• Korean Journal of Metals and Materials
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• v.50 no.4
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• pp.316-323
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• 2012

The aim of this study is to investigate the effect of post heat treatment on bonding properties of roll cladded Ti/MS/Ti materials. First grade Ti sheets and SPCC mild steel sheets were prepared and then Ti/MS/Ti clad materials were fabricated by a cold rolling and post heat treatment process. Microstructure and point analysis of the Ti/MS interfaces were performed using the SEM and EDX Analyser. Diffusion bonding was observed at the interfaces of Ti/MS. The thickness of the diffusion layer increased with post heat treatment temperature and the diffusion layer was verified as having $({\epsilon}+{\zeta})+({\zeta}+{\beta}-Ti)$ intermetallic compounds at $700^{\circ}C$ and an $({\zeta}+{\beta}-Ti)$ intermetallic compound at $800^{\circ}C$, respectively. The micro Knoop hardness of mild steel decreased with post heat treatment temperature; however, those of Ti decreased at a range of $500{\sim}600^{\circ}C$ and showed a uniform value until $800^{\circ}C$ and then increased rapidly up to $900^{\circ}C$. The micro Knoop hardness value of the diffusion layer increased up to $700^{\circ}C$ and then saturated with post heat treatment. A T-type peel test was used to estimate the bonding forces of Ti/Mild steel interfaces. The bonding forces decreased up to $800^{\circ}C$ and then increased slightly with post heat treatment. The optimized temperature ranges for post heat treatment were $500{\sim}600^{\circ}C$ to obtain the proper formability for an additional plastic deformation process.

• The Journal of Advanced Prosthodontics
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• v.1 no.3
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• pp.113-117
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• 2009

STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

• Korean Institute of Interior Design Journal
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• v.22 no.6
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• pp.3-10
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• 2013

This study intends to clarify the key elements of designing low energy residential building construction by planning out residential construction in nature oriented designing method utilizing nearby environment and nature oriented energy from designing stage instead of construction of low energy residential building. Development of building technology is proportional to the development of technology that lasts already. However, what is no less important than the advancement of technology, it is the study of fundamental phenomena energy use in response to climate, reduction, such as recycling. It is possible in such a purpose, it is assumed that there is a need to study elements implementation plan in accordance with the climatic characteristics of the study. Method for controlling the condition solar radiation, sunshine, depending on the characteristics of the weather, by utilizing the convection phenomenon of nature, to maintain the air comfort in the interior space is the essence of eco-friendly construction and passive Property This is an important architectural elements to be aim. For through the analysis of this case, corresponding to the phenomenon of the features of the macro climate and micro climate due to climate change, a combination building blocks of classification placement of each, shape, structure, elevation, space, of the material appeared in various it was possible to know the construction characteristics were. As shown in each case, construction method to address climate change has been found to apply to a comprehensive analysis climatic characteristics of each region, in response to this, the construction of element each corresponding.

• Journal of the Institute of Electronics Engineers of Korea SD
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• v.46 no.8
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• pp.6-11
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• 2009

The electro-optical characteristics of the Liquid Crystal on Silicon (hereinafter "LCOS") micro-display on vertically alignment (VA) mode were studied with 3-dimensional LC code. 5 different cell gaps, such as 1.4 ${\mu}m$, 1.8 ${\mu}m$, 2.1 ${\mu}m$, 2.4 ${\mu}m$ and 2.8 ${\mu}m$, were selected. The reflectance-voltage (R-V) characteristics, distribution of reflected light, reflectance, optical fill factor and contrast ratio were calculated and investigated depending on various cell gaps. Due to the surface anchoring effect, higher cell gap showed higher reflectance. However, considering the optical fill factor and contrast ratio, middle-height 2.1 ${\mu}m$ showed the best electro-optical characteristic. 0.7 inch Full-HD LCOS panels having same geometry and material property were fabricated. The reflected light intensity and contrast ratio were measured and the measured results were well-matched to the calculated results.

• Transactions of Materials Processing
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• v.20 no.2
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• pp.140-145
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• 2011

The aim of the present study is to derive optimized post heat treatment temperatures to get a proper formability for Ti/STS409L/Ti clad materials. These clad materials were fabricated by cold rolling followed by a post heat treatment process for 10 minutes at temperatures ranging from $500^{\circ}C$ to $850^{\circ}C$. The microstructure of the interface was observed using a Scanning Electron Microscope(SEM) and an Energy Dispersive X-ray Analyser(EDX) in order to investigate the effects of post heat treatment on the bonding properties of the Ti/STS409L/Ti clad materials. Diffusion bonding was observed at the interfaces with a diffusion layer thickness increasing with the post heat treatment temperature. The diffusion layer was composed of a type of(${\varepsilon}+{\zeta}$) intermetallic compound containing additional elements, namely, Fe, Ti and Ni. The micro Knoop hardness of the Ti/STS409L interfaces was found to increase with heat treatment up to $800^{\circ}C$ and then decrease for temperatures rising up to $850^{\circ}C$. The tensile strength was shown to decrease for heat treatment temperature increasing to $750^{\circ}C$ and then increase rapidly for temperature rising up to $850^{\circ}C$. A post heat treatment temperature range of $700{\sim}750^{\circ}C$ was found to optimize the formability of Ti/STS409L/Ti clad materials.

