• Title/Summary/Keyword: Particle size analysis

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Higher levels of serum triglyceride and dietary carbohydrate intake are associated with smaller LDL particle size in healthy Korean women

  • Kim, Oh-Yoen;Chung, Hye-Kyung;Shin, Min-Jeong
    • Nutrition Research and Practice
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    • v.6 no.2
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    • pp.120-125
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    • 2012
  • The aim of this study was to investigate the influencing factors that characterize low density lipoprotein (LDL) phenotype and the levels of LDL particle size in healthy Korean women. In 57 healthy Korean women (mean age, $57.4{\pm}13.1$ yrs), anthropometric and biochemical parameters such as lipid profiles and LDL particle size were measured. Dietary intake was estimated by a developed semi-quantitative food frequency questionnaire. The study subjects were divided into two groups: LDL phenotype A (mean size: $269.7{\AA}$, n = 44) and LDL phenotype B (mean size: $248.2{\AA}$, n = 13). Basic characteristics were not significantly different between the two groups. The phenotype B group had a higher body mass index, higher serum levels of triglyceride, total-cholesterol, LDL-cholesterol, apolipoprotein (apo)B, and apoCIII but lower levels of high density lipoprotein (HDL)-cholesterol and LDL particle size than those of the phenotype A group. LDL particle size was negatively correlated with serum levels of triglyceride (r = -0.732, $P$ < 0.001), total-cholesterol, apoB, and apoCIII, as well as carbohydrate intake (%En) and positively correlated with serum levels of HDL-cholesterol and ApoA1 and fat intake (%En). A stepwise multiple linear regression analysis revealed that carbohydrate intake (%En) and serum triglyceride levels were the primary factors influencing LDL particle size ($P$ < 0.001, $R^2$ = 0.577). This result confirmed that LDL particle size was closely correlated with circulating triglycerides and demonstrated that particle size is significantly associated with dietary carbohydrate in Korean women.

Effects of feed form and feed particle size with dietary L-threonine supplementation on performance, carcass characteristics and blood biochemical parameters of broiler chickens

  • Rezaeipour, Vahid;Gazani, Sepideh
    • Journal of Animal Science and Technology
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    • v.56 no.5
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    • pp.20.1-20.5
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    • 2014
  • An experiment was conducted to evaluate the effect of form and particle size of feed supplemented with L-threonine on growth performance, carcass characteristic and blood biochemical parameters of broiler chickens. The experimental design was a $2{\times}2{\times}2$ factorial arrangement of treatments evaluating two feed forms (pellet or mash), two feed particle sizes (fine or course), and two inclusion rates of dietary L-threonine (with or without) which adopted from 7 to 42 days of age. In this experiment, 360 a day old chicks in two sexes were assigned in each treatment and each experimental unit was included 15 chicks. Feed consumption and weight gain were measured weekly. At 35 days of age, blood samples were taken to analysis blood biochemical parameters. At the end of the experimental period, two birds were slaughtered in each treatment and carcass analysis was carried out. The results showed that the effect of feed form on body weight gain and feed intake in whole of experimental period was significant (P < 0.05). Broilers fed pelleted diets had more weight gain than the mash group. Growth performance parameters were not affected by feed particle size and dietary L-threonine supplementation in whole of experimental period (P > 0.05). The results of carcass analysis showed that liver and gizzard relative weights were influenced by feed form (P < 0.05). However, pancreas and liver relative weights were affected by feed particle size and dietary L-threonine supplementation, respectively (P < 0.05). Triglyceride and VLDL levels were affected by feed form and dietary L-threonine supplementation (P < 0.05). The effect of feed particle size on blood biochemical parameters was not significant (P > 0.05). In conclusion, the experimental results indicated that feed form increased feed consumption and weight gain in whole of experimental period (1 to 42 days of age) while feed particle size and dietary L-threonine had no effect on broiler performance.

Analysis of Solids in Runoff to Prevent Solids Pollution (오염저감 기법개발을 위한 유출수내 고형물질 특성 규명)

  • Lee, Young-Soo
    • Journal of Korean Society of Water and Wastewater
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    • v.18 no.1
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    • pp.22-28
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    • 2004
  • The fate and transport mechanism of pollutants which have affinities to particles, such as trace metals and some petroleum product based compounds, can be effectively explained by the movement of sediment. The sediment release from lands to adjacent water bodies due to rainfall events was investigated in an effort to predict the total suspended solids (TSS) concentrations in runoff. The contribution of sediment from land origin to the river TSS can be better understood by the relationship between TSS concentration and particle size in runoff. The sieve analysis was used to determine the particle size distribution and these results were incorporated into statistical models. The critical size of particles was set to $74{\mu}m$ which contributes to the river TSS concentration since fine particles (wash load) of the sediment in the runoff play the key role in constituting TSS in a water column of the river. Empirical relationships were developed to predict TSS in runoff from the percentage of the critical particle size and were proven statistically to be valid.

