• Title/Summary/Keyword: MicroSeal

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Fabrication of plastic CE (capillary electrophoresis) microchip by hot embossing process (핫 엠보싱 공정을 이용한 플라스틱 CE(capillary electrophoresis) 마이크로 칩의 제작)

  • Cha Nam-Goo;Park Chang-Hwa;Lim Hyun-Woo;Park Jin-Goo
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.1140-1144
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    • 2005
  • A plastic-based CE (capillary electrophoresis) microchip was fabricated by hot embossing process. A Si mold was made by wet etching process and a PMMA wafer was cut off from 1mm thick PMMA sheet. A micro-channel structure on PMMA substrate was produced by hot embossing process using the Si mold and the PMMA wafer. A vacuum assisted thermal bonding procedure was employed to seal an imprinted PMMA wafer and a blank PMMA wafer. The results of microscopic cross sectional images showed dimensions of channels were well preserved during thermal bonding process. In our procedure, the deformation amount of bonding process was below 1%. The entire fabrication process may be very useful for plastic based microchip systems.

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A Study on the Non-destructive Inspection for End Closure Welding of Nuclear Fuel Elements for the Irradiation Test (조사시험용 핵연료봉 용접부 비파괴검사에 관한 연구)

  • 김웅기;김수성;이철용;이도연;이정원
    • Proceedings of the KWS Conference
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    • 2004.05a
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    • pp.302-304
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    • 2004
  • Nuclear fuel elements containing dry recycling nuclear fuel pellets for the irradiation test in a reactor were remotely fabricated from spent PWR fuel materials in a hot cell. End closure welding as well as seal tube welding for thermal sensor of the elements was performed by Nd:YAG laser. The soundness of the end closure welds and seal tube welds for the elements were evaluated by a precise X-ray inspection system composed of a micro-focus X-ray generator with an image intensifier and a real time camera system. Then, helium leak test was performed for the elements. The soundness of the welds of the fuel elements was confirmed by the X-ray inspection and helium leak test. The irradiation test for the fuel elements were successfully completed at the HANARO research reactor.

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A Study for Comparing Road Noise by Surface Types using NCPX (NCPX를 이용한 도로 표층 유형별 노면 소음 비교 연구)

  • Kang, Won Pyoung;Moon, Hak Ryong
    • International Journal of Highway Engineering
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    • v.15 no.6
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    • pp.61-68
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    • 2013
  • PURPOSES : The purpose of this study is to study the noise reducing effect of Micro Surfacing by comparing general asphalt, longitudinal tining and Slurry Seal. METHODS : This study measures vehicles' noise of each section by the NCPX method that can measure noise between the road surface and the tire at the field. Total sound pressure and sound pressure level by the 1/3 octave band frequency are calculated through the field data of each section. Total sound pressure level is compared by ANOVA test statistically. After ANOVA test, post-hoc test is conducted to know mean difference of surface type by Tukey. RESULTS : As the result of CPB analysis to confirm sound pressure levels by frequency, it was shown that sound pressure levels by frequency are totally similar except for those of frequency bands between 100Hz and 500Hz. The result of ANOVA test and post-hoc test, it was shown that sections of surface type have a difference. The result of Micro Surfacing was lower 2~5dB(A) than other surface type. CONCLUSIONS : It is found that the noise reduction performance of Micro Surfacing was better than other surface type.

The Effectiveness of Obturating Techniques in Sealing Isthmuses (근관충전방법에 따른 근단부 isthmus의 폐쇄효과에 관한 비교연구)

  • Ho-Keel Hwang;Young-Guen Shin
    • Restorative Dentistry and Endodontics
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    • v.26 no.6
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    • pp.499-506
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    • 2001
  • 불완전하게 충전되거나 충전이 되지않은 isthmus는 다근치에 있어서 근관치료의 높은 실패율을 나타낸다 따라서 본 연구의 목적은 isthmus를 갖는 근관을 골라 근관계의 기구조작을 시행하고 여러 가지 근관충전 방법을 이용하여 근관을 충전한 다음 근단부 형성시 적절한 파일의 크기와 치근단부의 밀폐효과를 각 부위별로 비교평가 해보고자 하는 것이다. Isthmus를 갖는 66개의 발거한 치아를 대상으로 기구조작을 통하여 근관확대를 완성하고 무작위로 각각 20개씩 3군으로 분류한 다음 아래와 같은 방법으로 근관을 충전하였다. : A군 측방가압충전법으로 충전한 군, B군 Continuous wave 충전법으로 충전한 군, C군 MicroSeal$^{TM}$을 이용하여 충전한 군. 나머지 6개의 치아는 3개씩 양성대조군과 음성대조군으로 정하였으며 기구조작 후 근관은 충전하지 않은 채로 두었다. 대조군을 제외한 모든 군은 각각 제조회사의 지시에 따라 근관충전한 후 각 시편의 치근단부 2mm를 제외하고 나머지 부위는 두겹의 nail polish를 발라주었으며 2% methylene blue용액에 침잠시켰다 일주일 후 꺼내어 흐르는 물에 깨끗이 세척한 다음 치근단 부위에서부터 1mm씩 잘라가면서 20배의 배율에서 염색액의 침투정도를 평가하였다. 염색액의 침투정도는 다음과 같이 평가되었다. A군과 B군에서는 많은 수의 시편에서 4mm 이상의 절단면에 염색액의 침투를 보인 반면 C군에서는 단지 3mm절단면에서 총 20개 중 3개의 시편에서 염색액의 침투를 보였을 뿐 그 이상의 절단면에서는 염색액의 침투를 보이지 않았다. 뿐만 아니라 isthmus를 갖는 제2형 근관계의 근단부 형성은 40번 크기보다는 큰 MAF가 요구되는 것으로 나타났다. 이러한 결과를 비추어볼 때 isthmus를 갖는 다근치에서 근관충전시 적어도 40번 이상의 MAF로 근단부 형성을 한 후, 열가소성 Continuous wave 충전법과 MicroSeal$^{TM}$을 이용한 근관충전법이 기존의 측방가압충전법 보다는 효과적인 것으로 나타났다.

