• Title/Summary/Keyword: Melting method

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Coating Effect of Low Temperature Melting Bi-Sn Metalized Wood Composites on 10 Different Korean Wood Species (주요 국산재 10가지 수종에 대한 Bi-Sn 저온용융 합금주입 목재복합체의 도장 효과)

  • Park, Kye-Shin;Seo, In Soo;Lee, Hwa Hyoung;Kang, Seog Goo
    • Journal of the Korea Furniture Society
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    • v.25 no.3
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    • pp.223-232
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    • 2014
  • To make metalized wood composites of 10 different korean wood species, it was tested by Low temperature melting Bi-Sn alloy injection method at high temperature and high pressure condition. Metalized wood composite of each wood species had light ash color, but still maintained its own natural wood grain and wood figures. It was evaluated on coating properties. Furthermore, it also was check on effect of coating as like a changes of main color, wood grain and wood figures. The results of test were following as; a coating properties as like a cold resistance, heat resistance, acid resistance, alkali resistance, durability of abrasion, and cross-cut test was proper on the conditions of the KS standard. And, In aspect of color changes, the metalized wood composites of 10 different korean wood species had a light ash color, but still maintained its own natural wood grain and wood figures. Also, the more weight per gain of alloy is, the more grey background of metalized wood composite is.

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The Effect of Processing Parameters on HTS Tube Characteristics

  • Jung, Sengho;Jang, Guneik;Ha, Dongwoo;Sung, Taehyun
    • Transactions on Electrical and Electronic Materials
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    • v.5 no.2
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    • pp.55-60
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    • 2004
  • High-temperature Superconductor(HTS) tubes were fabricated in terms of different chemical compositions and various SrSO$_4$additions by centrifugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were 1050$^{\circ}C$, 1100$^{\circ}C$ and 550$^{\circ}C$ for 30 min, respectively. The mould rotating speed was 1000 rpm. A tube was annealed at 840$^{\circ}C$ for 72 hours in oxygen atmosphere. The plates like grains more than 20 $\mu\textrm{m}$ were well developed along the rotating direction of mould regardless of initial chemical compositions and the amounts of SrSO$_4$in Bi2212. The specimen with Bi2212 composition exhibited T$\_$c/ of 83 K, while the specimens fabricated with other compositions are lower than 60 K. The measured I$\_$c/ and J$\_$c/ at 77 K(B = 0 T) in Bi2212 with 7 % SrSO$_4$ composition were about 680 A and 380 A/$\textrm{cm}^2$.

Fabrication of Bi-2212/$SrSO_4$ Composite Superconductors by Melting Powder Mixtures

  • Kim, Kyu-Tae;Jang, Seok-Hern;Lim, Jun-Hyung;Park, Eui-Cheol;Joo, Jin-Ho;Lee, Hoo-Jeong;Hong, Gye-Won;Kim, Chan-Joong;Kim, Hye-Rim;Hyun, Ok-Bae
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1245-1246
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    • 2006
  • We fabricated Bi-2212/$SrSO_4$ composite superconductors and evaluated the effects of the powder mixing method and melting temperature on their microstructure and superconducting properties. The Bi-2212 powders were mixed with $SrSO_4$ by hand-mixing (HM) and planetary ball milling (PBM) and then the powder mixtures were melted at $1100^{\circ}C{\sim}1200^{\circ}C$, solidified, and annealed. We found that the powder mixture prepared by PBM was finer and more homogeneously mixed than that prepared by HM, resulting in more homogeneous microstructure and smaller $SrSO_4$ and second phases after annealing.