Development of Light Transmission Fluctuation for Particle Measurement in Solid-Gas Two Phase Flows

  • YANG, Bin;WANG, Zhan-ping;HE, Yuan;CAI, Xiao-Shu
    • Particle and aerosol research
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    • v.12 no.1
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    • pp.21-26
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    • 2016
  • In order to realize In-line and convenient measurement for solid-gas two phase flows, Light Transmission Fluctuation (LTF) based on the random variation of transmitted light intensity, light scattering theory and cross-correlation method was presented for online measurement of particle size, concentration and velocity. The statistical relationship among transmitted light intensity, particle size and particle number in measurement zone was described by Beer-Lambert Law. Accordingly, the particle size and concentration were determined from the fluctuation signal of transmitted light intensity. Simultaneously, the particle velocity was calculated by cross-correlation analysis of two neighboring light beams. By considering the influence of concentration variation in industrial applications, the improved algorithm based on spectral analysis of transmitted light intensity was proposed to improve measurement accuracy and stability. Therefore, the online measurement system based on LTF was developed and applied to measure pulverized coal in power station and raw material in cement plant. The particle size, concentration and velocity of powder were monitored in real-time. It can provide important references for optimal control, energy saving and emission reduction of energy-intensive industries.

Strength Analysis of Particle-Reinforced Aluminum Composites with Length-Scale Effect based on Geometrically Necessary Dislocations (기하적 필수 전위에 의한 길이효과를 고려한 입자 강화 알루미늄 복합재의 강도해석)

  • Sub, Y.S.;Kim, Y.B.;Rhee, Z.K.
    • Transactions of Materials Processing
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    • v.18 no.6
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    • pp.482-487
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    • 2009
  • A finite element based microstructural modeling for the size dependent strengthening of particle reinforced aluminum composites is presented. The model accounts explicitly for the enhanced strength in a discretely defined "punched zone" around the particle in an aluminum matrix composite as a result of geometrically necessary dislocations developed through a CTE mismatch. The density of geometrically necessary dislocations is calculated considering volume fraction of the particle. Results show that predicted flow stresses with different particle size are in good agreement with experiments. It is also shown that 0.2% offset yield stresses increases with smaller particles and larger volume fractions and this length-scale effect on the enhanced strength can be observed by explicitly including GND region around the particle. The strengths predicted with the inclusion of volume fraction in the density equation are slightly lower than those without.

Effect of Grinding Methods on Particle Size and Crystalline Structure of Copper Phthalocyanine (분쇄방법에 따른 구리프탈로시아닌 입자크기 및 결정구조 변화)

  • Lee, Jeong Se;Lee, Hak Sung
    • Applied Chemistry for Engineering
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    • v.18 no.1
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    • pp.41-47
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    • 2007
  • Crude copper phthalocyanine (Cupc) was synthesized by Wyler process, then grounded using various methods such as acid pasting, kneader, attritor and SC-mill. Particle size, shape and crystalline structure were compared and evaluated after particle size reductions. Cupcs prepared by acid pasting and kneader methods that are excellent manufacturing processes in industry were used as our standards. Particle properties of Cupcs prepared either by attritor or by SC-mill were compared with particle size analyzer, scanning electron microscopy (SEM) and X-ray diffraction (XRD). Particle size analyzer and SEM were used to analyze the variation of particle sizes of Cupc with milling time. Particle size was initially decreased up to the 90 min of milling time, thereafter it reversely began to increase in case of SC-mill. Cupc obtained from dry milling with attritor displayed strong cohesion so that particle size was not possible to determine with particle size analyzer. However, the optimum milling time was indirectly approximated from the analysis of XRD peak intensity.

Synthesis of scheelite-type nanocolloidal particles by pulsed laser ablation in liquid and their size distribution analysis

  • Lee, Jung-Il;Shim, Kwang Bo;Ryu, Jeong Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.3
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    • pp.111-119
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    • 2014
  • A novel pulsed laser ablation process in liquid was investigated to prepare scheelite-type ceramic [calcium tungstate ($CaWO_4$) and calcium molybdate ($CaMoO_4$)] nanocolloidal particles. The crystalline phase, particle morphology, particle size distribution, absorbance and optical band-gap were investigated. Stable colloidal suspensions consisting of well-dispersed $CaWO_4$ and $CaMoO_4$ nanoparticles with narrow size distribution could be obtained without any surfactant. Particle tracking analysis using optical microscope combined with image analysis was applied for a fast determination of particle size distribution in the prepared nanocolloidal suspensions. The mean nanoparticle size of $CaWO_4$ and $CaMoO_4$ colloidal nanoparticles were 16 nm and 30 nm, with the standard deviations of 2.1 and 5.2 nm, respectively. The optical absorption edges showed blue-shifted values about 60~70 nm than those of reported in bulk crystals. And also, the estimated optical energy band-gaps of $CaWO_4$ and $CaMoO_4$ colloidal particles were 5.2 and 4.7 eV. The observed band-gap widening and blue-shift of the optical absorbance could be ascribed to the quantum confinement effect due to the very small size of the $CaWO_4$ and $CaMoO_4$ nanocolloidal particles prepared by pulsed laser ablation in liquid.

