• Title/Summary/Keyword: Hot pressing method

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The effect of MEA fabrication procedure on PEMFC performance (고분자전해질 연료전지의 MEA 제조방법에 따른 성능비교)

  • Cho Yong-Hun;Cho Yoon-Hwan;Park In-Su;Choi Baeckbom;Jung Dae-Sik;Sung Yung-Eun
    • 한국신재생에너지학회:학술대회논문집
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    • 2005.06a
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    • pp.291-295
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    • 2005
  • The PEMFC behavior is quite complex and is influenced by several factors, including composition and structure of electrodes and membrane type. Fabrication of MFA is important factor for proton exchange membrane fuel cell. MFA of PEMFC with hot pressing and direct coating method were prepared, and performances were evaluated and compared each other. The effect of MEA preparation methods, hot pressing methods and direct coating methods, on the cell performance was analyzed by impedance spectroscopy and SEM. The performance of PEMFC wi th direct coat ing method was better than wi th hot pressing method because membrane internal resistance and membrane-:-interfacial resistance were reduced by elimination of hot pressing process in MEA fabrication. In addition the micro structure of MEA with direct coating method reveals uniform interface between membrane and catalyst layer.

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Fabrication and Properties Analysis of MEA for PEMFC (고분자전해질 연료전지용 MEA 제조 및 특성평가)

  • Cho Y.H.;Cho Y.H.;Park I.S.;Sung Y.E.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.230-234
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    • 2005
  • Fabrication of MEA is important factor for proton exchange membrane fuel cell (PEMFC). MEA of PEMFC with hot pressing and direct coating method were prepared, and performances were evaluated and compared each other. The effect of MEA preparation methods, hot pressing methods and direct coating methods, on the cell performance was analyzed by impedance spectroscopy and SEM. The performance of PEMFC with direct coating method was better than with hot pressing method because membrane internal resistance and membrane-interfacial resistance were reduced by elimination of hot pressing process in MEA fabrication. In addition the micro structure of MEA with direct coating method reveals uniform interface between membrane and catalyst layer.

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A Performance characteristics of Pt/C Electrode prepared by Hot Pressing Method (Hot Pressing법에 의해 제조된 Pt/C 전극의 성능특성)

  • 김진수;서동우;설용건;이태희
    • Journal of Energy Engineering
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    • v.1 no.1
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    • pp.58-65
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    • 1992
  • Pt loaded porous carbon Pt/C electrode was prepared by hot pressing process to enhance the electrode performance in PAFC (phosphoric acid fuel cell). By changing the hot pressing conditions and PTFE contents, Pt/C electrodes were prepared and the electrochemical characteristics of oxygen reduction and unit-cell performance were evaluated. The optimum condition of hot press to make electrode is 360$^{\circ}C$ and 10 kg/$\textrm{cm}^2$. Maximum performance was obtained at 30 wt% PTFE content in the catalyst layer with 80% utilization of platinum clusters. Unit-cell performance of hot pressed Pt/C electrode was 200 mA/$\textrm{cm}^2$ at 700 ㎷ and stable performance was maintained more than 200 hr.

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Optimal Shape Design of a Container Under Hot Isostatic Pressing by a Finite Element Method (열간등가압소결 공정에서 유한요소법을 이용한 컨테이너 형상의 최적설계)

  • Jeong, Seok-Hwan;Park, Hwan;Jeon, Gyeong-Dal;Kim, Gi-Tae;Hwang, Sang-Mu
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.9 s.180
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    • pp.2211-2219
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    • 2000
  • Near net shape forming of 316L stainless steel powder was investigated under hot isostatic pressing. To simulate densification and deformation of a powder compact in a container during hot isostatic pressing, the constitutive model of Abouaf and co-workers was implemented into a finite element analysis. An optimal design technique based on the design sensitivity was applied to the container design during hot isostatic pressing. The optimal shape of the container was predicted from the desired final shape of a powder compact by iterative calculations. Experimental data of 316L stainless steel powder showed that the optimally designed container allowed precise forming of the desired powder compact during hot isostatic pressing.

Microstructures and Tensile Properties of $A_2O_3$ Short Fiber/Al-Si-Mg Alloy Composites Fabricated by Rheo-compocasting and Hot Pressing (Rheo-compocasting 및 Hot Pressing에 의하여 제조한 $Al-Si-Mg/Al_2O_3$ 단섬유강화 복합재료의 조직 및 인장특성)

  • Kwak, Hyun-Man;Lee, Hag-Ju
    • Journal of Korea Foundry Society
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    • v.13 no.6
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    • pp.547-554
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    • 1993
  • Aluminum alloy matrix composites reinforced with various amounts of $Al_2O_3$ short fibers have been produced by rheo-compocasting accompanied by hot pressing. When composites reinforced with fibers are produced by rheo-compocasting, S-L process is the most effective method for homogeneous dispersion of fibers. A sound composites with the improved orientation(3 dimension${\rightarrow}$2 dimension) of the fibers and increased volume fraction of them have been fabricated through the hot pressing of the casted composites. Fibers are broken down when rheo-compocasting, hot pressing, and $T_6$ treating. Among them fibers are broken down most heavily in the hot pressing. And even in the case of the composite reinforced with 30 vol% fibers, which showed the hardest fiber break down, aspect ratio(11.6) is higher than critical aspect ratio(10.7). The fiber strengthening effect in the composites has showed upto 573K. As the test temperature increases to the range of 573K, the effect has been higher. The fracture of composites is controlled by fiber from room temperature to 473K, but the fracture of composites is controlled by interface between fiber and matrix alloy above 473K.

