient)를 측정하였다. CuPc 박막의 전기전도도 특성을 UV 흡수도를 통한 에너지 밴드갭의 shift 현상과 관련지어 설명하고 또한 x-ray diffraction(XRD) data를 통해 박막의 결정 특성과 비교하였다. 박막 표면 특성은 SEM(scanning microscope microscopy)을 통해 관측하였다. 열처리 조건에 따른 CuPc 박막의 전기전도도 특성은 후열 처리한 박막의 경우 예열 처리한 박막보다 전기 전도 특성이 향상되었음을 관측할 수 있었다.

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