• Title/Summary/Keyword: Rapid Heating

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Rapid Synthesis and Sintering of Nanostructured MgTiO3 Compound by High-Frequency Induction Heating (고주파 유도 가열에 의한 급속 나노구조 MgTiO3 화합물 합성 및 소결)

  • Kang, Hyun-Su;Doh, Jung-Mann;Yoon, Jin-Kook;Park, Bang-Ju;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.50 no.12
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    • pp.891-896
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    • 2012
  • Nanopowders of MgO and $TiO_2$ were made by high energy ball milling. The rapid synthesis and sintering of the nanostructured $MgTiO_3$ compound was investigated by the high-frequency induction heated sintering process. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition grain growth. Nanocrystalline materials have received much attention as advanced engineering materials with improved physical and mechanical properties. As nanomaterials possess high strength, high hardness, excellent ductility and toughness, undoubtedly, more attention has been paid for the application of nanomaterials. A highly dense nanostructured $MgTiO_3$ compound was produced with simultaneous application of 80 MPa pressure and induced current within 2 min. The sintering behavior, gain size and mechanical properties of $MgTiO_3$ compound were investigated.

Rapid Sintering and Synthesis of Nanostuctured FeCrAlSi-Al2O3 Composite by High-Frequency Induction Heating (고주파유도 가열에 의한 나노구조의 FeCrAlSi-Al2O3 복합재료의 합성 및 급속소결)

  • Du, Song Lee;Cho, Sung-Hun;Ko, In-Yong;Doh, Jung-Mann;Yoon, Jin-Kook;Park, Sang-Whan;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.49 no.3
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    • pp.231-236
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    • 2011
  • Nanopowder of $Fe_2O_3$, Al, Cr and Si was fabricated by high energy ball milling. A dense nanostuctured $A_2O_3$ and $6.06Fe_{0.33}Cr_{0.16}Al_{0.23}Si_{0.29}$ composite was simultaneously synthesized and consolidated using high frequency induction heated sintering method within 1 minute from mechanically activated powders of $Fe_2O_3$, Al, Cr and Si. The grain sizes of $Al_2O_3$ and $Fe_{0.33}Cr_{0.16}Al_{0.23}Si_{0.29}$ in composite are 80 and 18 nm, respectively.

A Rapid and Universal Direct PCR Method for Macrofungi

  • Park, Mi-Jeong;Lee, Hyorim;Ryoo, Rhim;Jang, Yeongseon;Ka, Kang-Hyeon
    • The Korean Journal of Mycology
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    • v.49 no.4
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    • pp.455-467
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    • 2021
  • Macrofungi are valuable resources as novel drug candidates, new biomaterials, and edible materials. Recently, genetic approaches pertaining to macrofungi have been continuously growing for their identification, molecular breeding, and genetic engineering. However, purification and amplification of fungal DNA is challenging because of the rigid cell wall and presence of PCR inhibitory metabolites. Here, we established a direct PCR method to provide a rapid and efficient method for PCR-grade macrofungal DNA preparation applicable to both conventional PCR and real-time PCR. We first optimized the procedure of lysis and PCR using the mycelia of Lentinula edodes, one of the most widely consumed macrofungal species. Lysates prepared by neutralizing with (NH4)2SO4 after heating the mycelia in a mixture of TE buffer and KOH at 65℃ for 10 min showed successful amplification in both conventional and real-time PCR. Moreover, the addition of bovine serum albumin to the PCR mixture enhanced the amplification in conventional PCR. Using this method, we successfully amplified not only internal transcribed spacer fragments but also low-copy genes ranging in length from 500 to 3,000 bp. Next, we applied this method to 62 different species (54 genera) of macrofungi, including edible mushrooms, such as Pleurotus ostreatus, and medicinal mushrooms such as Cordyceps militaris. It was found that our method is widely applicable to both ascomycetes and basidiomycetes. We expect that our method will contribute to accelerating PCR-based approaches, such as molecular identification, DNA marker typing, gene cloning, and transformant screening, in macrofungal studies.

