• Journal of the Korean institute of surface engineering
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• v.32 no.3
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• pp.249-252
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• 1999

Boriding is one of the chemical method to increase surface hardness as well as carburizing, and nitriding. Gas boriding and boron paste boriding methods were investigated to replace salt bath boriding. Boron paste boriding method is selected due to safety, small waste and low cost. And then boriding is also carried out micro-pulsed PECVD in order to increase efficiency of boriding. Mechanical properties, microstructure, surface concentration, and depth profile of borided layer is investigated by micro-vickers hardness tester, SEM, XRD, and AES.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.20 no.10
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• pp.38-43
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• 2021

Photocurable hydrogels are widely used as 3D printing materials in tissue engineering (e.g., scaffold fabrication) as well as optical fibers (or optical sensors) materials. Photocurable hydrogels can control optical and mechanical properties such as chemical or fabrication conditions. In previous research, we introduced a new 3D printing method to fabricate a freestanding overhanging hydrogel structure without supporting structure. This study was measured and analyzed the difference of the mechanical properties of the photocurable hydrogel according to the light intensity using a micro tensile tester. In practically, it was difficult to perform a direct tensile test on a micro (less than 1 mm) size fiber. In this study, the tensile test of the hydrogel fibers could be measured simply and repeatedly using a paper carrier.

• Journal of the Korean institute of surface engineering
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• v.42 no.4
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• pp.179-185
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• 2009

Diamond-like carbon(DLC) films were deposited by linear ion source(LIS)-physical vapor deposition method changing the anode voltages from 800 V to 1800 V, and characteristics of the films were investigated using residual stress tester, nano-indentation, micro raman spectroscopy, scratch tester and Field Emission Scanning Electron Microscope(FE-SEM). The results showed that the residual stress and hardness increased with increasing the ion energy up to anode voltage of 1400 V. It was also found that the content of $SP^3$ carbon increased with increasing the anode voltage $SP^3/SP^2$ ratio through investigation of $SP^3/SP^2$ ratio by the micro-raman analysis. From these results, it can be concluded that the physical properties of DLC films such as residual stress and hardness are increased with increasing the anode voltage. These results can be explained that 3-dimensional cross-links between carbon atoms and Dangling bond are enhanced and the internal compressive stress also increased with increasing the anode voltage. The optimal anode voltage is considered to be around 1400 V in these experimental conditions.

• Tribology and Lubricants
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• v.22 no.5
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• pp.237-242
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• 2006

Surfaces found in nature, including biological surfaces have been providing inspiration to modify/fabricate artificial surfaces as solutions for tribological applications. As an example, the concept of 'lotus-effect' has motivated tribologists world wide to modify/fabricate surfaces for enhanced tribological performance. These was done by creating nano/micro-scale asperities on various surfaces using ion beam milling and ion-beam assisted roughening. In order to understand the attributes of natural surfaces, which are inspirational to tribologists, we characterized the surface of two natural surfaces-Nelumbo nucifera (lotus) and Colocasia esculenta leaves. Further, we evaluated their micro-scale friction property, both in their fresh and dried conditions. The characterization of surfaces was conducted using a confocal microscope and SEM, which involved the evaluation of size and distribution of protuberances. The micro-scale friction property was evaluated using a ball-on-flat type micro-tribo tester, under reciprocating motion. A soda lime glass ball (2 mm diameter) was used in these tests. Tests were conducted at the applied normal load of $3000{\mu}N$, at a sliding speed of 1 mm/sec for a scan length of 3 mm. All experiments were conducted at ambient temperature ($24{\pm}1^{\circ}C}$) and relative humidity ($45{\pm}5%$). It was observed that the friction behaviour of the natural surfaces was influenced by their surface characteristics (morphology and distribution of protuberances) and also by the condition (fresh or dried) in which they were tested.

• Journal of the Korean institute of surface engineering
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• v.31 no.6
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• pp.359-370
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• 1998

TiAl-based intermetallic compounds were electro-bornizel in the mixture of $Na_2B_4O_7$, KCL and LiCl in the termetature rage between 850 and $1000^{\circ}C$for various times (1-5 hours)under the fixed current density of 0.5 A/$cm^2$. The optimized composition of electrolyte in this work was decided to be 76.9 wt% $Na_2B_4O_7$-19.2 wt.%(0.7KCl-0.3LiCl) -3.9 wt.% al. The samples with boronized layer were investigated by SEM, XRD and EDS. The surface micro-hardness of boronized TiAl was also evaluated using Micro Vickers Hardness Tester. The sample, boronized at $900^{\circ}C$ for 4 hours in the above composition of electrolyte under the current density of 0.5 A/$\textrm{cm}^2$, has about 36$\mu\textrm{m}$ think layer on the surface, and its surface micro-hardness was measured to be 1263 Hv. From the results of SEM, XRD and EDS, the layer consisted of $TiB_2$ sublayer and Al-oxide sub layer. Al-depleted layer below the Al-oxide sudlayer was also detected. The activation energy for formation of boronized layer in this study was calculated as 178 Kcal/moleK.

