• 제목/요약/키워드: Mixing of materials

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화학소재 생산용 반응 모듈의 혼합 성능 해석 (Characterization of Mixing in Reaction Modules for the Production of Chemical Materials)

  • 서정현;김유석;최재훈
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.537-538
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    • 2006
  • Split and recombine type reaction module was made by electrical discharge machining. The reaction module has special features to well mix the two reactants which have high flow ratio or high concentrations difference. It could be achieved by deviding one flow equally by two and inserting second flow in between. The mixing performance was measured by a parallel competing reaction with iodide-iodate system. The result shows that the developed three inlets micromixer has better mixing efficiency than comercialized Y type micromixer.

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열 수소화법에 의해 제조된 TiO2-Co 복합분말 SPS 소결체의 미세구조 및 기계적 성질 (The Microstructure and the Mechanical Properties of Sintered TiO2-Co Composite Prepared Via Thermal Hydrogenation Method)

  • 고명선;박일송;박제신
    • 한국분말재료학회지
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    • 제26권4호
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    • pp.290-298
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    • 2019
  • $TiO_2$-particles containing Co grains are fabricated via thermal hydrogenation and selective oxidation of TiCo alloy. For comparison, $TiO_2$-Co composite powders are prepared by two kinds of methods which were the mechanical carbonization and oxidation process, and the conventional mixing process. The microstructural characteristics of the prepared composites are analyzed by X-ray diffraction, field-emission scattering electron microscopy, and transmission electron microscopy. In addition, the composite powders are sintered at $800^{\circ}C$ by spark plasma sintering. The flexural strength and fracture toughness of the sintered samples prepared by thermal hydrogenation and mechanical carbonization are found to be higher than those of the samples prepared by the conventional mixing process. Moreover, the microstructures of sintered samples prepared by thermal hydrogenation and mechanical carbonization processes are found to be similar. The difference in the mechanical properties of sintered samples prepared by thermal hydrogenation and mechanical carbonization processes is attributed to the different sizes of metallic Co particles in the samples.

고엔트로피합금 분말야금재와 알루미늄 주조재 사이의 계면 반응 연구 (Interfacial Reaction between Spark Plasma Sintered High-entropy Alloys and Cast Aluminum)

  • 김민상;손한솔;정차희;한주연;김정준;김영도;최현주;김세훈
    • 한국분말재료학회지
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    • 제29권3호
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    • pp.213-218
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    • 2022
  • This study investigates the interfacial reaction between powder-metallurgy high-entropy alloys (HEAs) and cast aluminum. HEA pellets are produced by the spark plasma sintering of Al0.5CoCrCu0.5FeNi HEA powder. These sintered pellets are then placed in molten Al, and the phases formed at the interface between the HEA pellets and cast Al are analyzed. First, Kirkendall voids are observed due to the difference in the diffusion rates between the liquid Al and solid HEA phases. In addition, although Co, Fe, and Ni atoms, which have low mixing enthalpies with Al, diffuse toward Al, Cu atoms, which have a high mixing enthalpy with Al, tend to form Al-Cu intermetallic compounds. These results provide guidelines for designing Al matrix composites containing high-entropy phases.

In vitro cytotoxicity of four calcium silicate-based endodontic cements on human monocytes, a colorimetric MTT assay

  • Khedmat, Sedigheh;Dehghan, Somayyeh;Hadjati, Jamshid;Masoumi, Farimah;Nekoofar, Mohammad Hossein;Dummer, Paul Michael Howell
    • Restorative Dentistry and Endodontics
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    • 제39권3호
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    • pp.149-154
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    • 2014
  • Objectives: This study was performed to evaluate the cytotoxicity of four calcium silicate-based endodontic cements at different storage times after mixing. Materials and Methods: Capillary tubes were filled with Biodentine (Septodont), Calcium Enriched Mixture (CEM cement, BioniqueDent), Tech Biosealer Endo (Tech Biosealer) and ProRoot MTA (Dentsply Tulsa Dental). Empty tubes and tubes containing Dycal were used as negative and positive control groups respectively. Filled capillary tubes were kept in 0.2 mL microtubes and incubated at $37^{\circ}C$. Each material was divided into 3 groups for testing at intervals of 24 hr, 7 day and 28 day after mixing. Human monocytes were isolated from peripheral blood mononuclear cells and cocultered with 24 hr, 7 day and 28 day samples of different materials for 24 and 48 hr. Cell viability was evaluated using an MTT assay. Results: In all groups, the viability of monocytes significantly improved with increasing storage time regardless of the incubation time (p < 0.001). After 24 hr of incubation, there was no significant difference between the materials regarding monocyte viability. However, at 48 hr of incubation, ProRoot MTA and Biodentine were less cytotoxic than CEM cement and Biosealer (p < 0.01). Conclusions: Biodentine and ProRoot MTA had similar biocompatibility. Mixing ProRoot MTA with PBS in place of distilled water had no effect on its biocompatibility. Biosealer and CEM cement after 48 hr of incubation were significantly more cytotoxic to on monocyte cells compared to ProRoot MTA and Biodentine.

