• Title/Summary/Keyword: O-D 분석

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The Fabrication of Micro-electrodes to Analyze the Single-grainboundary of ZnO Varistors and the Analysis of Electrical Properties (ZnO 바리스터의 단입계면 분석을 위한 마이크로 전극 제작과 전기적 특성 해석)

  • So, Soon-Jin;Lim, Keun-Young;Park, Choon-Bae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.3
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    • pp.231-236
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    • 2005
  • To investigate the electrical properties at the single grainboundary of ZnO varistors, micro-electrodes were fabricated on the surface which was polished and thermally etched. Our micro-electrode had 2000 $\AA$ silicon nitride layer between micro-electrode and ZnO surface. This layer was deposited by PECVD and etched by RIE after photoresistor pattering process using by mask 1. The metal patterning of micro-electrodes used lift-off method. We found that the breakdown voltage of single grainboundary is about 3.5∼4.2 V at 0.1 mA on I-V curves. Also, capacitance-voltage measurement at single grainboundary gave several parameters( $N_{d}$, $N_{t}$, $\Phi$$_{b}$, t) which were related with grainboundary.ary.

Environmental Effect on Corrosion Behaviour of Zr-2.5Nb Alloy (Zr-2.5Nb 합금의 부식거동에 미치는 부식 매질 효과)

  • Ju, Gi-Nam;Gwon, Sang-Cheol;Kim, Yeong-Seok
    • Korean Journal of Materials Research
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    • v.8 no.1
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    • pp.3-9
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    • 1998
  • 40$0^{\circ}C$ H$_{2}$O, D$_{2}$O및 $O_{2}$분위기에서 Zr-2.5Nb합금의 부식거동을 분석하였다. Martensitic $\alpha$'-Zr상이나 $\alpha$-Zr과 $\beta$-Zr상의 Zr-2.5Nb합금인 경우, 부식분위기에 매우 민감하여, $O_{2}$속에서 가장 큰 부식속도를 보였다. 반면, $\alpha$-Zr나 $\beta$-Zr상의 경우, 부식 매질에 따른 별다른 차이없이 높은 부식저항성을 보였다. 이러한 Zr-2.5Nb 합금의 미세조직 및 부식 매질에 따른 부식거동변화는 Zr-2.5Nb 합금의 음극 지배 부식반응의 관점으로 해석되었으며, 이들 결과를 이용하여 CANDU 형및 RBMK 형 Zr-2.5Nb 압력관의 가동조건 차이를 설명할 수 있었다. Zr-2.5Nb 합금의 모든 조직에서 주로 단사정 ZrO$_{2}$산화물이 형성되었으며, 산화물내 정방정 ZrO$_{2}$비율은 산화물 두께가 증가함에 따라 감소하였다.

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화학증기수송법을 이용한 금속 몰리브덴 박막 증착

  • Park, Chang-Won;Lee, Yeong-Jung;Kim, Dae-Geon;Kim, Yeong-Do
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.53.2-53.2
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    • 2009
  • 몰리브덴(Mo)은 우수한 전기전도도와 고온 안정성으로 인해 전자부품의 전극으로 널리 사용되고, 미래 에너지인 태양전지 분야에서 CIS계 화합물박막태양전지의 후면전극으로 이용되고 있는 재료로서 현재 증착 방법으로는 D.C. sputtering이 가장 널리 이용되고 있다. 또한 $MoO_3$ 분말이 Mo 분말로 수소 환원되는 과정은 $MoO_3+H_2{\rightarrow}MoO_2+H_2O$$MoO_2+2H_2{\rightarrow}Mo+2H_2O$의 2단계를 통해서 수행되며 이중 첫 번째 단계에서 $MoO_3(OH)_2$라는 기상을 통해 지배적으로 일어난다고 알려져 있고 이를 화학증기수송(Chemical vapor transport : CVT)이라고 한다. 본 연구에서는 $MoO_3$분말의 수소 환원 과정 중에 발생하는 기상인 $MoO_3(OH)_2$을 이용하여 몰리브덴 옥사이드 박막을 증착하고 이를 다시 수소분위기에서 수소 환원하는 증착 방법을 통해 균일하고 부착성이 우수한 Mo 박막을 제조하고자 하였다. 기판으로 사용된 Glass를 $MoO_3$ 분말 위에 홀더를 이용하여 $MoO_2$ 박막을 증착하고 이를 다시 수소분위기에서의 수소 환원을 통해 Mo 박막을 성공적으로 제조하였다. 제조된 Mo박막의 결정구조 및 미세조직을 XRD 와 SEM을 통해 분석하였다.

