• 제목/요약/키워드: Mass standards

검색결과 465건 처리시간 0.03초

여대생의 신체조성과 골밀도의 관계 (The Relationship Between Body Composition and Bone Mineral Density in College Women)

  • 김명희;김주성
    • 대한간호학회지
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    • 제33권3호
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    • pp.312-320
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    • 2003
  • Purpose: To investigate body compositons and bone mineral density(BMD) in college women and to find the relationship between them. Method: From January to March of 2001, BMD at four parts(forearm, lumbar, femur and whole body), body mass index(BMI), body fat mass(BFM), lean body mass(LBM) and body fat percentage(%Fat) were measured with the Dual Energy X-ray Absorptiometry. Other physical characteristics were measured with a scale, a height measurer, and questionnaires. Result: Grouping by the BMI, 43.2% showed low weight, and 5% over weight. When applying the percent Fat, 43.8 % was diagnosed as obesity group. The fact indicate that a majority of college women have unbalanced body composition with high percent Fat, compared to their body weight. Assessing the BMD with the WHO standards, 91.4~95.7% of the BMD of forearm and whole body was normal. But, 40.3% and 33.1~43.9% showed osteopenia at lumbar and femur, and 104 %, 0.7~7.2% showed osteoporosis. The BMD at all parts showed significant correlation each other(r=.29~.89, p=.001~.000). Body weight and BMI showed correlations to with BMDs at all parts of the body(r=.19~46, p=.025~.000; r=18~.45, p=.039~.000). But the percent Fat had a correlation with only femur neck BMD(r=.19, p=.024). Conclusion: This study showed a majority of healthy college women were exposed to the risk for osteoporosis. Additional study is required to develop nursing interventions to remove the risk factors of osteoporosis. In particular, the acquisition of balanced body composition is necessary, increasing body weight and BMI through the increase of LBM, not through the quantitative increase of BFM.

Improvement of Measurement Precisions for Uranium Isotopes at Ultra Trace Levels by Modification of the Sample Introduction System in MC-ICP-MS

  • Park, Ranhee;Lim, Sang Ho;Han, Sun-Ho;Lee, Min Young;Park, Jinkyu;Lee, Chi-Gyu;Song, Kyuseok
    • Mass Spectrometry Letters
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    • 제7권2호
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    • pp.50-54
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    • 2016
  • Multi-collector inductively coupled plasma mass spectrometry (MC-ICP-MS) is currently used in our laboratory for isotopic and quantitative analyses of nuclear materials at ultra-trace levels in environmental swipe samples, which is a very useful for monitoring undeclared nuclear activities. In this study, to improve measurement precisions of uranium isotopes at ultratrace levels, we adopted a desolvating nebulizer system (Aridus-II, CETAC., USA), which can improve signal sensitivity and reduce formation of uranium hydride. A peristaltic pump was combined with Aridus-II in the sample introduction system of MC-ICP-MS to reduce long-term signal fluctuations by maintaining a constant flow rate of the sample solution. The signal sensitivity in the presence of Aridus-II was improved more than 10-fold and the formation ratio of UH/U decreased by 16- to 17- fold compared to a normal spray chamber. Long-term signal fluctuations were significantly reduced by using the peristaltic pump. Detailed optimizations and evaluations with uranium standards are also discussed in this paper.

식품중 발기부전 치료제 및 유사물질 함량에 관한 조사연구 (A Study on Contents of Anti-impotence drug/drug-like compounds in Food)

  • 홍해근;방선재;박광희;이인숙;박민정;박정화;김종찬
    • 환경위생공학
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    • 제22권3호
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    • pp.89-96
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    • 2007
  • To determine 8 anti-impotence drug/drug-like compounds such as sildenafil, vardenafil, tadalafil, homosildenafil, hydroxyhomosildenafil, aminotadalafil, pseudovardenafil and hongdenafil in foods, simultaneously, high performance liquid chromatography(HPLC) and liquid chromatography-mass spectrometry (LC/MS) were used. The HPLC/UV analysis was performed on a column of capcellpak $C_{18}$ with 0.1% sodium-1-hexansulfonate in 0.2M ammonium formate/acetonitrile as a mobile phase. Mass spectra of the compounds by LC/MS were investigated with SCAN mode(Mass range and Fragment voltage) and SIM(Selected Ion Monitoring) mode (Ion target and Fragment voltage). The results follow as; 1. The HPLC/UV analysis was detected from 5 out of 63 samples. The content of sildenafil was in the range of 32.80 ppm ${\sim}$ 60.13 ppm from 4 out of 5 samples. The contents of sildenafil, vardenafil, homosildenafil were in the range 47.14 ppm from 1 out of 5 samples. 2. The conformed result of LC/MS was equal of detected from 5 out of 63 samples in HPLC/UV analysis. An easily available, simultaneous determination of 8 standards in adulterated health related foods was established by using a combination of LC/MS methods.