• Journal of Korean Society of Industrial and Systems Engineering
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• v.36 no.2
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• pp.1-7
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• 2013

Cleanroom could be largely classified into industrial cleanroom that can be contaminated by particles and bio-cleanroom that can be contaminated by biological particles. Electrical manufacturing companies producing precision machines and electrical parts essentially have industrial cloom facilities and clean technologies to produce defects free products due to particles. Industrial cleanroom should be controlled in respect of 4M1E to prevent from foreign materials of sub-micro unit and to keep out contamination sources from outside. In this paper, a concept for a quantitative methodology to measure the particles from running components was suggested by combining both newly making clean booth such as wear tester and laser particle counter.

• Korean Journal of Materials Research
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• v.28 no.4
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• pp.221-226
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• 2018

The property changes of 18, 14, and 8K green gold alloys for jewelry are observed by adding 0.0, 3.0, and 5.0 wt% of indium (In), respectively. To check the composition of the alloys, an energy dispersive spectroscopy (EDS) analysis is conducted. Color and microstructure analysis is executed through bare-eye, macro camera, UV-VIS-NIR-colormeter, and optical microscope. The melting point, wetting angle, and hardness are measured using TGA-DTA, a wetting angle tester, and a Vickers hardness tester. The EDS analysis result demonstrates that each of the green gold alloys was manufactured with purposed contents. The color analysis result shows that the color of the alloys is similar to the color of the conventional 4 wt%-Cd 18K green gold, and the green color improves as the In content increases. The micro structure analysis result demonstrates that grain refinement improves as the amount of In increases. Enhancements in the melting point, wettability, and Vickers hardness changes appear as the In content increases and Au content decreases. The hardness is up to 260, which implies good durability. Therefore, the results suggest that the proposed 18, 14, and 8K In-added green gold alloys enhance the properties of jewelry products with regard to the green color, castability, and durability.

• Journal of the Korean institute of surface engineering
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• v.44 no.2
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• pp.55-59
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• 2011

In this study, the mechanical properties of boronized 316L austenitic stainless steel have been investigated. Boronizing was carried out in solid medium consisting of Ekabor powder at $900^{\circ}C$ and $1000^{\circ}C$ for 2, 4 and 8 hours, respectively. The properties of sample were analyzed by field emission scanning electron microscope, X-ray diffractometer, Glow discharge spectrometer, micro-hardness tester and ball-on-disk wear tester. Increasing the boronizing time and temperature, the hardness of boronized samples were shown over Hv 2000 and the thickness of boride layers were also increased linearly. XRD patterns of samples were revealed the presence of borides such as FeB, $Fe_2B$, CrB, $Cr_2B$ and $Ni_3B$. Friction coefficient of boronized STS 316L was shown the low value at $900^{\circ}C$ for 8 hours and $1000^{\circ}C$ for 4 hours, respectively.

• Journal of the Korean institute of surface engineering
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• v.42 no.4
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• pp.173-178
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• 2009

DLC film was synthesized on plastic injection mold(SKD11, $30\;mm\;{\times}\;19\;mm\;{\times}\;0.5\;mm$) and Si(100) wafer for 2 h at $130^{\circ}C$ under 6 mTorr using hybrid method of rf sputtering and ion source. The obtained film was analysed by Raman spectroscopy, AFM, TEM, Nano indenter and scratch tester, etc. The film was defined as an amorphous phase. In the Raman spectrum, broad peak of $sp^2$-bonded carbon attributed to graphite at $1550\;cm^{-1}$ were observed, and the ratio of ID($sp^3$ diamond intensity)/IG($sp^2$ graphite intensity) was approximately 0.54. The adhesion of DLC film was more than 80 N with scratch tester when $0.2\;{\mu}m$ thickness Cr was coated as interlayer. The micro-hardness was distributed at 35~37 GPa. The friction coefficient was 0.02~0.07, and surface roughness(Ra) was 0.34~1.64 nm. The lifetime of DLC coated plastic injection mold using as a connector part in computer was more than 2 times of non-coated mold.

• Transactions of The Korea Fluid Power Systems Society
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• v.3 no.4
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• pp.21-28
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• 2006

The proportional control solenoid valves as well as the PWM solenoid valves operated by electric signal play an important role in the hydraulic system for automatic transmissions to improve the shift quality. However it is not generally available for the performance data because most of the automotive parts manufacturer don't release the specific test results, especially dynamic performance that is essential to design a shift control algorithm. In this research, a performance test equipment that can be applied to various types of pressure control solenoid valve was developed. It was implemented by 8-bit micro-controller with many useful functions such as adjustable PWM carrier frequency, embedded function generator, current controller, data monitoring and acquisitions, etc. for the test of dynamic performance of solenoid valve as well as the steady-state pressure characteristics. The performance test results for the direct type proportional control solenoid valve show not only the validity of overall functions but also its usefulness as a hydraulic valve tester.