• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.26 no.2
• /
• pp.288-301
• /
• 2002

A vacuum freeze drying experiment of skim milk solution in a cylindrical container is conducted to investigate the multi-dimensional drying characteristics of the process during the primary drying stage. Temperature histories at several positions are measured under the same process condition that is carefully controlled. Then the measured temperature histories at different positions are combined to produce instantaneous temperature distribution fields inside the cylindrical container. Along with the temperature measurement, the mass reduction history of the skim milk solution is also measured. From the measured temperature distribution curved configurations of sublimation interfaces and 2-dimensional heat transfer is inferred. The freeze drying under the present experimental setup is simulated with a calculation program that is based on a finite volume method with a moving grid system. Good agreements between the numerical and experimental results are observed. The present experimental results and the numerical approaches can be useful information in developing the analysis tools for practical vacuum freeze drying processes.

• Transactions of the Korean hydrogen and new energy society
• /
• v.32 no.4
• /
• pp.205-211
• /
• 2021

Recently, it is necessary for study on renewable energy due to environmental pollution and fossil fuel depletion. Therefore, in this study, the filling temperature according to the nozzle geometry was evaluated based on the limit temperature specified in SAEJ2601 for charging hydrogen, a new energy. There are three types of nozzles, normal, angle and round, fixed the average pressure ramp rate at 52.5 MPa/min, and the injection temperature was set at 293.4 K. As a result, the lowest temperature distribution was found in the round type, although the final temperature did not differ significantly in the three types of nozzles. In addition, Pearson's coefficient was calculated to correlate the mass flow rate with the heat transfer rate at the inner liner wall, which resulted in a strong linear relationship of 0.98 or higher.

• Journal of the Korean Society of Safety
• /
• v.35 no.6
• /
• pp.32-45
• /
• 2020

The problem of determining the discharge rates of gases from pressurized vessels through pressure relief devices was dealt with comprehensively. First, starting from basic fluid flow equations, detailed modeling procedures were presented for isentropic nozzle flows and frictional flows in a pipe, respectively. Meanwhile, physical explanations were given to choking phenomena in terms of the acoustic velocity, elucidating the widespread use of Mach numbers in gas flow models. Frictional flows in a pipe were classified into adiabatic, isothermal, and general flows according to the heat transfer situation around the pipe, but the adiabatic flow model was recommended suitable for gas discharge through pressure relief devices. Next, for the isentropic nozzle flow followed by adiabatic frictional flow in the pipe, two equations were established for two unknowns that consist of the Mach numbers at the inlet and outlet of the pipe, respectively. The relationship among the ratio of downstream reservoir pressure to upstream pressure, mass flux, and total frictional loss coefficient was shown in various forms of MATLAB 2-D plot, 3-D surface plot and contour plot. Then, the profiles of gas properties and velocity in the pipe section were traced. A method to quantify the relationship among the pressure head, velocity head, and total friction loss was presented, and was used in inferring that the rapid increase in gas velocity in the region approaching the choked flow at the pipe outlet is attributed to the conversion of internal energy to kinetic energy. Finally, the Levenspiel chart reproduced in this work was compared with the Lapple chart used in API 521 Standatd.

• New & Renewable Energy
• /
• v.18 no.4
• /
• pp.12-21
• /
• 2022

The pyrolysis characteristics of high-density polyethylene (HDPE), low-density polyethylene (LDPE), and polypropylene (PP) were analyzed numerically using a 1D plug flow reactor (PFR) model. A lumped kinetic model was selected to simplify the pyrolysis products as wax, oil, and gas. The simulation was performed in the 400-600℃ range, and the plastic pyrolysis and product generation characteristics with respect to time were compared at various temperatures. It was found that plastic pyrolysis accelerates rapidly as the temperature rises. The amounts of the pyrolysis products wax and oil increase and then decrease with time, whereas the amount of gas produced increases continuously. In LDPE pyrolysis, the pyrolysis time was longer than that observed for other plastics at a specified temperature, and the amount of wax generated was the greatest. The maximum mass fraction of oil was obtained in the order of HDPE, PP, and LDPE at a specified temperature, and it decreased with temperature. Although the 1D model adopted in this study has a limitation in that it does not include material transport and heat transfer phenomena, the qualitative results presented herein could provide base data regarding various types of plastic pyrolysis to predict the product characteristics. These results can in turn be used when designing pyrolysis reactors.