의류봉제업체의 생산현황과 대량맞춤에 대한 인식 (The Production Situations of Apparel Sewing Company and the Perceptions about the Mass Customization)

  • 홍경희;이지수;김영미;양진옥;이윤정
    • 한국의류산업학회지
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    • 제12권2호
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    • pp.162-171
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    • 2010
  • This study aims to discuss what changes Korean clothing companies and manufacturers have undergone with production facilities moving abroad due to offshore outsourcing and examine what conditions the clothing manufacturers are facing and how the clothing companies recognize those manufacturers. For these purposes, in-depth interviews were conducted with 24 firms with annual production capacity of more than 200,000 pieces among clothing brands for the domestic market, clothing exporters and promotion agencies. Those interviewed firms were the companies who were found to produce more than 200,000 pieces of clothing per year, and the interview-based survey was conducted from December 18, 2008 to January 30, 2009. The key findings from this study are as follows; first, a high percentage of interviewed firms were producing only a small number of items in Korea with a large part of their production line transferred abroad or outsourcing all of their production abroad only with their headquarters in Korea. Second, many were employing contractors rather than their own factories. Third, when asked about the wage levels of clothing manufacturers, many of the clothing companies gave responses such as: 'They are just our contractor, so we respect their decision,' 'We don't know because it's none of our business,' or 'We don't know at all.' Fourth, when asked about the work environment of clothing manufacturers, the clothing companies gave responses such as: 'We know in part,' 'To our knowledge, they conform to the Labor Standards Law,' or 'We don't know at all.' Fifth, the production line of clothing manufacturers featured straight-line systems, specialization, pairing and compounding/mixing. Sixth, it was found that clothing companies had interest in mass customization but their preparations were not satisfactory.

A successful experience of soil-transmitted helminth control in the Republic of Korea

  • Hong Sung-Tae;Chai Jong-Yil;Choi Min-Ho;Huh Sun;Rim Han-Jong;Lee Soon-Hyung
    • Parasites, Hosts and Diseases
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    • 제44권3호
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    • pp.177-185
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    • 2006
  • Soil-transmitted helminths (STH), namely Ascaris, Trichuris and hookworms (Ancylostoma and Necator), present a global health problem to about a half of the earth's population. In the Republic of Korea, STH were highly prevalent and were considered a high priority target for national control. To promote the control, a non-governmental organization named Korea Association for Parasite Eradication (currently Korea Association of Health Promotion) was founded in 1964, and mass fecal examination followed by selective mass chemotherapy with anthelmintics was performed twice a year from 1969 to 1995 targeting whole nationwide schoolchildren. Meanwhile, decreasing patterns of national STH infections have been monitored by 7 times' quinquennial national surveys targeting general population. In 1971, the overall intestinal helminth egg positive rate was 84.3% (Ascaris 58.2%, Trichuris 65.4%, and hookworms 10.7%), which became 63.2% in 1976, 41.1% in 1981, 12.9% in 1986, 3.8% in 1992, 2.4% in 1997, and 4.3% (Ascaris 0.03%, Trichuris 0.02%, and hookworms 0%) in 2004. During the control period, national economy rapidly developed, and living standards including environment, sanitation, and agricultural technology greatly improved, which undoubtedly boosted the STH control effects. Our experience indicates that social driving force to establish an eligible national control system to conduct repeated mass chemotherapy, together with improvement of environment and sanitation, is important for initiating and achieving STH control in a developing community.

