• Title/Summary/Keyword: Measuring control standard

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Uncertainty Evaluation of the Analysis of Methamphetamine and Amphetamine in Human Hair by GC/MS (GC/MS를 이용한 모발 중 메스암페타민 및 암페타민 분석의 측정불확도 평가)

  • Kim, Jin-Young;Kim, Jong-Sang;Kim, Min-Kyoung;Lee, Jae-Il;Suh, Yong-Jun;In, Moon-kyo
    • YAKHAK HOEJI
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    • v.51 no.3
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    • pp.206-213
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    • 2007
  • Recently estimating the uncertainty of an analytical result has become an essential part of quantitative analysis. This study describes the uncertainty of the measurement for the determination of methamphetamine and its major metabolite amphetamine in human hair, The method consists of washing, drying, weighing, incubation and extraction with methanolic HCI solution, clean-up, trifluoroacetyl derivatization, and qualification/quantification of residues by gas chromatography/mass spectrometry (GC/MS). Traceability of measurement was established through traceable standards and calibrated volumetric equipment and measuring instruments. Measurement uncertainty associated with each analyte in real samples was estimated using quality control (QC) data. The main source of combined standard uncertainty comprised two components, which are uncertainties associated with calibration linearity and variations in QC, while those associated with preparation of analytical standards and sample weighing were not so important considering the degree of contribution. Relative combined standard uncertainties associated with the described method ranged for individual analytes from 4.99 to5.03%.

Equipment Development for Inorganic-Compound Concentration Measurement in a Hydroponic Culture Solution (수경배양액 무기성분농도 측정장치 개발)

  • Heo, Jeong-Wook;Park, Kyeong-Hun;Hong, Seung-Gil;Lee, Jae-Su;Baek, Jeong-Hyun;Park, Jong-Taek;Lee, Seung-Kee
    • Korean Journal of Environmental Agriculture
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    • v.39 no.4
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    • pp.319-326
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    • 2020
  • BACKGROUND: Measurement equipment was developed for inorganic nutrient concentration inside the hydroponic culture medium with several macro- and micro compositions, and applied for measuring the compositions of conventional medium. METHODS AND RESULTS: Before the equipment development, sonicator and heater were utilized to control temperature around of the module mixing with color reagents and target samples among the inorganic compositions. The measurement module and multi-sampler were also manufactured based on the COMS (Complementary Metal-Oxide Semiconductor) and installed inside the measurement equipment. Concentration of standard solution, value measured by the equipment, standard deviation or measured average value were used for estimating the accuracy and average recall of the equipment. Yamazaki solutions with EC of 0.5, 1.5, and 2.5 dS/m were offered to confirm the equipment accuracy and standard error. CONCLUSION: It was suggested that the developed equipment could be automatically applied for measurement with accuracy of over 96% and standard errors of less than 5% on 12 macro- and micro compositions such as a NO3-N, PO43- or Fe.

Case Study on the Evaluation of Capture Velocity of Local Exhaust Ventilation System in a Laboratory (연구 실험실 내 국소배기장치의 제어풍속 평가 사례)

  • Daesung Lim
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.34 no.3
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    • pp.189-192
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    • 2024
  • Objectives: To protect researchers using chemicals, it is necessary to monitor whether the working environment is well managed through the performance evaluation of the local exhaust system in the research laboratory. These results need to be reflected in the work environment management policy of research laboratories in the future. Methods: By measuring the capture velocities of fume hoods and arm hoods, which are the most commonly used local exhaust systems in research laboratories in a domestic research institute, we tried to confirm the degree to which the actual capture velocity values and legal standards were satisfied. The capture velocities were measured using a hot wire wind speedometer (TSI 9565-P, USA, 2016 with all exhaust systems in operation in the laboratory. As for the measurement position for each local exhaust system, in the case of the fume hood, the wind speed in the center of the opening surface was measured after opening 50% of the door of the hood. For the arm hood the capture velocities were measured at a distance of 10 cm vertically from the opening surface of the hood Conclusions: The total number of arm hoods measured was 546, and the average capture velocity was 0.61 m/sec with an S.D of 0.49. Among them, 99 satisfied the capture velocity standard of 1m/sec, meaning only 18.1% of the total satisfied with the standard. The total number of fume hoods measured was 625, and the average control wind speed was 0.48 m/sec with an S.D. of 0.17. Among them, the number of fume hoods that satisfied the capture velocity standard of 0.4 m/sec was 518, meaning 82.9% of the total satisfied the standard. Therefore, research institutes that operate local exhaust systems to protect researchers from chemicals should further strengthen the capture velocity management of hoods, and government agencies need to reflect this in work environment management policies based on further evaluation results.

Exploratory approach to measuring facility performance in public service facilities (공공서비스시설에서의 시설성능 요인에 대한 탐색적 연구)

  • Lee, So-Young;Shin, Hee-Young
    • Proceeding of Spring/Autumn Annual Conference of KHA
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    • 2009.04a
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    • pp.284-287
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    • 2009
  • In order to plan and manage public facilities effectively and efficiently, it is necessary to diagnose the current status of facilities and decide the objective features. Performance measurement is to provide managers with the information they need to measure competitive advantages. This paper discusses public facility performance in order to establish the conceptual framework for performance measurement for public facilities. In order to develop the measurement of public facility performance, a pilot study was conducted with facilities managers of facilities management corporation of public districts in Seoul. We investigated how public facilities management teams have assessed their performance and collected data regarding financial aspects, service aspects, community aspects, and building aspects. There is no standard format to measure facility performance since building sizes, programs, community needs widely differ. However, it is necessary to have a more consistent system to measure facility performance. In addition, each public municipal district needs to empower each district facilities management corporation to participate in managerial decisions and budget control.