• Journal of the Korean Society of Propulsion Engineers
• /
• v.27 no.1
• /
• pp.49-57
• /
• 2023

The autogenous pressurization has been widely adopted for propulsion systems of next-generation reusable rockets due to its low cost and high reliability. The autogenous pressurization has a simple structure, but an understanding of the heat and mass transfer occurring inside the tank is essential. For this reason, a simulation test of the autogenous pressurization was conceived. The experiment equipment was constructed based on overseas pressurization test facilities cases and expert advice. Unlike the actual autogenous pressurization system, the propellant tank was insulated to exclude external influences. The pressurized gas supply line and the propellant pipe were separated. Using the manufactured autogenous pressure experiment equipment, it is possible to evaluate the condensation phenomenon of pressurants in cryogenic propellants, comparison of the efficiency of pressurization using helium and evaporated gas and the pressurization capacity according to the temperature of pressurant.

• Journal of the Korean Institute of Gas
• /
• v.27 no.1
• /
• pp.78-85
• /
• 2023

Fixed-bed reactor Computational Fluid Dynamics (CFD) simulation of methanol steam reforming reaction was performed using the intrinsic kinetic data of the copper-impregnated hydrotalcite catalyst. The activation energy of the copper hydrotalcite catalyst obtained from the previous study results was 97.4 kJ/mol, and the pre-exponential was 5.904 × 10¹⁰. Process simulation was performed using the calculated values and showed a similar tendency to the experimental results. And the conversion rate according to the change of the reaction temperature (200 - 450 ℃) and the molar ratio of methanol and water was observed using the intrinsic kinetic data. In addition, mass and heat transfer phenomena analysis of a commercial reactor (I.D. 0.05 - 0.1m, Length 1m) was predicted through axial 2D Symmetry simulation using the power law model of the above kinetic constants.

• Advances in materials Research
• /
• v.13 no.3
• /
• pp.161-171
• /
• 2024

This study aimed to investigate the effect of physicochemical properties and mix ratios of iron ore (oxide feed): coke (reductant) on the carbothermic reductions of iron ore. Coke size was fixed at ≤63 ㎛ while iron ore size varied between 150-63 ㎛ and ≤63 ㎛ respectively. Mix ratios were changed from 100:0 (reference) to 80:20 and 60:40 while the temperature, heating rate and soaking duration in muffle furnace were fixed at 1100 ℃, 10 ℃/min and 1 hour. Particle size analyzer, XRF, CHNS and XRD analyses were used for determination of raw feed characteristics. The occurrence of phase transformations from various forms of iron oxides to iron during the carbothermal reductions were identified through XRD profiles and supported with weight loss (%). XRF analysis proved that iron ore is of high grade with 93.4% of Fe₂O₃ content. Other oxides present in minor amounts are 2% Al₂O₃ and 1.8% SiO₂ with negligible amounts of other compounds such as MnO, K₂O and CuO. Composite pellet with finer size iron particles (≤63 ㎛) and higher carbon content of 60:40 exhibited 45.13% weight lost compared to 32.30% and 3.88% respectively for 80:20 and 100:0 ratios. It is evident that reduction reactions can only occur with the presence of coke, the carbon supply. The small weight loss of 3.88% at 100:0 ratio occurs due to the removal of moisture and volatiles and oxidations of iron ore. Higher carbon supply at 60:40 leads into better heat and mass transfer and diffusivity during carbothermic reductions. Overall, finer particle size and higher carbon supply improves reactivity and gas-solid interactions resulting in increased reductions and phase transformations.

