• Journal of Ceramic Processing Research
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• v.19 no.5
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• pp.434-438
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• 2018

The sintering behavior of $BaFe_{12}O_{19}$ with the addition of one and three weight % of $CuWO_4$ as a liquid phase sintering aid is studied. Samples are sintered in the temperature range $900-1250^{\circ}C$ and the effect of $CuWO_4$ addition on density, microstructure, phase composition and magnetic properties is examined. Compared to $BaFe_{12}O_{19}$ with no sintering aid addition, addition of 1 wt % $CuWO_4$ retards densification. Addition of 3 wt % $CuWO_4$ promotes densification at lower sintering temperatures but retards densification at temperatures > $1050^{\circ}C$. Three wt % $CuWO_4$ addition induces the formation of $BaWO_4$ and $Ba_3WFe_2O_9$ secondary phases at temperatures ${\geq}1100^{\circ}C$. Addition of $CuWO_4$ causes a decrease in saturation magnetization, remanent magnetization and coercivity.

• Journal of Powder Materials
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• v.9 no.6
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• pp.381-393
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• 2002

Recent developments in nanocrystalline and nanocomposite rare earth-transition metal magnets are reviewed and emphasis is placed on research work at IFW Dresden. Principal synthesis methods include high energy ball milling, melt spinning, mold casting and hydrogen assisted methods such as reactive milling and hydrogenation-disproportionation-desorption-recombination. These techniques are applied to NdFeB-, PrFeB- and SmCo-type systems with the aim to produce high remanence magnets with high coercivity. Concepts of maximizing the energy density in nanostructured magnets by either inducing a texture via anisotropic HDDR or hot deformation or enhancing the remanence via magnetic exchange coupling are evaluated. With respect to high temperature applications melt spun $Sm(Co_{0.74}Fe_{0.1}Cu_{0.12}Zr_{0.04})_{7.5}$ ribbons were prepared, which showed coercivities of up to 0.53 T at 50$0^{\circ}C$. Partially amorphous $Nd_{60}Fe_xCo_{30-x}Al_{10}(0{\leq}x{\leq}30)$ alloys were prepared by copper mold casting. The effect of transition metal content on the glass-forming ability and the magnetic properties was investigated. The $Nd_{60}Co_{30}Al_{10}$ alloy exhibits an amorphous structure shown by the corresponding diffraction pattern. A small substitution of Co by 2.5 at.% Fe results In the formation of Fe-rich crystallites embedded in the Nd-rich amorphous matrix. The Fe-rich crystallites show hard magnetic behaviour at room temperature with a coercivity value of about 0.4 T, relatively low saturation magnetization and a Curie temperature of 500 K.

• Journal of the Korean Magnetics Society
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• v.21 no.2
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• pp.77-82
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• 2011

The use of soft magnetic materials have been increasing in the various industrial fields according to the increasing demand for high performance, automatic, miniaturing equipments in the recent our life. In this study, we investigated the effect of factors on the core loss and magnetic properties of electrical steel and soft magnetic composites. Furthermore, we reviewed the major efforts to reduce the core loss and improve the soft magnetic properties in the two main soft magnetic materials. Domain purification which results from reduced density of defects in cleaner electrical steels is combined with large grains to reduce hysteresis loss. The reduced thickness and the high electrical conductivity reduce the eddy current component of loss. Furthermore, the coating applied to the surface of electrical steel and texture control lead to improve high permeability and low core loss. There is an increasing interest in soft magnetic composite materials because of the demand for miniaturization of cores for power electronic applications. The SMC materials have a broad range of potential applications due to the possibility of true 3-D electromagnetic design and higher frequency operation. Grain size, sintering temperature, and the degree of porosity need to be carefully controlled in order to optimize structure-sensitive properties such as maximum permeability and low coercive force. The insulating coating on the powder particles in SMCs eliminates particle-to-particle eddy current paths hence minimizing eddy current losses, but it reduces the permeability and to a small extent the saturation magnetization. The combination of new chemical composition with optimum powder manufacturing processes will be able to result in improving the magnetic properties in soft magnetic composite materials, too.

• Journal of Magnetics
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• v.15 no.4
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• pp.179-184
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• 2010

We have investigated the effects of post annealing on iron oxide nanoparticles synthesized by the novel hydrothermal synthesis method with the $FeSO_4{\cdot}7H_2O$. To investigate the post annealing effect, the as-synthesized iron oxide nanoparticles were annealed at different temperatures in a vacuum chamber. The morphological, structural and magnetic properties of the iron oxide nanoparticles were investigated with high resolution X-ray powder diffraction (XRD), high resolution transmission electron microscopy (HRTEM), Mossbauer spectroscopy, and vibrating sample magnetometer analysis. According to the XRD and HRTEM analysis results, as-synthesized iron oxide nanoparticles were only magnetite ($Fe_3O_4$) phase with face-centered cubic structure but post annealed iron oxide nanoparticles at $700^{\circ}C$ were mainly magnetite phase with trivial maghemite ($\gamma-Fe_2O_3$) phase which was induced in the post annealing treatment. The crystallinity of the iron oxide nanoparticles is enhanced by the post annealing treatment. The particle size of the as-synthesized iron oxide nanoparticles was about 5 nm and the particle shape was almost spherical. But the particle size of the post annealed iron oxide nanoparticles at $700^{\circ}C$ was around 25 nm and the particle shape was spherical and irregular. The as-synthesized iron oxide nanoparticles showed superparamagnetic behavior, but post annealed iron oxide nanoparticles at $700^{\circ}C$ did not show superparamagnetic behavior due to the increase of particle size by post annealing treatment. The saturation of magnetization of the as-synthesized nanoparticles, post annealed nanoparticles at $500^{\circ}C$, and post annealed nanoparticles at $700^{\circ}C$ was found to be 3.7 emu/g, 6.1 emu/g, and 7.5 emu/g, respectively. The much smaller saturation magnetization value than one of bulk magnetite can be attributed to spin disorder and/or spin canting, spin pinning at the nanoparticle surface.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.17 no.1
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• pp.11-17
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• 2007