Evaluating Feasibility of Producing Fermented Organic Fertilizer with Vegetable Waste

  • Kim, Eui-Yeong;Kook, Seung-Woo;Oh, Taek-Keun;Lee, Chang-Hoon;Ko, Byong-Gu;Kim, Seok-Cheol;Kim, Sung-Chul
    • 한국토양비료학회지
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    • 제49권6호
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    • pp.760-767
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    • 2016
  • Food waste (FW) has been recognized as a critical problem in Korea and many research was conducted to efficiently utilize or treat FW. Main purpose of this research was to evaluate a feasibility for producing fermented organic fertilizer with vegetable waste (VW). Three different organic materials (saw dust, coco peat, and waste mushroom media) were mixed with VW at the rate of 30, 40, 50% respectively. Total days of composting experiment were 35 days and each sub samples were collected at every 5 days from starting of composting. Result showed that inner temperature of composting was increased to $60{\pm}4^{\circ}C$ within 5~10 days depending on varied organic materials and mixing ratio. Among different treatment, the highest increase of inner temperature was observed when 30% of saw dust was mixed with VW. After finishing composting experiment, maturity of each compost was evaluated with solvita and germination test. Maturity index (MI) of each treatment was ranged between 5~7 indicating that manufactured fertilizer was curing or finished stage. Calculated germination index (GI) was at the range of 57.83~101.16 depending on organic materials and mixing ratio. Both MI and GI showed that manufactured fertilizer was met for fertilizer criteria while control (VW only) was not adequate for composting. Overall, VW can be utilized for making organic fertilizer mixing with saw dust, coco peat and more research should be conducted to make high quality of organic fertilizer with vegetable waste.

웨어러블 패키징용 Polydimethylsiloxane (PDMS) 신축성 기판의 강성도 변화거동 (Variation of Elastic Stiffness of Polydimethylsiloxane (PDMS) Stretchable Substrates for Wearable Packaging Applications)

  • 최정열;박대웅;오태성
    • 마이크로전자및패키징학회지
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    • 제21권4호
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    • pp.125-131
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    • 2014
  • 웨어러블 패키징용 신축성 기판을 개발하기 위해 투명한 PDMS인 Sylgard 184와 검정색 PDMS인 Sylgard 170에 대해 base/curing agent 혼합비에 따른 탄성계수의 변화거동을 분석하였다. Sylgard 184와 Sylgard 170의 공칭응력-공칭변형률 곡선에서 구한 공칭탄성계수에 비해 진응력-진변형률 관계로부터 구한 진탄성계수가 2배 이상 높았으며, 진탄성계수와 공칭탄성계수의 차이는 PDMS의 강성도가 높아질수록 증가하였다. Sylgard 184에서는 base/curing agent의 혼합비가 10일 때 탄성계수의 최대값을 얻을 수 있었으며, 이때 공칭탄성계수는 1.74 MPa, 진탄성계수는 3.57 MPa이었다. Sylgard 170에서는 base/curing agent 혼합비가 2일 때 탄성계수가 최대가 되었으며, 이때 공칭탄성계수와 진탄성계수는 각기 1.51 MPa와 3.64 MPa이었다.

$LiCoO_2$의 재합성시(再合成時) 전극특성(電極特性)에 미치는 탄소(炭素)의 영향(影響) (Effect of Carbon on Electrode Characteristics of $LiCoO_2$ Resynthesis)

  • 이철경;박정길;손정수
    • 자원리싸이클링
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    • 제16권6호
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    • pp.10-19
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    • 2007
  • 폐리튬이온전지의 리싸이클링을 위하여 폐전지의 기계적 처리에 의한 Co의 농축과 습식처리에 의한 Co의 회수기술이 개발되었다. 전 연구에서는 폐전지 리싸이클링의 부가가치를 향상시키기 위하여 Co 농축 침출액으로부터 양극활물질을 재합성하는 공정으로 citrate precursor combustion법을 제안하고 가능성을 확인하였다. 기존의 전극제조 공정에서는 활물질인 $LiCoO_2$와 첨가제인 탄소의 비중 및 크기 차이로 균일한 혼합이 이루어지지 않으므로 충방전 용량이 이론용량에 비하여 매우 낮고 또한 싸이클이 반복될수록 용량이 크게 감소하는 경향을 보였다. 본 연구에서는 합성된 $LiCoO_2$ 전극특성을 향상시키는 일환으로 합성공정의 개선을 통하여 초미립 $LiCoO_2$을 합성하였으며, 탄소 첨가시 혼합법의 개선에 의하여 우수한 충방전 특성을 갖는 리튬전지용 양극을 개발하였다.

주거공간 마감재에 대한 오브제개념의 적용특성 연구 - 대구지역 $99m^2$(30평형)~$162m^2$(40평형)의 아파트 주거공간을 중심으로 - (A Study on the Application Characteristic of Objet Concept to Materials in Housing Space - Focused on the Housing Space of $99m^2{\sim}162m^2$ in Daegu -)

  • 서지은
    • 한국실내디자인학회논문집
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    • 제19권4호
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    • pp.58-65
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    • 2010
  • The purpose of this study is to be applied with the basic data for the design method in the housing space which is differential. So, we analyzed the expression method and the application characteristic to materials of units in housing complex. To that, we researched on the condition of finishing material about the kind of material, color, texture and pattern for components in living room space. The results of this study are as follows : First, at the present time, the Object concept is expressed by 'mixing' and 'juxtaposition' of material, texture and pattern of finishing materials in housing space. But, we could find that the Object concept was used restrictively in housing space. So, we have to find different expression methods to be the effective and differential design by being applied Object concept for the housing space. Second, the 'mixing' which is the method to express the Object concept is showed in only 'art wall'. so, we can estimate that the method is the limited method to plan the varied housing. It is needed various expression methods to design components for the housing space. Third, it showed that the 'mixing' was a passive expression method using a little differential for design of housing space. We could estimate that similar methods were applied to the housing design. By results of this study, we can think that the develop study is needed to find design methods for expression of the Object in housing space.