Using oscillatory shear to probe the effects of bidispersity in inverse ferrofluids

  • Ekwebelam, C.C.;See, H.
    • Korea-Australia Rheology Journal
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    • v.19 no.1
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    • pp.35-42
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    • 2007
  • The effects of particle size distribution on the magnetorheological response of inverse ferrofluids was investigated using controlled mixtures of two monodisperse non-magnetisable powders of sizes $4.6\;{\mu}m\;and\;80{\mu}m$ at constant volume fraction of 30%, subjected to large amplitude oscillatory shear flow. In the linear viscoelastic regime (pre-yield region), it was found that the storage and loss moduli were dependent on the particle size as well as the proportion of small particles, with the highest storage modulus occurring for the monodisperse small particles. In the nonlinear regime (post yield region), Fourier analysis was used to compare the behaviour of the $1^{st}\;and\;3^{rd}$ harmonics ($I_{1}\;and\;I_{3}\;respectively$) as well as the fundamental phase angle as functions of the applied strain amplitude. The ratio of $I_{3}/I_{1}$ was found to become more pronounced with decreasing particle size as well as with increasing proportion of small particles in the bidisperse mixtures. Furthermore, the phase angle was able to clearly show the transition from solid-like to viscous behaviour. The results suggested that the nonlinear response of a bidisperse IFF is dependent on particle size as well as the proportion of small particles in the system.

Quality Characteristics of Korean Red Ginseng Powder with Different Milling Methods (분쇄방법에 따른 고려홍삼분말의 품질특성)

  • 서창훈;이종원;도재호;김나미;양재원;장규원
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.3
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    • pp.370-374
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    • 2003
  • Cell cracking method using a non-collision was evaluated for the possibility of new red ginseng grinding technique. Based on particle size distribution analysis by 1size shaker, the ratios of 100 mesh penetrated particles were 94.9% for hammer mill (group A) and 95.6% for cell crack (group B). The ratio of 120 mesh penetrated particle of group A was higher than that in group B. The particle size distributions for 100 mesh non-penetrated Powder between 2 groups were not significantly different, and particle size distribution analysis by laser scattering analyzer showed that the particle size ranges were 0.77~128.07 ${\mu}{\textrm}{m}$ for group A and 4.24~180.07 ${\mu}{\textrm}{m}$ for group B. The Particle size distribution in group A was more broad than that in group B. The mean particle size in group B was larger than that in group A, while the standard deviation of particle size distribution in group B was less than that in group A. Structural surface characteristics, in group A, particle size distribution was broad and the distribution curve was amorphous. The structure of individual particles was similar to unequal stone which was roughly grinded and had soft cotton-like surface. In the contrary, in group B, particle size distribution was relatively narrow and also individual size particles were ubiquitously distributed. The structure of individual particles was unequal cut stone shape.

Particle Size and Reaction Temperature Effects on the Hydrolysis Reaction of Zinc in TGA (Thermo Gravimetric Analyzer) (열 중량 분석기에서 zinc 입자 크기와 반응 온도에 따른 물 분해 특성 연구)

  • Ahn, Seung-Hyuck;Kang, Kyoung-Soo;Kim, Chang-Hee;Bae, Ki-Kwang;Kim, Young-Ho;Park, Chu-Sik
    • Journal of Hydrogen and New Energy
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    • v.19 no.4
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    • pp.305-312
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    • 2008
  • ZnO/Zn redox cycle is the one of the promising thermochemical cycles for hydrogen production via water splitting with high temperature heat source like a concentrated solar energy. This paper reports the particle size effect of Zinc on water splitting behavior. Water splitting reaction experiments were carried out at isothermal conditions of 350 and 400$^{\circ}C$ in TGA (Thermo Gravimetric Analyzer) using four commercial Zinc powders (nano, <10 ${\mu}m$, <150 ${\mu}m$ and $150{\sim}600\;{\mu}m$ particle sizes). Before the experiments, average particle size of Zinc powders was analyzed by PSA (Particle Size Analysis). After the experiments, XRD (X-Ray Diffraction) and SEM (Scanning Electron Microscope) analyses were conducted on the samples. The experimental results showed that particle size had a effect on the conversion of Zinc to ZnO. Zinc conversion was increased, as the particle size decreased. Especially, the nano size particles were aggregated and the particle's morphology changed on the surface during hydrolysis reaction.