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Fabrication and Characterization of Highly Reactive Al/CuO Nano-composite using Graphene Oxide (산화그래핀을 적용한 고반응성 Al/CuO 나노복합재 제조 및 분석)

  • Lim, YeSeul
    • Journal of Powder Materials
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    • v.26 no.3
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    • pp.220-224
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    • 2019
  • The aluminum (Al)/copper oxide (CuO) complex is known as the most promising material for thermite reactions, releasing a high heat and pressure through ignition or thermal heating. To improve the reaction rate and wettability for handling safety, nanosized primary particles are applied on Al/CuO composite for energetic materials in explosives or propellants. Herein, graphene oxide (GO) is adopted for the Al/CuO composites as the functional supporting materials, preventing a phase-separation between solvent and composites, leading to a significantly enhanced reactivity. The characterizations of Al/CuO decorated on GO(Al/CuO/GO) are performed through scanning electron microscopy, transmission electron microscopy, and energy dispersive X-ray spectroscopy mapping analysis. Moreover, the functional bridging between Al/CuO and GO is suggested by identifying the chemical bonding with GO in X-ray photoelectron spectroscopy analysis. The reactivity of Al/CuO/GO composites is evaluated by comparing the maximum pressure and rate of the pressure increase of Al/CuO and Al/CuO/GO. The composites with a specific concentration of GO (10 wt%) demonstrate a well-dispersed mixture in hexane solution without phase separation.

The Leakage Current Analysis of ZnO Arrester Using Leakage Current Dete (피뢰기 누설전류 분석장치를 이용한 ZnO 피뢰기의 누설전류 변화 분석)

  • Kim, Young-Chun;Moon, Sun-Ho;Oh, Jung-Hwan;Kim, Jae-Chul;Lee, Young-Gil
    • Proceedings of the KIEE Conference
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    • 1998.07c
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    • pp.1082-1084
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    • 1998
  • In this paper, we developed a diagnosis device for ZnO arrester to detect on-line leakage current and acquire data from the power distribution system. The arrester is important power equipment used in power transmission and distribution systems to protect the generator and the main transformer from surge and overvoltage. First of all we developed a diagnosis device for ZnO arrester leakage current. And then we detect the total leakage current by the developed device without disconnecting the arrester ground wire and analysis the 3rd order harmonic by Fast Fourier Transform(FFT) to diagnose the ZnO arrester deterioration. With measuring the total current and the resistive current of power distribution system in operation, we analysis the trend of resistive current component in the total leakage current. We expect the result will be promote the method to protect electrical utility and customer from accident.

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Analysis and Comparison of Cerebroside Components from Soybean Fermented Foods (대두발효식품 Cerebroside의 구성성분 분석 및 비교)

  • 이은열;김희숙
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.31 no.2
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    • pp.177-183
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    • 2002
  • Cerebroside fatty acids, sugars and long-chain sphingoid bases in raw soybean and soybean fermented foods (chongkukjang and deunjang) were analyzed using gas chromatography-mass spectrometry (GC-MS) and high-pH anion exchange chromatography with pulsed amerometric detection (HPAEC-PAD). Fatty acids of acid-hydrolyzed cerebrosides were derivatized to O-TMS methylester and analysed. The major fatty acids in raw soybean and chongkukjang cerebrosides were identified as 2-hydroxyhexadecanoic acid (16 : 0h), 2-hydroxydocosanoic acid (22 : 0h) and 2-hydroxytetracosanoic acid (24 : 0h). In the case of deunjang cerebroside, 24 : 0h (40.9%) and 22 : 0h (23.4%) were major fatty acids, but 16 : 0h, 23 : 0h, 25 : 0h and 26 : 0h were also detected. Long-chain sphingoid bases of acid-hydrolyzed cerebrosides from raw soybean, chongkukjang and deunjang consisted primarily of 4-tracts, 8-tracts-sphingadienine (dihydroxy base, d18 : 2$\Delta$$^{4trans, 8trans}$) and sis-tracts isomers of 4-hydroxy-sphingenine (trihydroxy base, tl8:1$\Delta$$^{4trans or cis}$) with much less amounts of phytosphingosine (tl8: 0) and isomers of sphingenine (d18 : 1). Although deunjang is a soybean food fermented by fungi and microorganisms for a long period, 2-hydroxyoctadec-3-enoic acid (18 : 1h) and branched 9-methyl-4,8-sphingadienine known as compositional cerebroside fatty acids in Aspergillus species were not detected. Mass spectrum for sugar derivatives in cerebrosides of soybean foods including raw soybean and fermented soybean showed that C-1 of glucose moiety was linked to ceramide backbone as like a monoglucosylceramide.

Effect of O2/Ar+O2 concentration on phase stability of transparent Mn doped SnO2 monolayer film (혼합기체 O2/Ar+O2 농도 변화가 Mn 도핑된 SnO2 투명전도막의 상 안정성에 미치는 영향)

  • Kim, Taekeun;Jang, Guneik
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.31 no.4
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    • pp.154-158
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    • 2021
  • The optical transmittance of Mn-doped SnO2 monolayer film increased gradually from 80.9 to 85.4 % at 550 nm wavelengths upon increasing the O2/Ar+O2 concentration rate from 0 to 7.9 % and the band gap energy changed from 3.0 to 3.6 eV. The resistivity tended to decrease from 3.21 Ω·cm to 0.03 Ω·cm, reaching a minimum at 2.7 %, and then gradually increased from 0.03 to 52.0 Ω·cm at higher O2/Ar+O2 gas concentration ratio. Based on XPS spectra analysis, the Sn 3d5/2 peak of Mn-doped SnO2 single layer shifted slightly from 486.40 to 486.58 and O1s peak also shifted from 530.20 to 530.33 eV with increase the O2/Ar+O2 concentration ratio. Therefore, the XPS spectra results indicate that a multiphase with SnO and SnO2 coexisted in the sputtered Mn-doped SnO2 monolayer film.

