• 제목/요약/키워드: Official Method

검색결과 532건 처리시간 0.026초

Toxkits에 의한 물벼룩 급성독성시험방법의 제도적용 적합성 평가 (Evaluation of Alternative Acute Toxicity Test Method with Daphnia magna)

  • 김종민;신기식;이정서;이택준
    • 한국물환경학회지
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    • 제33권2호
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    • pp.181-186
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    • 2017
  • This paper aimed to evaluate the results of alternative acute toxicity test on 83 wastewater samples. Each sample was tested by traditional method (using laboratory cultured D. magna as a test organism) and alternative method (using Toxikit which can be purchased from a specialized company). The relationship between Lab. culture toxicity and Toxkits toxicity indicated good relation ($r^2=0.84$, p<0.01, n = 83). Number of samples which showed a small difference of lower than 0.5 between two test methods were 52 and they account for 63 percent of collected samples. In addition, these 52 samples had a lower average toxicity of TU 0.5 (Lab. culture method) and TU 0.45 (Toxkits method). Whereas samples which indicated big difference of test results between two methods, had a tendency to show higher toxicity. From these results, alternative toxicity test method could be applied to the official test method, if samples would have a lower toxicity less than TU 2. Also, Toxikit standard toxicant test results indicated $EC_{50}$ values between 0.93 and 1.68 mg/L and these results were considered as valid for quality control standard.

New Method for Simultaneous Quantification of 12 Ginsenosides in Red Ginseng Powder and Extract: In-house Method Validation

  • In, Gyo;Ahn, Nam-Geun;Bae, Bong-Seok;Han, Sung-Tai;Noh, Kil-Bong;Kim, Cheon-Suk
    • Journal of Ginseng Research
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    • 제36권2호
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    • pp.205-210
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    • 2012
  • For quality control of components in Korean red ginseng powder and extract, a new method for simultaneous quantification of 12 ginsenosides ($Rg_1$, Re, Rf, $Rh_1$, $Rg_2$[S], $Rg_2$[R], $Rb_1$, Rc, $Rb_2$, Rd, $Rg_3$[S], and $Rg_3$[R]) was studied. Compared to the official method for quantification of marker substances (ginsenosides $Rg_1$ and $Rb_1$), the proposed methods were guaranteed by in-house method validation. Several criteria such as linearity, specificity, precision and accuracy were evaluated. For red ginseng powder, recovery (averaging 95% to 105%) was calculated, and analysis of variance was carried out to estimate the relative standard deviation (0.20% to 2.12%). For red ginseng extract, the average recovery rate was 90% to 99% and the relative standard deviation was 0.39% to 2.40%. These results indicate that the proposed method could be used in the laboratory for determination of 12 ginsenosides in red ginseng powder and extract. In addition, this method was found to be suitable for quality control of ginseng products and potentially offer time and cost benefits.

일본 전통 도시형주택의 재생 및 보전방안에 관한 연구 : 교마치야를 중심으로 (Study on Regeneration and Utilization Method of Japanese Traditional Urban Housing : The Case Study of Kyo-Machiya)

  • 김도연;오혜경
    • 가정과삶의질연구
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    • 제27권3호
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    • pp.1-13
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    • 2009
  • The importance of the historical sites in cities has risen, and therefore this study was performed to find the methods to feasibly manage such sites. In line with the purpose, this study analytically reviews Japan's Kyo-machiya Restoration Policy, which has been systematically carried out under civil-official cooperation, and related policies. For reference, Kyo-machiya is the Kyoto-style wooden house. The results are derived as in the following. First of all, Kyo-machiya Restoration Policy was focused not only on traditional wooden houses but on residents and other buildings as well, and carried out under the cooperation among residents, the administrative office and enterprises. Kyoto citizens established their own ordinances that are suitable to each area so that historical sites may be managed in accordance with city planning. Also, the think tank actively participated in the establishment of municipal ordinances. Lastly, the policy was behind local residents and civic organizations so that they would continuously pay respect to historic sites in cities.

