• Title/Summary/Keyword: RSD

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FASTSOUND: PROBING THE ORIGIN OF COSMIC ACCELERATION BY GALAXY CLUSTERING AT z ~ 1.3 WITH SUBARU/FMOS

  • TOTANI, TOMONORI
    • Publications of The Korean Astronomical Society
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    • v.30 no.2
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    • pp.367-369
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    • 2015
  • The FastSound project is a galaxy redshift survey using Subaru/FMOS to detect $H{\alpha}$ emitting galaxies at z ~ 1:3, for the purpose of probing the origin of the accelerated expansion of the universe. The survey has detected ~4,000 galaxy redshifts in a total area of $30deg^2$, and detected the redshift space distortion at this redshift range for the first time. The redshift space distortion (RSD) signal will be used to derive a measurement of the growth rate of large scale structure, which will provide a test for modified gravity as a possible origin of accelerated cosmic explansion. Here we present an overview and the current status of the project.

Development of Web-based Bio-Image Retrieval System (웨이블릿 변환을 이용한 실시간 화재 감지 알고리즘)

  • Cheong, Kwang-Ho;Ko, Byoung-Chul;Nam, Jae-Yeal
    • Annual Conference of KIPS
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    • 2006.11a
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    • pp.227-230
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    • 2006
  • A content-based image retrieval system using MPEG-7 is designed and implemented in this thesis. The implemented system uses existing MPEG-7 Visual Descriptors. In addition, a new descriptor for efficient retrieval of bio images is proposed and utilized in the developed content-based image retrieval system. Comparing proposed CBSD(Compact Binary Shape Descriptor) with Edge Histogram Descriptor(EHD) and Region Shape Descriptor(RSD), it shows good retrieval performance in NMRR. The proposed descriptor is robust to large modification of brightness and contrast and especially improved retrieval performance to search images with similar shapes. Also proposed system adopts distributed architecture to solve increased server overload and network delay. Updating module of client efficiently reduces downloading time for metadata. The developed system can efficiently retrieve images without causing server's overload.

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Determination of Histidine by Spectrofluorometry (형광광도법에 의한 Histidine의 정량에 관한 연구)

  • Cha, Ki Won;Huang, Huazi
    • Analytical Science and Technology
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    • v.17 no.2
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    • pp.180-183
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    • 2004
  • A simple and sensitive determination method of histidine has been investigated using the spectrofluorometry. An emission peak of $Eu^{3+}$ - TTA- histidine complex occurs at 470 nm in aquous solution with excitation at 235 nm and the fluorescence intensity increased linearly with addition of histidine in the range of $1{\times}10^{-7}-4{\times}10^{-6}M$. The detection limits was $5{\times}10^{-7}M$ with 3.5% RSD. The present method was applied to determine histidine content in the synthetic sample.

Determination of Cyanide Ion by Adsorptive Stripping Voltammetry (흡착벗김 전압전류법에 의한 시안화이온의 정량)

  • Cha, Ki-Won;Ko, Su-Jin;Kim, Jea-Kyun
    • Analytical Science and Technology
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    • v.14 no.6
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    • pp.540-544
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    • 2001
  • Determination of cyanide ion has been studied by adsorptive stripping voltammetry using hanging mercury electrode. Cyanide ion complexed with copper ion is adsorpbed on the electrode and oxidised at the positive potential scan. Optimal conditions of CN determination were found to be ; supporting electrolyte solution ; 0.1 M NaCl of ammonium buffer at pH 10, accumulation potential; -800 mV vs Ag/AgCl, accumulation time ; 300 s, scan rate ; 50mV/s. The linear concentration of cyanide ion was observed in the range $1{\times}10^{-8}$, $1{\times}10^{-7}M$. The detection limit(n/s=3) was $0.13{\mu}g/L$($5{\times}10^{-9}M$) with 3.5% RSD.

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Dual Capillary Column System for the Qualitative Gas Chromatography: 1. Comparison Between Split and Splitless Injection Modes

  • Kim, Kyoung-Rae;Kim, Jung-Han;Park, Hyoung-Kook;Oh, Chang-Hwan
    • Bulletin of the Korean Chemical Society
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    • v.12 no.1
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    • pp.87-92
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    • 1991
  • A dual capillary column system is described for the simultaneous measurement of retention index (RI) and area ratio (AR) values of each peak on two capillary columns of different polarity, DB-5 & DB-1701. Both capillary columns were connected to a common splitless injector via a deactivated fused-silica capillary tubing of 1 m length and a 'Y' splitter, the dead volume effect of which was found to be negligible. RI and AR were measured with high reproducibility(${\leq}$0.05% RSD) and with high accuracy (<10% RE), respectively. When applied to the test samples of the organic acid mixture, each acid was positively identified by the combined computer RI library search-AR comparison.

Direct Anlysis of Impurities in Solides with Glow Discharge Mass Spectrometry

  • Ki Beom Lee;Dae Won Moon;Kwang Woo Lee
    • Bulletin of the Korean Chemical Society
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    • v.10 no.6
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    • pp.524-529
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    • 1989
  • A glow discharge mass spectrometric(GDMS) analytical method was developed for direct analysis of impurities in solids. Ions extracted from a glow discharge ion source with a sample as a cathode were analyzed by a quadrupole mass filter. Ion extractions were carried out through differentially-pumped orifices biased to positive and negative potentials. Operating parameters of the glow discharge source such as discharge current, orifice-to-cathode distance, energy analyzer setting and bias voltages have been optimized. The developed GDMS was applied to the analysis of KSS copper-base alloy standards certified by Korea Standards Research Institute(KSRI). In the analysis, the reproducibility and the detection limits were estimated to be about 2.5% RSD, and in the low ppm range, respectively.

