• 산업식품공학
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• 제15권2호
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• pp.122-129
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• 2011

오징어 젓갈과 한치 젓갈의 차이를 질량분석기를 기반으로 한 전자코를 이용하여 분석한 결과 두 시료의 mass spectrum은 뚜렷한 차이를 보였다. 판별함수분석을 통해 휘발성분의 패턴을 분석한 결과 오징어 젓갈과 한치 젓갈이 뚜렷이 구분되었으며 젓갈의 양념을 제거한 후 분석하였을 때 구분이 더 잘되었다. 결과적으로 전자코를 이용하여 유사 식품 간의 차이를 충분히 구분 가능하였으며 이러한 결과는 추후 젓갈뿐 아니라 다양한 방면에 적용 가능할 것으로 보여 EMA 식품을 선별하는 데에도 도움이 될 것으로 기대된다.

• 우주기술과 응용
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• 제3권1호
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• pp.26-43
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• 2023

우리나라의 첫 달 탐사선 다누리호가 달 궤도에 진입을 성공하면서 이후 화성 탐사와 같은 우리나라의 새로운 우주탐사 계획을 기대할 수 있게 되었다. 우리나라의 우주탐사 탑재체는 한정적인 분야에서만 개발되어 새로운 우주탐사 탑재체를 개발할 필요성이 있다. 국외에서는 우주탐사에 거의 기본적으로 탑재되는 장비로 질량분석기가 있으며, 탐사 대상의 대기와 휘발성 물질 관측과 더불어 유기물 분석을 통한 생명체 탐사까지 아우르는 매우 유용한 탑재체이다. 하지만 우리나라에선 우주탐사용으로 질량분석기 탑재체를 개발한 전적이 없으므로 앞으로의 우주탐사를 대비해 기술을 확보해야 할 필요가 있다. 그에 앞서 국외의 우주탐사용 질량분석기 탑재체의 과학적 성과를 살펴보고 동향을 파악해본다.

• Applied Science and Convergence Technology
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• 제24권5호
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• pp.142-150
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• 2015

A failure analysis of tungsten filaments used in quadrupole mass spectrometer for plasma process monitoring was carried by using SEM and EDS. Failed at high temperature, filaments showed two kinds of failure modes. The one is that diameter of filament became thinner gradually and finally snapped. The other is that filament abruptly snapped almost at a right angle. The EDS analysis showed Fe and C, including W and Fe, on the surface of failed filament. when failed filaments were treated with plasma in mixture of Ar and $CF_4$, the amount of Fe and C decreased. The failure analysis of filament showed that the cause of filament failure is thermal evaporation and grain growth of tungsten at high temperature.

• KSBB Journal
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• 제15권4호
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• pp.408-410
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• 2000

생리활성물질의 함유량이 많은 아가리쿠스버섯으로부터 초임계 유체 추출 기술을 이용하여 비극성 생리활성물질인 linoleic acid를 분리, 정제하였다. Gas chromatography - mass spectrometer를 이용하여 추출된 물질의 정성분석을 수행하여 추출된 물질은 약리작용 효과를 가지는 linoleic acid (cis-9, cis-12-octadecadienoic acid)로 분석되었다. 초임계 추출법을 이용한 아가리쿠스 버섯으로부터의 생리활성물질 추출공정의 최적화를 위하여 다양한 온도와 압력하에서 실힘을 수행하였으며 추출 효율을 비교한 결과 $50^{\circ}C, 200 kg_f/cm^2$의 최적 운전조건을 결정하였다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2003년도 추계학술대회 논문집 전기물성,응용부문
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• pp.293-296
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• 2003

We report on the fabrication and field emission of carbon nanotube field emitters for mass spectrometer. Due to its high aspect ratio and mechanical strength, we use vertically aligned multi-wall carbon nanotubes prepared by thermal chemical vapour deposition as cathodes, Electrons emitted from a CNT are to ionize some sample molecules. We have successfully attained patterned carbon nanotubes grown on two-dimensional 0.7 mm by 0.7 mm Ni square blocks on Si. The emission characteristics show that the field emission initiates at 200 V.

• Journal of Electrical Engineering and Technology
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• 제3권1호
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• pp.121-124
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• 2008

This paper presents the fabrication and field emission of carbon nanotube field emitters for a micro mass spectrometer. The carbon nanotube is an adequate material as a field emitter since it has good characteristics. We have successfully fabricated a diode field emitter and a triode field emitter. Each field emitter has been constructed using several micromachining processes and a thermal CVD process. In the case of the diode field emitter, to increase the electric field, the carbon nanotubes are selectively grown on the patterned nickel catalyst layer. The electron current of the diode field emitter is 73.2 ${\mu}A$ when the anode voltage is 1100V. That of the triode field emitter is 3.4 pA when the anode voltage is 1000V.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제55권4호
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• pp.204-208
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• 2006

In this study, we investigated the ion energy distributions in a chlorine based inductively coupled plasma by quadrupole mass spectrometer with an electrostatic ion energy analyzer. Ion energy distributions are presented for various plasma parameters such as $BCl_3/Ar$ gas mixing ratio, RF power, and process pressure. As the $BCl_3/Ar$ gas mixing ratio and process pressure decreases, and RF power increases, the saddle-shaped structures is enhanced. The reason is that there are ionized energy difference between $BCl_3$ and Ar, change of plasma potential, alteration of mean free path. and variety of ion collision in the sheath.

• Bulletin of the Korean Chemical Society
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• 제23권3호
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• pp.432-436
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• 2002

Benomyl, one of the known endocrine disrupting chemicals, was analyzed to understand the fate in the nature. Water, sediment and biota samples are acidified to hydrolyze benomyl into carbendazim then followed by extraction and concentration. The concentrations of carbendazim in the samples were determined by liquid chromatography/time-of-flight mass spectrometer. Analysis data showed that certain amount of carbendazim was accumulated in sediment. On the contrary, no sign of accumulation in biota was observed probably due to the increased degradation rate in vivo. It is, however, that no one can claim carbendazim is not harmful to biota, since carbendazim may give a negative effect against organisms at the point of intaking.

• 한국전기전자재료학회논문지
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• 제13권7호
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• pp.563-567
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• 2000

We presented the etch results of indium-tin oxide thin films by using SF$_{6}$/O$_2$gas electron cyclotron resonance plasma and conducted X-ray phtoelectron spectroscopy and quadrupole mass spectrometer analyses for the etch characteristics. The etch rate of the films was greatly dependent on that of oxygen which was the major constituent element of the films. The oxygen was removed by the forms like $O_2$or SOF$_2$. We examined the ratio of atomic content of O and In and the change of this ratio was related to the removal rate of InF$_{x}$ and the S-metal bonding.ing.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2005년도 추계학술대회 논문집
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• pp.65-66
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• 2005