통신위성 이용 멀티채널 양방향 시각비교 연구 (Multi-channel Two-Way Time Transfer Using a Communication Satellite)

  • 양성훈;이창북;이종구;이영규;이상정
    • 제어로봇시스템학회논문지
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    • 제15권3호
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    • pp.346-352
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    • 2009
  • UTC (Coordinated Universal Time) has been made by the comparison results and the statistical analysis of primary clocks maintained by national standard institutes. Some kinds of technique have been used for international time transfer; since 1980s the study on methods and development of time transfer has conducted with activation of GPS application. And the more accurate and easier method made it use the official time transfer method for the generation of UTC. But recently TWSTFT (Two-Way Satellite Time and Frequency Transfers) as well as GPS time transfer are increasing in number because the TWSTFT is able to improve the accuracy and precision of time comparison owing to the elimination of the ionospheric and tropospheric delay errors thanks to the reciprocal propagation path. In this paper, we introduce the TWSTFT results by a multi-channel modem comparing with GPS P3-code.

Demographic Trends and the Methods of their Regulation in the Republic of Kazakhstan

  • Nurlanova, Nailya K.;Meldakhanova, Marziya K.
    • The Journal of Asian Finance, Economics and Business
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    • 제2권3호
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    • pp.23-32
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    • 2015
  • The aim of this work is to study the specifics of demographic processes in the Republic of Kazakhstan and to justify proposals concerning improvement of tendencies and methods of realizations of demographic policy in the country. The following methods have been used in this study: the principles of system approach; methods of statistical and comparative economic analysis, sociological analysis; method of expert evaluations; generalization and system analysis. Statistical method is based on the accountability of statistics office of the Ministry of National Economy of the Republic of Kazakhstan (RK) and on the results of sociological studies. The official statistic information, materials of the population census of the RK, materials of the Ministry of Health and Social Development of RK, data from author's studies, carried out in the Institute of Economy of science committee of Ministry of Education and Science of the Republic of Kazakhstan were used in this study. The conclusion about positive tendencies in demographic processes and about necessity of improvement of demographic policy was made. A number of proposals and recommendations concerning creation of favorable social and economic conditions for improvement of demographic situation, enhancement of institutional basis of demographic policy, forms and methods of its realization considering priorities of future development of Kazakhstan were justified.

담배 중 pH와 Nicotine 함량에 의한 Free nicotine 측정 (Calculation of Free Nicotine by Determination of pH and Nicotine in Tobacco)

  • 이정민;장기철;황건중;김용하;이문수
    • 한국연초학회지
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    • 제27권2호
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    • pp.219-225
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    • 2005
  • Characterizing nicotine delivery from tobacco products is important in the understanding of their addictive potential. Most previous studies report total nicotine and have not differentiated between nicotine in its protonated or free-base form. The amount of free nicotine calculated by determining pH and nicotine contents. The pH and nicotine contents in smokeless tobacco product, tobacco products and tobacco leaves were analyzed by Health Canada-Official Method T-310 and CORESTA Recommended Method $N^{\circ}62$. The content of free nicotine was calculated according to the Henderson-Hasselbalch equation and the value of $\alpha_{fb}$(the fraction of nicotine that is in the free base form) by using a pKa value of 8.02 for nicotine. The percentage of free nicotine then was calculated by dividing the free nicotine content by total nicotine content. The pH value and percentage of free nicotine ranged from 5.01 to 5.45 and $0.10\%\;to\;0.27\%$ in cut tobacco and 5.10 to 7.10 and $0.12\%\;to\;10.73\%$ in tobacco leaves, respectively.

환각성 약물범죄와 경호안전상의 대응방안 (Measures against Security Safety and Hallucinogenic Drug Crimes)

  • 전경수
    • 시큐리티연구
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    • 제2호
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    • pp.211-226
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    • 1999
  • Troublesome problems are being caused by hallucinogenic drugs which come not only from illegal narcotics but also from unprohibited general drug-kinds such as cough-remedy agents of textromerupan, namely, Lamina, Rubi-king and the likes. Abuse and misuse of narcotics permeated into and threatens mental health of socially-known peoples, actor, actress, talents and businessmen as well. This study especially dealt with problems related with Mesampetamin, Rurajaepam, Texstrometropan and Karisofrodol which affects mental behaviour, and considered counter-measures through analysis and developed appropriate system of goods circulation for guidance to be complied by the medicine professionalists. The guidance sought here is recommended to the government ministries for further enforcement of crack-down of the drug crimes. Arquesa in method is recommend as a method of identifying behaviors and facial expressions of abusers and misusers of narcotics at the spot in place. This study is directed to curtailing hallucinogenic drugs use for absolute preventive security by detecting out black dealers of narcotics supplying to the abusers and misusers. There is a need of special education program to cut off the flow of narcotics or drugs crimes into official security force as well as private security personnel. This study introduced a priority and emphasis of real augmentation to theory and practice of the modern scientific security which can protect the mental health of the guarded persons as well especially in the light of security safety curriculum at the school.

