• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.17 no.4
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• pp.453-459
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• 2004

In this experiment, flux method was applied for preparing ferroxplana at low temperature, The common salt was used as a flux. The mole ratio of flux to Zn$_2$Y was varied with 0, 6.5, 13, 26 and 52 in dry ball-mixing. Zn$_2$Y was obtained after heat treatment of the mixed powder. Crystallization, particle morphology and magnetic properties of the prepared powder were investigated using XRD, VSM and SEM. The ferroxplana powder of 2-4 ${\mu}{\textrm}{m}$ was obtained with the mole ratio 26 by heat treating at the temperature of 110$0^{\circ}C$. The coercivity(H$_{c}$) and saturation magnetization(M$_{s}$) of the ferroxplana were 282Oe and 64.5emu/g, respectively.y.y.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2000.07a
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• pp.39-42
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• 2000

The effect of excess Pb contents on the etching of PZT thin films and their electrical properties has been investigated. Ferroelectric PZT(53/47) thin films were prepared by the metal alkoxide-based Sol-Gel method, in which they were spin-coating on P7Ti/Si02/Si substrate using the PZT(53/47) stock solutions with various excess Pb contents. Etching of PZT film was performed using planar inductively coupled Ar/Cl$_2$/BCl$_3$ plasma. The etch rate of PZT film was 2450 $\AA$/min at Ar(20)/BCl$_3$(80) gas mixing ratio and substrate temperature of 8$0^{\circ}C$.

• Proceedings of the Korea Concrete Institute Conference
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• 1998.10a
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• pp.262-268
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• 1998

This research is to examine the selected method of optimal mixing proportion and cost analysis in the super flowing concrete. As confined water $ratio($\beta_p$)$ and K is introduced, itis to establish optimal mixing design of super flowing concrete according to the steps of paste, mortar and concrete. From paste and mortar test, it was led to $$\beta_p$$ and $K_p$satisfying the optimum condions depending on the kinds of binders. Then $$\beta_p$$ and $K_p$ is reflected to the mix condition of super flowing concrete. The result of test, the mix condition of super flowing concrete satisfied the quality performance of concrete with adjustment of additional rate of the superplasticizer. Besides, in case of design strength $350kg/\textrm{cm}^2$ of concrete, material cost in super flowing concrete is able to be reduced 5~16% in replacement of fly ash 30% in ordinary portland cement and slag cement.

• Journal of Korean Society for Quality Management
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• v.42 no.4
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• pp.579-590
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• 2014

Purpose: Ball milling is a popular process for obtaining fine powders in the part and material industry. One of important issues in the ball milling is to produce particles with a uniform size. Although many factors affect uniformity of particles, this paper focuses on the choice of ball diameter. Consider a ball milling where balls can be taken with three different diameters. The purpose of this paper is to find a ball mix which minimizes the average particle size. Methods: Ball diameters are selected as 10mm, 3mm, and 0.5mm. In order to find an optimum mixing ratio, the method of mixture experiments is employed in this paper. Taguchi's signal-to-noise ratio (SNR) for smaller-the-better type is also used to analyze experimental data. Results: According to the experimental result, SNR is maximized when the ball mix is taken as either 7:3:0 or 6:4:0. Such mixing ratios can be technically validated in terms of porosity reduction. Conclusion: The ball mixing technique presented in this paper provides a useful way to improve the production efficiency with a low cost.

• Proceedings of the Korea Concrete Institute Conference
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• 2006.11a
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• pp.141-144
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• 2006

The main purpose of this study is to develop a Sprayed FRP repair and strengthening method, which is a new technique for strengthening the existing concrete structures by mixing carbon or glass shot fibers and the epoxy or vinyl ester resins with high-speed compressed air in open air and randomly spraying the mixture onto the concrete surface. At present, the Sprayed FRP repair and strengthening method using the epoxy resin has not been fully discussed. In order to investigate the material property of Sprayed FRP, this study carried out tensile tests of the material specimens which are changed with the combinations of various variables such as the length of shot fiber and mixture ratio of shot fiber and resin. These variables are set to have the material strength equal to one layer of the FRP sheet. As a result, the optimal length of glass and carbon shot fibers were derived into 3.8cm, and the optimal mixture ratio was also deriver into 1:2 from each variable. And also, the thickness of Sprayed FRP to have the strength equal to one layer of FRP sheet was finally calculated.

