• Title/Summary/Keyword: Modulus Measurement

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Sensitivity Analysis in the Estimation of Complex Elastic Modulus of Viscoelastic Materials by Transmissibility Measurements (전달율 측정에 의한 점탄성재료의 복소탄성계수 추출시의 민감도 분석)

  • 안태길;허진욱;김광준
    • Journal of KSNVE
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    • v.2 no.2
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    • pp.99-106
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    • 1992
  • The complex Young's modulus of a viscoelastic material can be obtained as a function of frequency from the measurements of relative motion between the two ends of a bar-type specimen. Non-resonance method is usually used to obtain the complex Young's modulus over wide range of frequency including resonance points, while in resonance method information at resonance frequencies only is used. However, the complex Young's modulus obtained by the non-resonance method is often unreliable in the anti-resonance frequency regions because of the measurement noise problems. In this study, the effects of the random measurement errors on estimating the complex Young's modulus are studied in the aspect of sensitivity, and how to obtain the reliable frequency region for a given measurement error level is shown. The usable frequency regions in determining the complex Young's modulus are represented by a non-dimensional parameter formed with the wave length and specimen length.

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Modulus Properties and Smoothness Measurement of Semiconducting Materials Using the DMA and SEM (DMA와 SEM을 사용한 반도전층 재료의 탄성특성과 평활도 측정)

  • Yang, Jong-Seok;Lee, Kyoung-Yong;Choi, Yong-Sung;Park, Dae-Hee
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.54 no.10
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    • pp.443-448
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    • 2005
  • To measure modulus, damping properties and smoothness of semiconducting materials in power cable, we have investigated those of semiconducting materials showed by changing the content of carbon black. Then they were produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[kg/cm$^{2}$]. The content of conductive carbon black was the variable, and their contents were 20, 30 and 40[wt$\%$], respectively. The modulus and tans were measured by DMA 2980. The ranges of measurement temperature were from -50[$^{\circ}C$] to 100[$^{\circ}C$] and measurement frequency was 1[Hz3. The modulus of specimens was increased according to a increment of a carbon black content. And modulus was rapidly decreased at the glass transition temperature. The tans of specimens was decreased according to a increment of a carbon black content. The smoothness was measured by JSM-6400. EEA resin from SEM measurement was best the dispersion of carbon back in base resin.

An experimental method to determine glass elastic modulus based on the fundamental frequency of the elastic support-free end beam

  • Kun Jiang;Danguang Pan
    • Structural Engineering and Mechanics
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    • v.88 no.2
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    • pp.189-200
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    • 2023
  • Silicate glass is usually a brittle and plate-like material, and it is difficult to measure the elastic modulus by the traditional method. This paper develops a test method for the glass elastic modulus based on the fundamental frequency of the cantilever beam with an elastic support and a free end. The method installs the beam-type specimen on a semi-rigid support to form an elastic support-free end beam. The analytic solution of the stiffness coefficients of the elastic support is developed by the fundamental frequency of the two specimens with known elastic modulus. Then, the glass elastic modulus is measured by the fundamental frequency of the specimens. The method significantly improves the measurement accuracy and is suitable for the elastic modulus with the beam-type specimen whether the glass is homogeneous or not. Several tests on the elastic modulus measurement are conducted to demonstrate the reliability and validity of the test method.

Modulus and Fractural Side Measurement of Semiconductive Shield (Materials) in Power Cable Using the DMA (DMA를 사용한 전력케이블 내 반도전층 재료의 탄성율 및 에너지 손실 측정)

  • Yang, Jong-Seok;Lee, Kyung-Yong;Choi, Yong-Sung;Nam, Jong-Chul;Park, Dong-Ha;Park, Dae-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.213-214
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    • 2005
  • To measure modulus and damping of semiconductive materials in power cable, we have investigated the modulus and damping of semiconductive materials showed by changing the content of carbon black. Then they were produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[$kg/cm^2$]. The content of conduct ive carbon black was the vailable, and their contents were 20, 30 and 40[wt%], respectively. The modulus and $Tan\delta$ experiments were measured by DMA 2980. Ranges of measurement temperature from -50[$^{\circ}C$] to 100[$^{\circ}C$] and measurement frequency is 1[Hz]. The modulus of specimens was increased according to a increment of a carbon black content. And modulus was rapidly decreased at the glass transition temperature. The $Tan\delta$ of specimens was decreased according to a increment of a carbon black content.

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A Study on the Measurement of Young's Modulus of Carbon Nano Tube (탄소 나노 튜브의 영 계수 측정에 관한 연구)

  • 이준석;최재성;강경수;곽윤근;김수현
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.682-685
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    • 2003
  • In this paper, we propose the method to measure the Young's modulus of carbon nano tube which was manufactured by chemical vapor deposition. We also made the tungsten tip by electrochemical etching process and the carbon nano tube which was detangled through ultra-sonication with isopropyl alcohol was attached to the tungsten tip. This tip which was composed of tungsten tip and carbon nano tube can be used in Young's modulus measurement by applying DC voltage with counter electrode. The attachment process and measurement of the deflection of carbon nano tube was done under optical microscope.