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Factors Affecting the Behavioral Intention and Behavior of Using E-Wallets of Youth in Vietnam

  • PHAN, Trong Nhan;HO, Truc Vi;LE-HOANG, Phuong Viet
    • The Journal of Asian Finance, Economics and Business
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    • 제7권10호
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    • pp.295-302
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    • 2020
  • The study examines an empirical case that explores the key constructs of the Unified Theory of Acceptance and Use of Technology (UTAUT) (Venkatesh, Morris, Davis & Davis, 2003) and the relationship between security and privacy of the Theory of Perceived Risk (TPR) (Bauer, 1960). This study employs survey data of 200 young Internet users aged 18 to 25. The study was conducted through two steps: preliminary research by qualitative research method to form the official research scale then formal research by quantitative research method using CFA and SEM to test the research model. The research results show that performance expectancy and social influence significantly predict behavioral intention to use e-wallets in payment. In contrast, the factors, namely, security and privacy, and effort expectancy, are statistically insignificant on behavioral intention. Nevertheless, the facilitating conditions factor still affects the behavior of using e-wallets. The study proposes a model to generalize the online payment environment through the integration of UTAUT and TPR models that are important for online payment management and researchers in the technology environment. The findings of this study suggest that social influence significantly affects the intention of young people to use e-wallets instead of security and privacy.

침입탐지 시스템 관리를 위한 침입경보 축약기법 적용에 관한 연구 (A Study on Intrusion Alert Redustion Method for IDS Management)

  • 김석훈;정진영;송정길
    • 융합보안논문지
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    • 제5권4호
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    • pp.1-6
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    • 2005
  • 네트워크 시스템에 대한 악의적인 접근과 정보위협이 증가하고, 그 피해또한 기업에서 개인 사용자까지 확대되고 있다. 침입탐지 시스템, 침입차단 시스템 등 단위 보안 기능만을 제공하는 제품은 분산화, 지능화 되어가고 있는 복합적인 침입에 대한 대응에 한계가 있다. 여러 보안 제품을 연동하여 해커의 침입탐지, 대응 및 역 추적을 위한 통합 보안 관리의 필요성이 대두되고 있다. 그러나 통합보안 관리의 특성상 다양한 보안 제품에서 전송된 이벤트와 침입경보의 양이 많아 분석이 어려워 서버측의 부담이 되고 있다. 따라서 본 논문에서는 이러한 문제점을 해결하고자 침입경보 데이터를 축약하는 방법에 대하여 연구하고자 한다.

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기체크로마토그래피를 이용한 식이보충제에서 메틸설포닐메탄의 검증된 분석법 개발 (Development of a Validated Determination of Methylsulfonylmethane in Dietary Supplement by Gas Chromatography)

  • 박상욱;이원재
    • KSBB Journal
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    • 제30권4호
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    • pp.141-147
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    • 2015
  • The convenient determination of methylsulfonylmethane (MSM) for a commercially available dietary supplement was developed using gas chromatography (GC)-flame ionization detector (FID). Chromatography was performed on a capillary column ($0.32mm\;I.D{\times}30m$, $0.25{\mu}m$) coated with dimethylpolysiloxane using diethylene glycol methyl ether as an internal standard. The performance characteristics of GC were evaluated in terms of selectivity, linearity, precision, accuracy, recovery, limit of detection (LOD) and limit of quantification (LOQ). The calibration curve was highly linear (the coefficient of determination: 0.9979) within the concentration range of $10.0{\sim}800.0{\mu}g/mL$ for MSM. The recoveries for three fortified concentrations were 96.7~97.1%, 96.6~97.3% and 96.8~97.2%, respectively. The LOD and LOQ of the method were $0.29{\mu}g/mL$ and $0.97{\mu}g/mL$, respectively. All obtained results were acceptable according to the guidelines of the Association of Official Analytical Chemists for dietary supplements. Thus, the validated analytical method using the GC-FID system is suitable for the determination of MSM in dietary supplement formulations for quality control.