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Evaluation of Micro-defects and Air Tightness of Al Die-casting by Impregnation of Organic Solvent (유기용제 함침법을 통한 알루미늄 다이캐스팅의 미세결함 및 기밀성 평가)

  • Lee, Jin-Wook;Cho, Chang-hyun;Kim, Sung-Gye;Ko, Young-Gun;Kim, Dong-Ju
    • Journal of Korea Foundry Society
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    • v.42 no.4
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    • pp.218-225
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    • 2022
  • For hydrogen-vehicle applications (air pressure control valve housing, APCVH), an investigation was conducted to determine how micro-defects in a high- pressure die-casted Al alloy (industrial code: ALDC12) could be controlled by means of a post-treatment using an organic-based impregnation solution in order to improve the air- tightness of the die-casted Al sample. Two different impregnation solutions were proposed and its test results were compared to a imported product from Japan with respect to the processing variables used. A structural investigation of the components under study was conducted by means of computer tomography and 3D X-ray micro-CT. These observations revealed that the use of the impregnation treatment to seal micro-defects led to highly significant and beneficial changes which were attributed mainly to interconnections among inherent micro-pores. A leak test after impregnation revealed that the performance improvement rate of the die-casted Al sample was ~70% for INNO-01. Therefore, the developed impregnation solutions offer an effective strategy to control the micro-defects found in various vehicle parts via die-casting.

Leakage-free Rotating Seal Systems with Magnetic Nanofluids and Magnetic Composite Fluids Designed for Various Applications

  • Borbath, Tunde;Bica, Doina;Potencz, Iosif;Borbath, Istvan;Boros, Tibor;Vekas, Ladislau
    • International Journal of Fluid Machinery and Systems
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    • v.4 no.1
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    • pp.67-75
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    • 2011
  • Recent results are presented concerning the development of magnetofluidic leakage-free rotating seals for vacuum and high pressure gases, evidencing significant advantages compared to mechanical seals. The micro-pilot scale production of various types of magnetizable sealing fluids is shortly reviewed, in particular the main steps of the chemical synthesis of magnetic nanofluids and magnetic composite fluids with light hydrocarbon, mineral oil and synthetic oil carrier liquids. Design concepts and some constructive details of the magnetofluidic seals are discussed in order to obtain high sealing capacity. Different types of magnetofluidic sealing systems and applications are reviewed. Testing procedures and equipment are presented, as well as the sealing capabilities of different types of magnetizable fluids.

THE EFFECT OF INTRACANAL BASE ON PREVENTION OF APICAL LEAKAGE OF BLEACHING AGENTS (무수치 표백술에서 근관내 Base가 표백약제의 누출 방지에 미치는 영향)