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Influence of Processing Conditions on PVDF Properties

  • Lebedev, S.M.;Gefle, O.S.;Semenikhin, M.V.
    • Journal of Powder Materials
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    • v.18 no.2
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    • pp.176-180
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    • 2011
  • Study of the main properties of PVDF films produced by two processing technologies such as hot pressing from a melt or solution casting was the aim of this paper. All samples were prepared of as-received PVDF powder. First group of samples was prepared by the hot pressing. Second group of samples was prepared by the solution casting method. PVDF powder was dissolved in dimethylformamide. To characterize properties of samples, different experimental methods such as FRA (dielectric spectroscopy), IR-spectroscopy and DSC/TGA analysis were used in this work. It was found that IR-spectra of both studied groups do not change compared to that for virgin PVDF powder. It confirms that molecular structure is practically independent on the processing technology of samples. The only difference has been found that new band centered at $1723\;cm^{-1}$ appears for samples prepared by the hot pressing method. This absorption band is related with formation of C=C bonds in samples prepared by the hot pressing method in contrast both to PVDF powder and samples prepared by the solution casting method.

Numerical Simulation for Pressing Process of Hot glass (고온 유리의 프레스 성형 공정 시뮬레이션)

  • Ji Suk Man;Choi Joo Ho;Kim Jun Bum;Ha Duk Sik
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.5 s.170
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    • pp.205-213
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    • 2005
  • This paper addresses a method for numerical simulation in the pressing process of hot glass. Updated Lagrangian finite element formulations are employed for the flow and energy equations to accommodate moving meshes. The model is assumed axi-symmetric and creep flow is assumed due to the high viscosity. Commercial software ANSYS is used to solve the coupled flow and energy equations. Moving contact points as well as free surface during the pressing are effectively calculated and updated by utilizing API functions of CAD software Unigraphics. The mesh distortion problem near the wall is overcome by automatic remeshing, and the temperatures of the new mesh are conveniently interpolated by using a unique function of ANSYS. The developed model is applied to the pressing process of TV glasses. In conclusion, the presented method shows that the pressing process accompanying moving boundary can be simulated by effectively combining general purpose software without resorting to special dedicated codes.

Hot Pressing Technology for Improvement of Density Profile and Sound Absorption Capability of Particleboard (파티클보드의 밀도경사와 흡음성 개선을 위한 열압기술)

  • Park, Hee Jun;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.30 no.1
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    • pp.25-33
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    • 2002
  • Improvement of density profile and sound absorption capability of particleboard was attempted. Three types of hot pressing methods examined ; flat-platen pressing method (A-type pressing), hot pressing in forming box (B-type pressing), and hot pressing set up jagged caul in forming box (C-type pressing). The raw materials were larch(Larix leptolepis (S, et. Z.) Gorden) shavings, phenol formaldehyde resin, and the particleboard perforated with stair type. The physical and mechanical properties such as specific gravity, bending strength (MOR), internal bonding strength (IB) and sound absorption coefficients were examined. The results are summarized as follows : 1) The MOR and internal bonding strength of the board pressed in forming box were higher than those of flat-platen pressed board. 2) The minimum density to average density ratio in thickness direction which pressed in forming box showed about 923%, in the case of 35 mm commercial particleboard and 50 mm flat-platen pressed board, its values showed about 66.4% and 865% respectively. 3) Sound absorption coefficients of the particleboard perforated with stair type were higher than those of flat-plated pressed board and commercial particleboard.

Preparation of a Li7La3Zr1.5Nb0.5O12 Garnet Solid Electrolyte Ceramic by using Sol-gel Powder Synthesis and Hot Pressing and Its Characterization

  • Lee, Hee Chul;Oh, Nu Ri;Yoo, Ae Ri;Kim, Yunsung;Sakamoto, Jeff
    • Journal of the Korean Physical Society
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    • v.73 no.10
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    • pp.1535-1540
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    • 2018
  • In this study, we prepared and characterized Nb-doped $Li_7La_3Zr_{2-x}O_{12}$ (LLZNO) powder and pellets with a cubic garnet structure by using a modified sol-gel synthesis and hot pressing. LLZNO powder with a very small grain size and cubic structure without secondary phases could be obtained by using a synthesis method in which Li and La sources in a propanol solvent were mixed together with Zr and Nb sources in 2-methoxy ethanol. A pure cubic phase LLZNO pellet could be fabricated from the prepared LLZNO and an additional 6-wt% of $Li_2CO_3$ powder by hot pressing at $1050^{\circ}C$ and 15.8 MPa. The hot-pressed LLZNO pellet with a relative density of 99% exhibited a very dense surface morphology. The total Li ionic conductivity of the hot-pressed LLZNO was $7.4{\times}10^{-4}S/cm$ at room temperature, which is very high level compared to other reported values. The activation energy for ionic conduction was estimated to be 0.40 eV.

Examination of Formaldehyde Emissions from the Hot-Pressing of Particleboard (파티클보드의 열압으로부터 포름알데히드 배출량 조사)

  • Oh, Yong-Sung;Kwak, Jun-Hyuk
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.33-39
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    • 2001
  • Laboratory particleboards (PBs) were made with urea-formaldehyde (UF) resins at four press times and two resin application rates. Enclosed caul system was used for collecting the exhaust gases materials generated during the hot-pressing of PB. Exhaust gases materials generated inside the enclosed caul during the hot-pressing of PB were collected in a controlled air stream. Formaldehyde from the exhaust gases collected was determined per a chromotropic method of the National Institute of Occupational Safety and Health Method 3500. The test results showed that formaldehyde emissions during the hot-pressing of PB increased with increasing press time, UF resin mole ratio, and resin application rate.

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