• Bulletin of the Korean Chemical Society
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• v.34 no.7
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• pp.1995-2000
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• 2013

Layered $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ was prepared by the mixed hydroxide method at various temperatures. Xray diffraction (XRD) pattern shows that this material has a ${\alpha}-NaFeO_2$ layered structure with $R{\bar{3}}m$ space group and that cation mixing is reduced with increasing synthesis temperature. Scanning electron microscopy (SEM) reveals that nano-sized $Li_{1.2}(Fe_{0.16}Mn_{0.32}Ni_{0.32})O_2$ powder has uniform particle size distribution. X-ray absorption near edge structure (XANES) analysis is used to study the local electronic structure changes around the Mn, Fe, and Ni atoms in this material. The sample prepared at $700^{\circ}C$ delivers the highest discharge capacity of 207 $mAhg^{-1}$ between 2-4.5 V at 0.1 $mAcm^{-2}$ with good capacity retention of 80% after 20 cycles.

• Journal of the Korean Recycled Construction Resources Institute
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• v.1 no.3
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• pp.219-224
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• 2013

In this study, the inorganic insulating material was fabricated with quartzite, ordinary portland cement(OPC), lime and anhydrous gypsum. After characteristic analysis of slurry, the optimum mixing ratio was derived with different $CaO/SiO_2$ mole ratio. Based on derived mixing ratio, the inorganic insulating material was fabricated at different water content and hydrothermal synthesis conditions. Specific gravity was $0.26g/cm^3$, compressive strength was 0.4 MPa, and thermal conductivity was 0.064 W/mK. This properties were enhanced performance of conventional ALC (Autoclaved Lightweight Concrete). And it can replace organic insulation with harmless inorganic insulation through continues research and development.

• Fire Science and Engineering
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• v.16 no.2
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• pp.22-26
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• 2002

It is very important to find out how to economically recycle waste tyres thrown away from the industry to the field. This one is also consistent with environmentally-friend policy. Many papers have been produced for focusing on the strength using waste-tyre material. Now, many kind of particle sizes of waste-tyre material are being produced in Korea, with support of the government. This study is to figure out how much the waste tyre mixing concrete resists against temperature at fire and how much decrease rate it shows. All the result are compared here in order to find out the way to applicate it to the practical structure for this area. The mixing proportion rate is selected with an experience and try-and error method. Eventually some of distinctive results are mentioned in the conclusion. The waste tyre concrete heated with $600^{\circ}C$ temperature was almost no change of its strength comparing with the normal one.

• Resources Recycling
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• v.16 no.6
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• pp.10-19
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• 2007

The mechanical process followed by hydrometallurgical treatment has been developed in order to recover cobalt and lithium from spent lithium ion battery. In the previous study, a citrate precursor combustion process to prepare cathodic active materials from the leaching solution was elucidated. Resynthesis of electrode materials should be more valuable in spent battery recycling. Conventional slurry mixing of $LiCoO_2$ and carbon cannot make uniform distribution, and therefore the cathode cannot reach the theoretical charge-discharge capacity and is easily degraded during the charge-discharge cycling. In this study, ultra-fine $LiCoO_2$ powders has been prepared by modification of the combustion process and fabricated the enhanced cathode by modification of mixing method of $LiCoO_2$ and carbon added.

• Journal of the Korean GEO-environmental Society
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• v.12 no.4
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• pp.17-24
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• 2011

For the purpose of cut off and ground stabilization, water glass chemical grouting method using sodium silicate has problems of weakening durability and ground water pollution because leaching was conducted when the homogel is exposed to the ground water as time elapses. The purpose of this study is to identify the effect of alkali silica sol ground injection materials, it was compared with the sodium silicate ground injection materials using water glasses. For sodium silicate and alkali silica sol by mixing each case is divided into four different specimens were made and tested. The characteristic of alkali silica sol ground injection material was analyzed by unconfined compression test and environmental impact statement of ordinary portland cement and blast furnace slag cement. Alkali silica sol specimens were made mixing A-solution and B-solution in the proportion of one on one. Through this study, alkali silica sol ground injection mixing blast furnace slag cement has excellent strength and environment-friendly.