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Properties, Structure and Crystallization of Poly Lactic Acid/Zinc Oxide Pillared Organic Saponite Nanocomposites (폴리락틱산/산화아연 기둥구조의 유기사포나이트 나노복합체의 특성, 구조 및 결정화)

  • Zhen, Weijun;Sun, Jinlu
    • Polymer(Korea)
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    • v.38 no.3
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    • pp.299-306
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    • 2014
  • ZnO pillared saponite was synthesized via a microwave hydrolysis method. To enhance interfacial compatibility between zinc oxide (ZnO) pillared saponite and poly lactic acid (PLA), ZnO pillared organic saponite was prepared by intercalation modification of cetyltrimethylammonium bromide. Moreover, PLA/ZnO pillared organic saponite nanocomposites were prepared by melting processing. The microstructure analysis of PLA/ZnO pillared organic saponite nanocomposites showed that ZnO pillared organic saponite was exfoliated and homogeneouslydispersed in PLA matrix. The property results showed that ZnO pillared organic saponite improved the mechanical properties and thermal stabilities of PLA/ZnO pillared organic saponite nanocomposites. Differential scanning calorimetry (DSC) demonstrated that ZnO pillared organic saponite restrained the appearance of cold crystallization, lowered the glass transition temperature and melting temperature of PLA, and improved the crystallinity of PLA. The results demonstrated that ZnO pillared organic saponite had a good interfacial compatibility and heterogeneous nucleation effect in PLA matrix, and also played an active role in accelerating the crystallization process of PLA.

Micro-defects in $LiNbO_3$ single crystals with congruent melting composition (조화용융성조성을 가진 $LiNbO_3$ 단결성의 미소결함)

  • 김현기;권달회;이선우;심광보;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.3
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    • pp.267-272
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    • 1999
  • Micro-defects in the undoped and MgO-doped $LiNbO_3$ single crystals, which were grown from a congruent melting composition (48.6 mol% $Li_2$O) by the CZ (Czochralski) method, were analyzed using microscopic techniques such as optical microscopy (OM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Effects of the dopant and g value (the fraction solidfied) on the domain structure and micro-defect were investigated to build a corelationship with a growth condition of crystal. It was observed that the micro-defect concentrated near the domain wall is caused by high stress. Especially, the micro-defect was observed to be biased toward a certain side of the domain wall.

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Electrical Characteristics of HIS Tube Depending on Processing Parameters (공정변수에 따른 초전도 튜브의 전기적 특성)

  • Park, Chi-Wan;Jang, Gun-Eik;Ha, Dong-Woo;Seung, Tae-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.5
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    • pp.468-472
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    • 2005
  • High-temperature Superconductor(HTS) tubes were fabricated in term of different processing variables such as preheating temperature, speed of mold rotation and cooling rate by centrigugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were $1050{\circ}C{\sim}1100{\circ}C\;and\;550{\circ}C\;for\;30\; min$, respectively The mould roating speed was 1000 rpm. A tube was annealed at $840 {\circ}C$ for 72 hours in oxygen atmosphere. The plate-like grains were well developed along the loafing direction and typical grain size was about more than $40{\mu}$. It was found that Ic values increased with increasing the Preheating temperature and speed of mold rotation. While Ic decreased with increasing the cooling rate. The measured Ic in $50mm{\times}70mm{\times}2.5mm$ tube was about 896 Amp.

Optical process of polysilicaon on insulator and its electrical characteristics (절연체위의 다결정실리콘 재결정화 공정최적화와 그 전기적 특성 연구)

  • 윤석범;오환술
    • Electrical & Electronic Materials
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    • v.7 no.4
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    • pp.331-340
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    • 1994
  • Polysilicon on insulator has been recrystallized by zone melting recrystallization method with graphite strip heaters. Experiments are performed with non-seed SOI structures. When the capping layer thickness of Si$\_$3/N$\_$4//SiO$\_$2/ is 2.0.mu.m, grain boundaries are about 120.mu.m spacing and protrusions reduced. After the seed SOI films are annealed at 1100.deg. C in NH$\_$3/ ambient for 3 hours, the recrystallized silicon surface has convex shape. After ZMR process, the tensile stress is 2.49*10$\^$9/dyn/cm$\^$2/ and 3.74*10$\^$9/dyn/cm$\^$2/ in the seed edge and seed center regions. The phenomenon of convex shape and tensile stress difference are completely eliminated by using the PSG/SiO$\_$2/ capping layer. The characterization of SOI films are showed that the SOI films are improved in wetting properties. N channel SOI MOSFET has been fabricated to investigate the electrical characteristics of the recrystallized SOI films. In the 0.7.mu.m thickness SOI MOSFET, kink effects due to the floating substrate occur and the electron mobility was calculated from the measured g$\_$m/ characteristics, which is about 589cm$\^$2//V.s. The recrystallized SOI films are shown to be a good single crystal silicon.