콩 함유 사포닌의 종류 및 함량 분석 (HPLC/MS/MS Method for Determination of Soyasaponins in the Soybean Varieties)

  • 한상준
    • 한국작물학회지
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    • 제56권3호
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    • pp.244-249
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    • 2011
  • 본 연구는 콩 함유 사포닌의 함량을 쉽고 빠르게 정량할 수 있는 방법을 개발하기 위하여 시도하였다. 사포닌 표준 물질인 soyasaponin I은 대두에서 직접 분리하여 동정하였고, 분석은 HPLC/MS/MS를 이용하였으며 그 결과는 다음과 같다. 1. DAD 또는 ELSD를 이용하여 분석할 때보다 전처리 과정을 획기적으로 줄일 수 있어 신품종 육성의 선발과 같은 대량의 분석에 적합하였다. 2. Soyasaponin I의 함량은 나물콩과 같은 소립종에서 대립종에 비해 함량이 유의하게 높은 것으로 나타났다.

A one-dimensional model for impact forces resulting from high mass, low velocity debris

  • Paczkowski, K.;Riggs, H.R.;Naito, C.J.;Lehmann, A.
    • Structural Engineering and Mechanics
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    • 제42권6호
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    • pp.831-847
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    • 2012
  • Impact from water-borne debris during tsunami and flood events pose a potential threat to structures. Debris impact forces specified by current codes and standards are based on rigid body dynamics, leading to forces that are dependent on total debris mass. However, shipping containers and other debris are unlikely to be rigid compared to the walls, columns and other structures that they impact. The application of a simple one-dimensional model to obtain impact force magnitude and duration, based on acoustic wave propagation in a flexible projectile, is explored. The focus herein is on in-air impact. Based on small-scale experiments, the applicability of the model to predict actual impact forces is investigated. The tests show that the force and duration are reasonably well represented by the simple model, but they also show how actual impact differs from the ideal model. A more detailed three-dimensional finite element model is also developed to understand more clearly the physical phenomena involved in the experimental tests. The tests and the FE results reveal important characteristics of actual impact, knowledge of which can be used to guide larger scale experiments and detailed modeling. The one-dimensional model is extended to consider water-driven debris as well. When fluid is used to propel the 1-D model, an estimate of the 'added mass' effect is possible. In this extended model the debris impact force depends on the wave propagation in the two media, and the conditions under which the fluid increases the impact force are discussed.

Evaluation of extraction methods for essential oils in mugwort (Artemisia montana) using gas chromatography-mass spectrometry

  • Kim, Jihwan;Oh, Si-Eun;Choi, Eunjung;Lee, Sung-Hoon;Hwang, In Hyun;Kim, Ju-Young;Lee, Wonwoong
    • 분석과학
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    • 제35권2호
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    • pp.53-59
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    • 2022
  • Mugwort (Artemisia montana), which is a perennial plant mainly distributed throughout Northeast Asian regions, has been used as a preferred source of various foods and traditional medicines in Korea. In particular, as essential oils extracted from mugwort were reported to be biologically active, its steam distillate has been widely used to treat various conditions, such as itching, hemorrhoids, and gynecological inflammation. Therefore, efforts have been devoted to develop effective methods for the collection of bioactive essential oils from mugwort. In this study, five mugwort extracts were obtained using different extraction conditions, namely, 6 % ethanol at room temperature and at 80 ℃, pure ethanol, n-hexane, and an adsorbent resin. To evaluate the five extracts of mugwort, area-under-the-curve values (AUCs), chemical profiles, and major bioactive essential oil contents were investigated using gas chromatography-mass spectrometry (GC-MS). An overall assessment of the volatile components, including essential oils, in the five extracts was conducted using AUCs, and the individual essential oil in each extract was identified. Furthermore, the four major essential oils (1,8-cineole, camphor, borneol, and α-terpineol), which are known to possess anti-microbial and anti-inflammatory activities, were quantified using authentic chemical standards. Based on the evaluation results, pure ethanol was the best extractant out of the five used in this study. This study provides evaluation results for the five different mugwort extracts and would be helpful for developing extraction methods to efficiently collect the bioactive oil components for medical purposes using chemical profiles of the extracts.