Microwave hybrid sintering of NTC themistor (마이크로파 하이브리드 소결법에 의한 NTC 서미스터의 제조)

  • 최영락;안진용;안주삼;백동규;최승철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.3
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    • pp.508-512
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    • 1998
  • The NTC thermistors were sintered by using microwave hybrid heating method at $1100^{\circ}C$~$1300^{\circ}C$ and those electrical properties were investigated. The obtained $B_{25^{\circ}C/85^{\circ}C}$ values from temperature dependence of electrical resisitivity were around 3100~3200 K which were almost the same values as conventionally sintered ones. Compared with conventional sintering process, this process could complete whole sintering process within 20 minutes. This the processing time and energy consumption could be reduced through this rapid heating by using microwave hybrid heating.t there were showed only two peaks, glycolide melting peak and lower molecular weight melting peak without lauryl alcohol. Conversion increased slowly with the reaction time up to 50 minutes, and then gave a sudden increase above that. The reaction time to disappear in glycolide melting peak during polymerization was shortened with the increase of lauryl alcohol content. Zero-shear viscosity of polyglycolic acid decreased with the increase of free acid content in glycolide.ssional energy and bending hysteresis increased. \circled3 Surface characteristics such as friction coefficient and thickness variation of highly shrinkage fabrics became relatively roughened state. \circled4 Since stiffened and roughened characteristics of highly shrinkage fabrics, drapabilities of them were significantly lowered. Additionally thermal insulation property of high shrinkage fabric was higher than that of low shrinkage fabric due to bulky and thickened feature. From the results, it is considered that the silk fabrics with high filling shrinkage have the good bulkiness and heat keeping properties and thus they have the suitable characteristics for high quality men's and women's formal garments.

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The development of ultra high-speed metal film deposition system and process technology for a heat sink in digital devices (디지털 소자용 방열판 제작을 위한 초고속 금속필름 증착장치 및 공정기술 개발)

  • Yoon, Hyo Eun;Ahn, Seong Joon;Han, Dong Hwan;Ahn, Seungjoon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.7
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    • pp.17-25
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    • 2017
  • To resolve the problem of the temperature rise in LED or OLED lighting, until now a thick metal film has been used as a heat-sink. Conventionally, this thick metal film is made by the electroplating method and used as the heat-dissipating plate of the electronic devices. However, nowadays there is increasing need for a Cu metal film with a thickness of several hundred micrometers that can be formed by the dry deposition method. In this work, we designed and fabricated a Cu film deposition system where the heating element is separated from the ceramic crucible, which makes ultra-rapid deposition possible by preventing heat loss. In addition, the resulting induction heating also contributes to the high deposition rate. By tuning the various parameters, we obtained a $100-{\mu}m$ thick Cu film whose heat conductivity is high and whose thickness uniformity is better than 2%, while the deposition rate is as high as $1000{\AA}/s$.

플라즈마 도핑 후 급속열처리법을 이용한 n+/p 얕은 접합 형성

  • Do, Seung-U;Seo, Yeong-Ho;Lee, Jae-Seong;Lee, Yong-Hyeon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.50-50
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    • 2009
  • In this paper, the plasma doping is performed on p-type wafers using $PH_3$ gas(10 %) diluted with He gas(90 %). The wafer is placed in the plasma generated with 200 W and a negative DC bias (1 kV) is applied to the substrate for 60 sec under no substrate heating. the flow rate of the diluted $PH_3$ gas and the process pressure are 100 sccm and 10 mTorr, respectively. In order to diffuse and activate the dopant, annealing process such as rapid thermal annealing (RTA) is performed. RTA process is performed either in $N_2$, $O_2$ or $O_2+N_2$ ambient at $900{\sim}950^{\circ}C$ for 10 sec. The sheet resistance is measured using four point probe. The shallow n+/p doping profiles are investigated using secondary ion mass spectromtry (SIMS). The analysis of crystalline defect is also done using transmission electron microscopy (TEM) and double crystal X-ray diffraction (DXRD).