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A Study on the Fiber Laser welding of Ultra-Low Carbon Interstitial Free Steel for Automotive (자동차용 무침입형 극저탄소강의 파이버 레이저 용접에 대한 연구)

  • Oh, Yong-Seok;Shin, Ho-Jun;Yang, Yun-Seok;Hwang, Chan-Youn;Yoo, Young-Tae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.3
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    • pp.342-349
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    • 2011
  • The purpose of this paper is to describe experimental results about the butt welding and bead on plate welding of the high power Continuous Wave (CW) Fiber laser for Ultra-low carbon Interstitial Free(IF) steel plate for gear part of car. After being welded of the gear parts by the fiber laser and electron beam Microstructures of melting zone had been mixed acicular, granular bainitic, quasi-polygonal and widmanstatten ferrite because of a radical thermal diffusion after welding, difference of critical volume and grain size. As a result of experiment, when gear parts were welded by the fiber laser and electron beam, the fiber laser welding has been stable properties without internal defects more than the electron beam welding. Therefore it has the very advantages of welding high quality and productivity more than conventional melting method. The optimal welding processing parameters for gear parts were as follows : the laser power and welding speed were 3kWatt, 30mm/sec respectively. At this time heat input was $21.2{\times}10^3J/cm^2$.

Rapid Fabrication of Bi2212 Superconducting Films on Cu Tape with Cu-free Precursor (Cu-free 전구체를 이용한 동 테이프 위의 Bi2212 초전도 후막의 급속 제조)

  • 한상철;성태현;한영희;이준성;김상준
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.11a
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    • pp.69-72
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    • 1999
  • A Well oriented Bi$_2$re$_2$CaCu$_2$O$\sub$8/(Bi2212) superconductor thick films were formed successfully on a copper substrate by liquid reaction between a Cu-free precursor and Cu tape using method in which Cu-free BSCO powder mixture was printed on copper plate and heat-treated. And we examined the mechanism for the rapid formation of Bi2212 superconducting films from observing the surface microstructure with heat-treatment time. At heat-treatment temperature, the printing layer partially melt by reacting with CuO of the oxidizing copper plate, and the nonsuperconducting phases present in the melt are typically Bi-free phases and Cu-free phases. Following the partial melting, the Bi$_2$Sr$_2$CaCu$_2$O$\sub$8/ superconducting phase is formed at Bi-free phase/liquid interface by nucleation and grows. It was confirmed that the phase colony from the phase diagram of Bi$_2$O$_3$-(SrO+CaO)/2-CuO system is similar to the observed result.

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YBCO Bulk Superconductors Prepared by Solid-liquid Melt Growth (고액용융성장법을 이용한 YBCO 단결정 제조)

  • Han, Sang-Chul;Lee, Jeong-Phil;Park, Byeong-Cheol;Jeong, Neyon-Ho;Park, Byung-Jun;Jung, Se-Yong;Han, Young-Hee;Sung, Tae-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.22 no.10
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    • pp.860-863
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    • 2009
  • YBCO bulks with fine $Y_2BaCuO_5$(Y211) particles have been prepared by the top-seed modified powder melting process method, Solid-Liquid Melt Growth(SLMG), with $Y_2O_3$, $BaCuO_2$ and CuO mixing precursor. By using $Y_2O_3$ instead of $Y_2BaCuO_5$ as precursor, the processing became to be simpler and cheaper than the current powder melting process. The microstructures, trapped field and critical current density of the various conditioned YBCO bulks have been analyzed and the effect of Pt additive was studied. The different trapped magnetic field values of the several samples have been explained in the viewpoint of their microstructures. The fabrication of large-sized YBCO single domain has been conducted.