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Determination of Elastic Modulus by Time Average ESPI and Euler-Bernoulli Equation (Time Average ESPI와 Euler-Bernoulli 방정식에 의한 탄성계수 측정)

  • Kim, Koung-Suk;Lee, Hang-Seo;Kang, Young-June;Kang, Ki-Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.7 s.196
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    • pp.69-74
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    • 2007
  • The paper proposes a new sonic resonance test for a elastic modulus measurement which is based on time-average electronic speckle pattern interferometry(TA-ESPI) and Euler-Bernoulli equation. Previous measurement technique of elastic constant has the limitation of application for thin film or polymer material because contact to specimen affects the result. TA-ESPI has been developed as a non-contact optical measurement technique which can visualize resonance vibration mode shapes with whole-field. The maximum vibration amplitude at each vibration mode shape is a clue to find the resonance frequencies. The dynamic elastic constant of test material can be easily estimated from Euler-Bernoulli equation using the measured resonance frequencies. The proposed technique is able to give high accurate elastic modulus of materials through a simple experiment set up and analysis.

Evaluation of Mechanical Properties of Structural Ceramics ($Al_{2}O_{3}$) Using the High Frequency Ultrasonic C - Scan (초음파 C-Scan을 이용한 구조용 세라믹스의 기계적 특성평가)

  • Chang, Y.K.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.9 no.2
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    • pp.18-24
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    • 1989
  • Computer-aided high frequency ultrasonic is applied to aluminum oxide(85w%, 94w%, 96w%, and 99w%) MOR(modulus of rupture) samples to evaluate mechanical properties such as density variation, pore content, elastic modulus, shear modulus, and poisson's ratio. Ultrasonic wave velocity and attenuation measurement techniques were used as an evaluator of such properties. Pulse-echo C-Scan images with different fate setting method using 50MHz center frequency 1 inch focal length transducer allows evaluation of density variation and pore content. Elastic modulus calculated with the relation of density and ultrasonic velocity. It shows good reliability as compared with resonance method. Sintered density variation of $0.025g/cm^{3}$, that is 0.6% of theoretical density in $Al_{2}O_{3}$ samples can be observed by ultrasonic velocity measurement. Attenuation measurement method qualitatively agree with 4-point fracture testing result concerning of porosity content.

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A Pilot study of poroelastic modulus measurement in micro-bone tissue (미세 골조직의 공극탄성계수 측정을 위한 예비 연구)

  • 박영환;홍정화
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1038-1041
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    • 2004
  • In this study, developed a micro-level experimental setup to measure pore pressure and poroelastic modulus in various strain and strain rate about a stress in micro-structure of bone tissue. It is essential device in the development of the model to analysis the interstitial bone fluid flow of the lacuno-canalicular system to be known that would effect on the bone remodeling. The constitution of the experimental setup is as follows, microscopic image processing system; actuator control unit; load measurement system. A pilot study was used an artificial chemical wood to have similar poroelastic property of bone matrix and conducted to validate the suitability of the measurement system.

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ESTIMATION TECHNIQUE Of AIR CONTENT IN TUTOMATIC TRANSMISSION FLUID BY MEASURING EFFECTIVE BULK MODULUS

  • Cho, Baek-Hyun;Lee, Hyoun-Woo;Oh, Jong-Sun
    • International Journal of Automotive Technology
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    • v.3 no.2
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    • pp.57-62
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    • 2002
  • It is well known that the entrained air in oil causes appreciable reduction in the stiffness of hydraulic systems. It makes the response delay of the systems and sometimes destroys the stability. Because the hydraulic systems of automatic transmissions are operated in relatively low pressure and high temperature, it is very important to analyze the effects of the air included in automatic transmission fluid. However, it is difficult to derive the generalized model to describe the effective bulk modulus theoretically or measure it in actual operating conditions of automatic transmissions. This paper reviews previous studies of the air effects in hydraulic systems and the measurement techniques of the effective bulk modulus in operating conditions. Based on this work, the theoretical model with moderate complexity and the measurement technique of the effective bulk modulus considering entrained air effect at real operating conditions are suggested. Our paper also shows that the quantity of the entrained air in the automatic transmission fluid can be estimated from the experimental results.

The Measurement Errors of Elastic Modulus and Hardness due to the Different Indentation Speed (압입속도의 변화에 따른 탄성계수와 경도의 오차 연구)

  • Lee, Kyu-Young;Lee, Chan-Bin;Kim, Soo-In;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.19 no.5
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    • pp.360-364
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    • 2010
  • Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.