• Journal of the Korea Concrete Institute
• /
• v.15 no.2
• /
• pp.314-322
• /
• 2003

Pipe cooling method is widely used for reduction of hydration heat and control of cracking in mass concrete structures. However, in order to effectively apply pipe cooling systems to concrete structures, the coefficient of flow convection relating the thermal transfer between inner stream of pipe and concrete must be estimated. In this study, a device measuring the coefficient of flow convection was developed. Since a variation of thermal distribution caused by pipe cooling has a direct effect on internal forced flows, the developed testing device is based on the internal forced flow concept. Influencing factors on the coefficient of flow convection are mainly flow velocity, pipe diameter and thickness, and pipe material. Using experimental results from the developed device, the coefficient of flow convection was calculated. Finally, a general prediction model was proposed by theoretical procedures. The proposed prediction model is able to estimate the coefficient of flow convection with flow velocity and material properties of pipe. From comparison with experimental results, the coefficient of flow convection by this model was well agreed with those by experimental results.

• Journal of Ginseng Research
• /
• v.41 no.4
• /
• pp.572-577
• /
• 2017

Background: Panax ginseng Meyer is cultivated because of its medicinal effects on the immune system, blood pressure, and cancer. Major ginsenosides in fresh ginseng are converted to minor ginsenosides by structural changes such as hydrolysis and dehydration. The transformed ginsenosides are generally more bioavailable and bioactive than the primary ginsenosides. Therefore, in this study, hydrothermal processing was applied to ginseng preparation to increase the yields of the transformed ginsenosides, such as 20(S)-Rg3, Rk1, and Rg5, and enhance antioxidant activities in an effective way. Methods: Ginseng extract was hydrothermally processed using batch reactors at $100-160^{\circ}C$ with differing reaction times. Quantitative analysis of the ginsenoside yields was performed using HPLC, and the antioxidant activity was qualitatively analyzed by evaluating 2,2'-azino-bis radical cation scavenging, 2,2-diphenyl-1-picrylhydrazyl radical scavenging, and phenolic antioxidants. Red ginseng and sun ginseng were prepared by conventional steaming as the control group. Results: Unlike steaming, the hydrothermal process was performed under homogeneous conditions. Chemical reaction, heat transfer, and mass transfer are generally more efficient in homogeneous reactions. Therefore, maximum yields for the hydrothermal process were 2.5-25 times higher than those for steaming, and the antioxidant activities showed 1.6-4-fold increases for the hydrothermal process. Moreover, the reaction time was decreased from 3 h to 15-35 min using hydrothermal processing. Conclusion: Therefore, hydrothermal processing offers significant improvements over the conventional steaming process. In particular, at temperatures over $140^{\circ}C$, high yields of the transformed ginsenosides and increased antioxidant activities were obtained in tens of minutes.

• Journal of the Korean Institute of Intelligent Systems
• /
• v.14 no.5
• /
• pp.648-654
• /
• 2004

The Mass Flow Controller(MFC) has become crucial in semiconductor manufacturing equipments. It is an important element because the quality and the yield of a semiconductor process are decided by the accurate flow control of gas. Therefore, the demand for implementing the high speed and the highly accurate control of MFCs has been increasing. It is hard to find an article of the control algorithm applied to MFCs. But, it is known that commercially available MFCs adopt PID control algorithms. Particularly, when the system detects the flow by way of heat transfer, the MFC control problem includes the slow response and the nonlinearity. In this paper, MFC control algorithm with a superior performance to the conventional PID algorithm is discussed and the superiority is demonstrated through the experiment. A fuzzy controller was utilized in order to compensate the nonlinearity and the slow response, and the performance is compared with that of an MFC currently available in the market. The control system, in this paper, consists of a personal computer, the data acquisition board and the control algorithm carried out by LabWindows/CVI program on the PC. In addition, a method of estimating the actual flow from the sensor output with the slow response is presented. In conclusion, according to the result of the experiment, the proposed algorithm shows better accuracy and is faster than the conventional controller.