The spherical NiZn ferrite particles were prepared by ultrasonic spray pyrolysis with mixed solution of aqueous metal nitrates. The NiZn ferrite particle was observed with nano-sized primary particles of about 10 nm or less before annealing which represented as paramagnetic behavior measured at 77 K and room temperature. The typical abnormal growth of primary particles like polyhedral primary particles was observed by annealing at 1273 K with Zn-concentration dependency. The XRD patterns showed good crystallinity of NiZn ferrite powder after annealing. In annealing process, the intra-particle sintering phenomenon was observed and the spherical particle morphology was collapsed at 1673 K. The saturation magnetization of NiZn ferrite powder for each annealing temperature was decreased with measuring temperature of $77{\sim}$300K.

• Journal of Electrical Engineering and Technology
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• v.12 no.1
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• pp.110-116
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• 2017

This paper proposed a new real-time parameter tracking algorithm. Unlike the convenience algorithms, the proposed real-time parameter tracking algorithm can estimate parameters through three-phase voltage and electric current without coordination transformation, and does not need information on magnetic flux. Therefore, it can estimate parameters regardless of the change according to operation point and cross-saturation effect. In addition, as the quasi-real-time parameter tracking technique can estimate parameters through the four fundamental arithmetic operations instead of complicated algorithms such as numerical value analysis technique and observer design, it can be applied to low-performance DSP. In this paper, a new real-time parameter tracking algorithm is derived from three phase equation. The validity and usefulness of the proposed inductance estimation technique is verified by simulation and experimental results.

• Proceedings of the KIEE Conference
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• 2011.07a
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• pp.997-998
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• 2011

본 논문에서는 영구자석 동기전동기의 영구자석 평균온도를 다이나모 시험을 통해 얻어진 토크 데이터로부터 간접적으로 계산하는 방법이 제시된다. 특히 영구자석의 온도에 따른 잔류자속밀도 변화에 자기 포화 효과를 고려하여 다양한 운전점에서의 온도추이를 간단하고 정확히 계산할 수 있다.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.56 no.3
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• pp.519-523
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• 2007

In this paper, we propose a precise parameter extraction of interior permanent magnet (IPM) motors based on finite element analysis. For the calculation of the two-axis inductances Ld and Lq, the slotting effect and cross magnetization due to torque angle are considered. It is examined that back electro-motive force (BEMF) constant is affected by the magnetic saturation in different ways dependent on motor types. Numerical analyses and some measurements are performed for a spoke type and a flux barrier type IPM motors

• Proceedings of the KIPE Conference
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• 2017.11a
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• pp.71-72
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• 2017

본 논문에서는 비선형 최적화 기법을 이용하여 자기 포화(magnetic saturation) 및 교차 결합 현상(cross-coupling effect)을 고려한 매입형 영구자석 전동기(IPMSM)의 실시간 MTPA 제어 방법을 제안한다. 이는 토크 지령 추종과 최소 동손 운전을 만족하는 제한 최적화(constraint optimization) 문제로 접근할 수 있다. 이를 통해 유도한 연립 비선형 방정식의 경우, Levenberg-Marquardt 수치 해석법을 적용하여 안정적이면서 빠르게 해를 구할 수 있다. 이러한 방법을 이용하면 참조표(look-up table) 없이 운전 환경의 실시간 변동을 고려한 효율적인 MTPA 운전이 가능하다. 시뮬레이션을 통해 제안된 알고리즘의 전류 해가 최적 운전점과 일치함을 확인하였다.

• 제어로봇시스템학회:학술대회논문집
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• 1992.10a
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• pp.664-669
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• 1992

In this paper, we present a DSP-based high dynamic performance torque control scheme of variable reluctance motors(VRM's) for DD(Direct Drive) robots via function inversion technique. The VRM with our controller behaves like DC motors, and hence developed torque tracks given torque command accurately with no torque ripples. Furthermore, our torque control algorithm ensures the production of maximum constant torque under maximum current limitation, minimizes power loss in each phase resistance, and takes magnetic saturation effect into account. Also, since our control algorithm is represented in the form of look-up table, it can be easily implemented with simple digital circuits and this tabular design method is computationally more accurate and simpler compared to the prior methods.