동위원소희석 액체크로마토그래피/질량분석법에 의한 혈청 내 콜레스테롤의 정량 (Quantification of cholesterol in human serum by isotope dilution liquid chromatography/mass spectrometry)

  • 신혜선;이화심;이계호
    • 분석과학
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    • 제21권6호
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    • pp.502-509
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    • 2008
  • 혈청 내 콜레스테롤을 정량분석하기 위한 일차분석법으로 동위원소희석 액체크로마토그래피/질량분석법(isotope dilution liquid chromatography/mass spectrometry)을 사용하였다. 콜레스테롤은 Thermo ODS hypersil $C^{18}$ 칼럼을 사용하여 분리하였고, 이동상은 100% 메탄올, 유속은 0.3 mL/min으로 하였다. 콜레스테롤과 콜레스테롤-$3,4-13C_2$$[M-H_2O+H]^+$이온에 해당하는 m/z 369.4와 371.3에서 모니터링하여 정량에 합당한 크로마토그램을 얻을 수 있었다. 방법의 유효성을 증명하기 위해서 NIST SRM 909b를 분석한 결과 인증값과 불확도 범위 내에서 일치하는 것을 확인하였다. 이 방법을 바탕으로 혈청 인증표준 물질 4 종류를 제조하여 인증을 실시하였다. 인증 결과, 반복성의 상대표준오차는 0.1~0.8%, 재현성의 경우 0.24%이하, 확장 불확도는 95% 신뢰도구간에서 약 1.43%로 나타났다.

양호한 연속체 암반사면의 예비 판정기준 설정 연구 (A Study on Setup for Preliminary Decision Criterion of Continuum Rock Mass Slope with Fair to Good Rating)

  • 김형민;이수곤;이벽규;우재경
    • 지질공학
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    • 제29권2호
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    • pp.85-97
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    • 2019
  • 암반으로 구성되어 있는 급경사($65{\sim}80^{\circ}$) 암반사면들이 장기간 안정한 상태로 유지되고 있는 것을 관찰할 수 있다. 이와 유사한 지반상태로 이루어진 굴착 암반사면에서 불연속구조가 비탈면의 안정성에 유리한 방향으로 분포하고 있는 경우에는 발파암 경사기준인 1 : 0.5 ($63^{\circ}$)보다 급한 경사를 적용할 수 있을 것이다. 비탈면 설계기준의 경사 결정 과정에서 급경사로 적용할 수 있는 예비 암반조건이 정량적으로 설정되어 있으면 설계 실무측면에서 지침으로 활용할 수 있을 것이다. 이 연구에서는 상기 암반을 양호한 연속체 암반으로 정의하고, 양호한 연속체 암반조건에 대해 공학적인 준거를 제공할 목적으로 범용적인 RMR, SMR, GSI 분류를 활용하여 정량적인 설정기준 범위를 제안하고자 하였다. 연구방법으로는 다음과 같다. 암석종류별로 급경사 $65{\sim}80^{\circ}$)에서 안정한 비탈면을 연구 대상으로 선정하고, Face mapping 결과를 반영하여 RMR과 SMR 및 GSI 분류하였다. Hoek-Brown 파괴기준을 활용하여 산정된 강도정수를 현 상태의 암반사면 안정해석에 적용하여 나타난 결과를 검토하였다. 급경사로 안정하게 유지되는 지반조건으로서 예비기준의 타당성을 검증하기 위한 것이다. 상기 연구방법으로 분석 검토한 결과, 양호한 연속체 암반비탈면은 Basic RMR ${\geq}50$ (퇴적암에서는 45), GSI SMR ${\geq}45$로 설정할 수 있을 것으로 분석되었다. 한계평형 해석의 안전율은 Fs = 14.08~67.50 (평균 32.9)이고, 유한요소해석의 변위는 0.13~0.64 mm (평균 0.27 mm)이다. 이는 급경사($65{\sim}80^{\circ}$)로 오랜 기간 동안 안정하게 유지되고 있는 양호한 연속체 암반사면의 안정성을 정량적으로 표현하고 확인하는 결과로 볼 수 있다. 양호한 연속체 암반사면에 대한 암반기준 설정범위는 자료가 축적되면 좀 더 세부적인 설정기준을 확립할 수 있을 것이고 추후 연구과제이기도 하다. 1 : 0.1~0.3의 급경사에서도 안정할 경우에, 해외 설계기준 및 사례를 참고하여 급경사의 상한 기준을 1 : 0.3으로 설계하면 경제성과 친환경성을 확보하는 이점이 있게 된다. 또한 굴착기술과 식생기술 발달 및 다양한 친환경적 사면 설계기법으로 급경사에 따른 심리적 불안감과 급격한 지반이완을 극복할 수 있을 것이다.