  • Choi, Seung-Ho;Ro, Byeng-Duck;Park, Sung-Ho;Lee, Seung-Jong
    • Restorative Dentistry and Endodontics
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    • v.24 no.3
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    • pp.453-464
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    • 1999
  • The non-vital bleaching technique has been used widely as a very effective treatment method on discolored non-vital teeth. But periodontal tissue deterioration and cervical external root resorption have been reported because of the high toxicity of hydrogen peroxide in bleaching agents. So in previous studies, placement of base over the root canal obturation prior to bleaching has been suggested in order to prevent microleakage of bleaching agents, however, the effectiveness of base is still controversial. The purpose of this study was to evaluate the effects of base and root canal sealer on prevention of leakage of bleaching agents in non-vital bleaching. Fifty-two extracted sound teeth with single root were used. For root canal obturation, Tubuli seal$^{(R)}$(Kerr Co., USA) was used in 39 teeth and in others, AH-26$^{(R)}$(De Trey Dentsply, Inc., Switzerland) was used as a root canal sealer. 26 teeth among the teeth obturated with Tubuli seal$^{(R)}$ were divided into two groups, and Dentin cement$^{(R)}$(GC corp., Japan) and JRM$^{(R)}$(De Trey Dentsply, Inc. Germany) were used in each group as a intracanal base. In all teeth, non-vital bleaching using bleaching agent mixed with methylene blue dye was performed and all specimens were stored in $37^{\circ}C$ water bath for 72 hours. After sectioning longitudinally, the depth of dye leakage was measured with digital vernier calipers under the stereobinocular microscope using ${\times}40$ magnification. It can be concluded as follows: 1. The microleakage of bleaching agent was observed ill all groups regardless of type of the base and the sealer. 2. The microleakage in the groups using AH-26$^{(R)}$ as a sealer was significantly reduced (p<0.05). 3. In the groups with intracanal base, micro leakage was observed through almost the whole depth of the base and there was no significant difference between Dentin cement$^{(R)}$ and IRM$^{(R)}$ group(p>0.05). In conclusion, all the basing materials and the sealers in this study did not prevent the microleakage of bleaching agent. Therefore further studies and attempts to seal off the pulp chamber will be necessary.

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The Fabrication of SOB SOI Structures with Buried Cavity for Bulk Micro Machining Applications

  • Kim, Jae-Min;Lee, Jong-Chun;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.739-742
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    • 2002
  • This paper described on the fabrication of microstructures by DRIE(deep reactive ion etching). SOI(Si-on-insulator) electric devices with buried cavities are fabricated by SDB technology and electrochemical etch-stop. The cavity was fabricated the upper handling wafer by Si anisotropic etch technique. SDB process was performed to seal the fabricated cavity under vacuum condition at -760 mmHg. In the SDB process, captured air and moisture inside of the cavities were removed by making channels towards outside. After annealing($1000^{\circ}C$, 60 min.), The SDB SOI structure was thinned by electrochemical etch-stop. Finally, it was fabricated microstructures by DRIE as well as an accurate thickness control and a good flatness.

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Thermoplastic Fusion Bonding of UV Modified PMMA Microfluidic Devices (UV 개질된 PMMA 미세유체 장치의 열가소성 폴리머 용융 접합)

  • Park, Taehyun
    • Journal of the Korean Society for Precision Engineering
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    • v.31 no.5
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    • pp.441-449
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    • 2014
  • Thermoplastic fusion bonding is widely used to seal polymer microfluidic devices and optimal bonding protocol is required to obtain a successful bonding, strong bonding force without channel deformation. Besides, UV modification of the PMMA (poly-methyl methacrylate) is commonly used for chemical or biological application before the bonding process. However, study of thermal bonding for the UV modified PMMA was not reported yet. Unlike pristine PMMA, the optimal bonding parameters of the UV modified PMMA were $103^{\circ}C$, 71 kPa, and 35 minutes. A very low aspect ratio micro channel (AR=1:100, $20{\mu}m$ depth and $2000{\mu}m$ width) was successfully bonded (over 95%, n>100). Moreover, thermal bonding of multi stack PMMA chips was successfully demonstrated in this study. The results may applicable to fabricate a complex 3 dimensional microchannel networks.

Effect of Nd:YAG laser irradiation on adherence of retrograde filling materials: evaluation by micro-computed tomography

  • Kim, Minyoung;Kim, Hyeon-cheol;Kwak, Sang Won;Yoon, Tai Cheol;Kim, Euiseong
    • The Journal of the Korean dental association
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    • v.54 no.11
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    • pp.865-873
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    • 2016
  • Background/Purpose: The purpose of this study was to evaluate the effect of Nd:YAG irradiation on adherence of retrograde filling materials (mineral trioxide aggregate [MTA] and Super-EBA) by micro-computed tomography (CT) measurement and to observe the dentinal surface after irradiation by scanning electron microscopy (SEM). Materials and methods: Forty retrofilling models using extracted human teeth were divided into four groups according to the material and method used: ProRoot MTA (MTA group), Super-EBA (EBA group), MTA with Nd:YAG laser irradiation (LMTA group), and Super-EBA with Nd:YAG laser irradiation (LEBA group). All specimens were stored in 100% humidity for 24 hours until micro-CT was performed. The gap volume of the tooth/material interface was measured using the CTAn program. In six samples, the laser-irradiated dentin surface was observed using SEM. Results: The mean percent difference in gap volume was not statistically significant between the Nd:YAG laser-irradiated groups and non-irradiated in both materials(P > 0.05). The gap volume in the MTA group was significantly lower than that in the EBA group (P < 0.05). Examination of the non-irradiated specimens by SEM showed patent dentinal tubules. In contrast, alterations in the texture of the dentin surface and obliteration of the dentinal tubules were evident in the Nd:YAG laser-irradiated specimens. Conclusion: In this study, changes in the dentinal surface after Nd:YAG irradiation did not affect adherence between the apical filling material and the dentin wall.

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