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Heat-Generating Behavior of SiC Fiber Mat Composites Embedded with Ceramic Powder for Heat Conservation

  • Joo, Young Jun;Cho, Kwang Youn
    • Journal of the Korean Ceramic Society
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    • v.56 no.6
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    • pp.583-588
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    • 2019
  • Silicon carbide (SiC) fiber mats generate large amounts of heat through microwave interactions and are used as heating elements in rapid heat treatment furnaces. However, SiC fibers cool immediately when the microwave power is turned off. Therefore, ceramic layers are inserted between the SiC fiber layers to improve the heat conservation performance of SiC fiber mats. In this study, we fabricated SiC fiber mat composites (SMCs) with ceramic layers under various pressures. The SMC fabricated under 0.007 kPa showed the lowest heat-generating temperature and deviation because less necking was observed between the materials. On the other hand, the SMC fabricated under 0.375 kPa showed the highest heat-generating temperature of 1532.33℃. The SMCs prepared in this study using ceramic powder not only showed heat-generating temperatures comparable to those of conventional SiC fiber mats but also exhibited excellent heat-preserving ability.

A Study on System for Real-time Measurement of Welding Distortion (실시간 용접변형 계측을 위한 시스템에 관한 연구)

  • Jeong, Jae-Won;Kim, Ill-Soo;Kim, In-Ju;Son, Sung-Woo;Shim, Ji-Yeon
    • Journal of Welding and Joining
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    • v.27 no.5
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    • pp.62-67
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    • 2009
  • Welding deformation during the assembly process is affected by not only local shrinkage due to rapid heating and cooling, but also root gap and misalignment between parts to be welded. Therefore, the prediction and control of welding deformation have become of critical importance. In this study, it was focused on the development of the 3-axis apparatus for real-time measurement of the welded deformation. To achieve the objective, a D-H algorithm has been carried out to check the behavioral and performance evaluation for the developed robot. The sequence experiments were taken the base materials of $400{\times}200{\times}4.5mm$ plate for butt welding. The real-time experimental measurements are in good agreement with the measured results.

SI Engine Hydrocarbon Emissions Reduction with Secondary Air Injection and Coolant Control (2차 공기분사 및 냉각수제어에 의한 SI 엔진의 탄화수소 배기저감)

  • 박기수;조영진;박심수
    • Transactions of the Korean Society of Automotive Engineers
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    • v.8 no.4
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    • pp.51-58
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    • 2000
  • It is well known that the majority of the emissions measured from vehicle exhaust in the US Federal Test Procedure(FTP-75) are emitted during the first 60 seconds. This paper describes an experimental study on SI engine emissions reduction after cold start with interval secondary air injection and coolant control. Secondary air injection after cold start to reduce exhaust emissions causes an exothermic reaction at the exhaust port and gives sufficient air to the catalyst. For that reason engine-out emissions oxidized in the exhaust port and the rapid heating of a catalytic converter after cold start with CSAI and ISAI are estimated. The influence of the coolant temperature on SI engine emissions has been estimated. In the present studycoolant control of the cylinder head tempeature is used to investigate the effect of coolant temperature on SI engine emissions. The results show that engine-out hydrocarbon and carbon monoxide emissions are considerably reduced with interval secondary air injection and coolant control.

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Mechanical Synthesis and Rapid Consolidation of Nanostructured W-Al2O3 Composite

  • Lee, BooRak;Jeong, GeolChae;Park, GeunO;Shon, In-Jin
    • Korean Journal of Materials Research
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    • v.28 no.6
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    • pp.343-348
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    • 2018
  • Recently, the properties of nanostructured materials as advanced engineering materials have received great attention. These properties include fracture toughness and a high degree of hardness. To hinder grain growth during sintering, it is necessary to fabricate nanostructured materials. In this respect, a high-frequency induction-heated sintering method has been presented as an effective technique for making nanostructured materials at a lower temperature in a very short heating period. Nanopowders of W and $Al_2O_3$ are synthesized from $WO_3$ and Al powders during high-energy ball milling. Highly dense nanostructured $W-Al_2O_3$ composites are made within three minutes by high-frequency induction-heated sintering method and materials are evaluated in terms of hardness, fracture toughness, and microstructure. The hardness and fracture toughness of the composite are $1364kg/mm^2$ and $7.1MPa{\cdot}m^{1/2}$, respectively. Fracture toughness of nanostructured $W-Al_2O_3$ is higher than that of monolithic $Al_2O_3$. The hardness of this composite is higher than that of monolithic W.