Prefetch R-tree: A Disk and Cache Optimized Multidimensional Index Structure (Prefetch R-tree: 디스크와 CPU 캐시에 최적화된 다차원 색인 구조)

  • Park Myung-Sun
    • The KIPS Transactions:PartD
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    • v.13D no.4 s.107
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    • pp.463-476
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    • 2006
  • R-trees have been traditionally optimized for the I/O performance with the disk page as the tree node. Recently, researchers have proposed cache-conscious variations of R-trees optimized for the CPU cache performance in main memory environments, where the node size is several cache lines wide and more entries are packed in a node by compressing MBR keys. However, because there is a big difference between the node sizes of two types of R-trees, disk-optimized R-trees show poor cache performance while cache-optimized R-trees exhibit poor disk performance. In this paper, we propose a cache and disk optimized R-tree, called the PR-tree (Prefetching R-tree). For the cache performance, the node size of the PR-tree is wider than a cache line, and the prefetch instruction is used to reduce the number of cache misses. For the I/O performance, the nodes of the PR-tree are fitted into one disk page. We represent the detailed analysis of cache misses for range queries, and enumerate all the reasonable in-page leaf and nonleaf node sizes, and heights of in-page trees to figure out tree parameters for best cache and I/O performance. The PR-tree that we propose achieves better cache performance than the disk-optimized R-tree: a factor of 3.5-15.1 improvement for one-by-one insertions, 6.5-15.1 improvement for deletions, 1.3-1.9 improvement for range queries, and 2.7-9.7 improvement for k-nearest neighbor queries. All experimental results do not show notable declines of the I/O performance.

Comparison of Several Methods for the Evaluation of Available Soil P in Upland Soils (전토양(田土壤)의 유효인산 분석방법(分析方法) 비교(比較))

  • Yoon, Jung-Hui;Shin, Cheol-Woo;Ryu, In-Sao;Hong, Chong-Woon
    • Korean Journal of Soil Science and Fertilizer
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    • v.10 no.4
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    • pp.219-224
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    • 1978
  • To compare various methods for available soil P test, in terms of correlation between crop yield and amounts of available soil P, a pot experiment was conducted with soybean as test plant using four upland soils differing in phosphorus status. The results are summarized as following. 1. There was highly significant correlation between grain yield and amount of P uptake observed at the floral differentiation stage. Highly significant correlations were also observed between grain yield and available soil P of different methods, and between the amount of P uptake and available soil P. The consistency of correlations between soil P and plant parameters was Olsen${\geq}$Lancaster P>Bray No.1 P${\geq}$Bray No.2 P>Truog P. 2. The magnitute of available soil P values of different methods was in the order of Bray No.2>Lancaster P${\geq}$Bray No.1 P>Olsen P>Truog P. 3. The amounts of available P measured by various methods showed significant correlation with the amounts of Al-P, Fe-P and Ca-P. 4. As conclusion, Olsen-P, Lancaster-P, and Bray-P are reliable information for evaluating soil P status. However, Olesen-P seemed to be better than the others.

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An analysis of optimal design conditions of LDPC decoder for IEEE 802.11n Wireless LAN Standard (IEEE 802.11n 무선랜 표준용 LDPC 복호기의 최적 설계조건 분석)

  • Jung, Sang-Hyeok;Na, Young-Heon;Shin, Kyung-Wook
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.14 no.4
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    • pp.939-947
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    • 2010
  • The LDPC(Low-Density Parity-Check) code, which is one of the channel encoding methods in IEEE 802.11n wireless LAN standard, has superior error-correcting capabilities. Since the hardware complexity of LDPC decoder is high, it is very important to take into account the trade-offs between hardware complexity and decoding performance. In this paper, the effects of LLR(Log-Likelihood Ratio) approximation on the performance of MSA(Min-Sum Algorithm)-based LDPC decoder are analyzed, and some optimal design conditions are derived. The parity check matrix with block length of 1,944 bits and code rate of 1/2 in IEEE 802.11n WLAN standard is used. In the case of $BER=10^{-3}$, the $E_b/N_o$ difference between LLR bit-widths (6,4) and (7,5) is 0.62 dB, and $E_b/N_o$ difference for iteration cycles 6 and 7 is 0.3 dB. The simulation results show that optimal BER performance can be achieved by LLR bit-width of (7,5) and iteration cycle of 7.