The Simultaneous Analysis of Benzene, Toluene, Ethylbenzene, o,m,p-Xylenes and Total Petroleum Hydrocarbons in Soil by GC-FID after Ultra-Sonication

  • Sin, Ho Sang;Gwon, O Seung
    • Bulletin of the Korean Chemical Society
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    • v.21 no.11
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    • pp.1101-1105
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    • 2000
  • A simultaneous determination method of BTEX (benzene, toluene, ethylbenzene, o,m.p-xylene) and TPH (kerosene, diesel, jet fuel and bunker C) in soil with gas chromatography/flame ionization detection (GC-FID) was described. The effects of extracti on method, extraction solvent, solvent volume and extraction time on the extraction performance were studied. A sonication method was simpler and more efficient than Soxhlet or shaking methods. Sonication with 10 mL of acetone/methylene chloride (1 : 1, v/v) for 10 min was found to be optimal extraction conditions for 20 g of soil. Peak shapes and quantification of BTEX and TPH were excellent, with linear calibration curves over a wide range of 1-500 mg/L for BTEX and 10-5000 mg/L for TPH. Good reproducibilities by sonication were obtained, with the RSD values below 10%. By using about 20 g of soil, detection limits were 0.8 mg/L for BTEX and 10 mg/L for TPH. The advantages of this procedure are the use of simple and common equipment, reduced volumes of organic solvents, rapid extraction periods of less than 20 min, and simultaneous analysis of volatile and semivolatile compounds.

Diagnostic ex vivo assay of glucose in live cell using voltammetry

  • Ly, Suw Young;Leea, Chang Hyun
    • Journal of the Korean Applied Science and Technology
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    • v.35 no.4
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    • pp.1379-1385
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    • 2018
  • The hand held voltammetry systems searched diabetic assay using glucose sensor of fluorine nafion doped carbon nanotube electrode (FCNE). An inexpensive graphite carbon pencil was used as an Ag/AgCl reference and Pt counter electrode. Upon combining and using three electrode systems, optimum square wave (SW) stripping results were attained to 1.0-9.0 ug/L with 8 points. Statistic RSD precision was of 6.02 % with n=15 in 0.1 mg/L glucose. After a total of 200 second accumulation times, analytical detection limit of 0.8 ug/L was obtained. This developed technique was applied to urine samples from diabetic patients urine for fluid analysis, it was determined that the sensor can be used with a diagnostics in the ex vivo of live cells and non treated biological fluid.

Electrochemical Determination of Capsaicin by Ionic Liquid Composite-Modified Electrode

  • Kim, Dong-Hwan;Nam, Sungju;Kim, Jaeyoon;Lee, Won-Yong
    • Journal of Electrochemical Science and Technology
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    • v.10 no.2
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    • pp.177-184
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    • 2019
  • An electrochemical detection method for capsaicin has been developed using ionic liquid (IL) doped graphene-titania-Nafion composite-modified electrode. The combination of IL (1-hexyl-3-methylimidazolium with hexafluorophosphate counter ion) in the composite-modified electrode resulted in a significantly increased electrochemical response for capsaicin compared to that obtained at the corresponding electrode without IL. The increased electrochemical signal could be ascribed to the decreased electron transfer resistance through the composite film and also to the effective accumulation of capsaicin on the electrode surface due to ${\pi}-{\pi}$ interaction of the imidazole groups of IL with the aromatic rings of capsaicin. The present IL composite-modified electrode can detect capsaicin with a concentration range from $3.0{\times}10^{-8}M$ to $1.0{\times}10^{-5}M$ with a detection limit of $3.17{\times}10^{-9}M$ (S/N = 3). The present sensor showed good reproducibility (RSD = 3.2%).

Dual Capillary Column System for the Qualitative Gas Chromatography: 2. Comparison between Splitless and On-Column Injection Modes

  • Kim, Kyoung-Rae;Kim, Jung-Han;Park, Hyoung-Kook;Oh, Chang-Hwan
    • Bulletin of the Korean Chemical Society
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    • v.14 no.2
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    • pp.250-255
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    • 1993
  • A dual capillary column system is described for the simultaneous analysis of a given sample and measurement of retention index (RI) and area ratio (AR) values of each peak on two capillary columns of different polarity, DB-5 & DB-1701 from a single injection. Both capillary columns were connected to either a splitless injector or an on-column injector via a deactivated fused-silica capillary tubing of 1 m length and a 'Y' splitter. Both injection modes allowed to measure RI and AR values with high reproducibility (<0.01% RSD) and high accuracy (<10% RE), respectively with the exception that the trace and high boiling solutes required the on-column mode for the accurate quantification and AR comparison. When the dual capillary column system in on-column injection mode was applied to the blind samples containing organic acids, each acid was positively indentified by the combined computer RI library search-AR comparison.