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Remote Measurement of ECU Self-Diagnostic Signal based on the Windows CE

  • Lee, Seong-Cheol;Yun, Yeo-Hung;Se, Ji-Won;Kwon, Tae-Kyu;Lee, Young-Chun;Jang, Bong-Choon
    • 제어로봇시스템학회:학술대회논문집
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    • 2002.10a
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    • pp.68.2-68
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    • 2002
  • The purpose of this paper is to monitor ECU's self-diagnostic signal without wire. In order to measure the ECU's self-diagnostic signal, the interfaced circuit is developed to communicate ECU with a designed display terminal according to the ISO, SAE regulation of communication protocol standard. An 80C196KC processor is used for communicating ECU's self-diagnostic signal and communication data are sent to PDA monitoring system that is based on the Windows CE. Software on PDA is developed to monitor the ECU's self-diagnostic signal in which RS232 port is programmed by half duplex method. The algorithms for measuring the ECU's self-diagnostic signals are verified to mo...

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A Study of Korean (Industrial) Standards for Pneumatic Servo Valve (공압서보밸브 KS규격 정립에 관한 연구)

  • 김동수;이원희;최병오
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1231-1234
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    • 2003
  • Pneumatic servo valve which is widely applied in industrial world is advanced technology compounded with electric, electronic and machine. And It is consist of Linear Force Motor. Spool Commutation Mechanism and Microprocessor. In this study, we accomplished test method of Linear Force motor test, Static characteristic test, Dynamic characteristic test for KS(Koran industrial standard) of Pneumatic servo valve. we accomplished study about the main item of Static characteristic test which is related to unload flow characteristic test. And Dynamic characteristic test was step input test and frequency response test. Specially about frequency response test, There was a difficulty resulting from the time delay problem caused by the basic compressibility of air. In order to solve the problem in this study. we proposed two methods. First, displacement of the servo valve spool was directly measured by using a laser sensor. Second, method of calculating control flow by measuring pressure and temperature of chamber.

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Characteristics of Bond Strength with Measuring Methods of Concrete (시험방법에 따른 신ㆍ구 콘크리트의 부착강도 특성)

  • 장흥균;김성환;홍창우;윤경구
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.05a
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    • pp.597-600
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    • 2003
  • The development and maintenance of a sound bond are an essential requirements of concrete repair and replacement. The bond property of a bonded overlay to its substrate concrete during the lifetime is one of the most important performance requirements which should be quantified. A standard or a verified bond strength measurement method is required at field for screening, selecting materials and quality control for overlay or repair materials. This study compares the nipple pipe direct tensile test, flexural adhesion test, and core pull-off test with their test results. Substantial differences in the failure stresses of three test methods were attributed to their different geometries and loading conditions. From these comparison and investigation, core pull-off test was relatively good because the coefficient of variation values were about 2%. It would be suitable for use in-situ because of its simplicity and accuracy.

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Real-time Monitoring of Glucose Using a Differential Refractive Index Detector (시차 굴절률 측정에 의한 실시간 글루코오스 모니터링)

  • 정진갑;이명희;최은경
    • Textile Coloration and Finishing
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    • v.16 no.2
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    • pp.47-51
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    • 2004
  • A differential refractive index detector was used for monitoring glucose contents in textile processing solutions. The sensitivity of the device was high enough to measure 0.05% aqueous glucose solution that could not be measured by normal refractive index measurement. The device was set to monitor glucose concentration continuously in real time by measuring differential refractive index and calibrated by standard glucose solutions in a range of 0.1 to 1.0%. The possibility of industrial application of the device was demonstrated by real-time monitoring of glucose concentration in textile processing solutions such as desizing bath and cellulase treatment bath. Both of solutions contained glucose as a major degraded product. The device would be able to control the weight loss of cellulosic fiber during cellulase treatment since the amount of degraded products in a processing bath is proportional to its weight loss.

Automation of an OTF measurement system using a fishtail edge (Fishtail Edge를 이용한 OTF 측정장치의 자동화)

  • 김태희;최옥식;조현모;이윤우;이인원
    • Korean Journal of Optics and Photonics
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    • v.8 no.1
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    • pp.7-13
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    • 1997
  • This paper describes the automation of an object generator and an image analyser in a knife scan OTF equipment to enhance the accuracy of OTF measurement. Pinholes and slits of various size in the object generator are used as an objects. A fishtail edge is mounted to the image analyzer and is translated to the direction of 45 degree angle with the horizontal to measure MTF simultaneously in the radial and tangential azimuths. The stepping motor control unit and software for the image analyzer are modified and the accuracy of this equipment is evaluated by measuring the OTF of SIRA group 50 mm standard lens.

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Relationships Between Learning-Related Social Skills and Literacy Development of Young Children (유아의 학습관련 사회적 기술과 문식성 발달과의 관계)

  • Ahn, Sun Hee;Kwon, Heekyoung
    • Korean Journal of Child Studies
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    • v.26 no.4
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    • pp.173-188
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    • 2005
  • To examine relationships between learning-related social skills(LRSS) and literacy development a sample of 167 children aged 5-6 years were selected from 3 preschools in Seoul. Instruments for measuring LRSS were the cooperation, assertion, and self-control scales of the Social Skills Rating System (Gresham & Elliott, 1990) and the mastery behaviors scales of the Child Behavior Rating Scale (Bronson, et al. 1990). Literacy development was measured by the Concepts about Print(Woon, 1999), the Learning Readiness Scale(Korean Educational Development Institution 1998), and the Writing Development Scale(Lee, 1997). Teachers rated children's LRSS. Data were analyzed by mean, standard deviation, t-test, bivariate correlation, and regression analysis. LRSS correlated with children's literacy development. Mastery behaviors were the best predictor of literacy development.

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