• Progress in Superconductivity
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• v.6 no.1
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• pp.64-68
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• 2004

We fabricated cube-textured Ni and Ni-W alloy substrates for coated conductors and characterized the effects of W addition on microstructure, mechanical strength, and magnetic properties of the substrate. Pure Ni and Ni-(2, 3, 5at.%)W alloys were prepared by plasma arc melting, heavily cold rolled and then annealed at various temperatures of $600-1300^{\circ}C$. The texture was evaluated by pole-figure and orientation distribution function (ODF) analysis. Mechanical properties were investigated by micro Vickers hardness and tension test. Ferromagnetism of the substrate was measured by physical property measurement system (PPMS). It was observed that Ni-W substrates had sharp cube texture, and the full-width at half-maximums (FWHMs) of in-plane texture was $^{\circ}$-5.57$4.42^{\circ}$, which is better than that of pure Ni substrate. In addition cube texture of Ni-W substrates was retained at higher temperature up to $1300^{\circ}C$. Microstructural observation showed that the Ni-W substrates had fine grain size and higher mechanical properties than the pure Ni substrate. These improvements are probably due to strengthening mechanisms such as solid solution hardening and/or grain size strengthening. PPMS analysis showed that addition of W effectively reduced saturation magnetization in applied magnetic field and Curie temperature.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.8
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• pp.851-856
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• 2012

The design process of a micro-probe tip is very complicated and expensive. To avoid these problems, in this study, we used element (FE) analysis. To simplify design process. A new pre-probe tip (cobra-needle type) made of Ni and Co was designed by FE analysis. Experimental results were compared with those obtained by FE analysis to verify the reliability of the analysis. The contact force and over drive were respectively found to be 12.5 gf(Contact Force) and $100{\mu}m$(Over drive). We propose the new designed probe tip. Material of new designed probe tip is NiCo. Values of Property are 1~2 gf(Contact Force) and $100{\mu}m$(Over drive).

• Journal of the Korean Society for Nondestructive Testing
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• v.20 no.5
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• pp.390-396
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• 2000

The dynamic elastic constants of the simulated weld HAZ (heat-affected zone) of SA 508 Class 3 reactor pressure vessel (RPV) steel were investigated by resonant ultrasound spectroscopy (RUS). The resonance frequencies of rectangular parallelepiped samples woe calculated from the initial estimates of elastic stiffness $c_{11},\;c_{12}\;and\;c_{44}$ with an assumption of isotropic property, dimension and density. Through the comparison of calculated resonant frequencies with the measured resonant frequencies by RUS, very accurate elastic constants of SA 508 Class 3 steel were determined by iteration and convergence processes. Clear differences of Youngs modulus and shear modulus were shown from samples with different thermal cycles and microstructures. Youngs modulus and shear modulus of samples with fine-grained bainite were higher than those with coarse-grained tempered martensite. This tendency was confirmed from other results such as micro-hardness test.

• Journal of Aerospace System Engineering
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• v.12 no.5
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• pp.1-7
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• 2018

In this study, we proposed a high frequency induction hardening analysis method based on electromagnetic-thermal co-simulation. In the high frequency induction heating analysis, the results of the finite element analysis (FEA) (considering the change of the material property and the cooling factor according to the temperature) and those of the high frequency induction hardening experiment (using the S45C specimen) were compared. The hardness of the S45C specimens was measured using the micro Vickers hardness test to determine the depth of hardening. The measurement results were then compared with the results of FEA. The result of high frequency induction heating analysis showed that the temperature was more than $750^{\circ}C$, which is the A2 transformation point of S45C, while the temperature during quenching was below $200^{\circ}C$. The results showed that the difference of the depth of hardening between the FEA and the experiment is 0.2mm.

• Nuclear Engineering and Technology
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• v.48 no.1
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• pp.164-168
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• 2016

Lean duplex stainless steels with 0.087 wt.% gadolinium (Gd) were inert arc-melted and cast in molds of size $10mm{\times}10mm{\times}20mm$. The micro-hardnesses of the rolling direction (RD), transverse direction (TD) and short transverse (ST) direction were $258.5H_V$, $292.3H_V$, and $314.7H_V$, respectively. A 33% cold rolled specimen had the crystallographic texture that (100) pole was mainly concentrated to the normal direction (ND) and (110) pole was concentrated in the center of ND and RD. The corrosion potential and corrosion rate in artificial seawater and $0.1M\;H_2SO_4$ solution were in the range of $105.6-221.6mV_{SHE}$, $0.59-1.06mA/cm^2$, and $4.75-8.25mV_{SHE}$, $0.69-1.68mA/cm^2$, respectively. The friction coefficient and wear loss of the 0.087 w/o Gd-lean duplex stainless steels in artificial seawater were about 67% and 65% lower than in air, whereas the wear efficiency was 22% higher. The corrosion and wear behaviors of the 0.087 w/o Gd-lean duplex stainless steels significantly depended on the Gd phases.