• 한국측량학회지
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• 제13권2호
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• pp.285-289
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• 1995

본 논문은 GPS로부터 측정된 타원체고와 Spirit Levelling으로부터 측정한 정표고를 이용하여 기하학적인 방법에 의하여 지오이드를 결정하였다. 기하학적인 지오이드고의 계산을 위하여 88점의 GPS측정데이타를 사용하였으며, 지오이드고는 간단하게 타원체고와 정표고의 차이를 구하고 보간법에 의하여 지오이드면을 결정하였다. 또한 보간법의 정확도를 평가하기 위하여 Minimum Curvature 방법과 Least Square Plane Fit방법을 사용하여 보간한 결과와 실측치를 비교하였으며, FFT를 적용하여 중력학적인 방법으로 결정한 지오이드고와 비교, 분석하였다.

• 통합자연과학논문집
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• 제3권4호
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• pp.210-214
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• 2010

Relationship between etch current and morphology and porosity of porous silicon (PS) has been investigated. The gravimetric method is applied to measured the porosity of PS. As the current density increase, the silicon dissolution rate increases, resulting in a higher porosity and etching rate. The result shows that linear dependence of PS porosity and etching rate as a function of current density. The morphology of porous silicon was investigated by using cold field emission scanning electron micrograph (FE-SEM). The size of pores formed during anodization is predominantly controlled by the current density, with an increase in the pore size corresponding to an increase in the current density.

• Bulletin of the Korean Chemical Society
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• 제32권1호
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• pp.117-121
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• 2011

Size-controlled Ag nanoparticles (NPs) were prepared from the decomposition of Ag(I) carboxylates using ethanolamine derivatives as a reducing agent without an additional stabilizing agent. The size of the Ag NPs with a narrow size distribution (sub-10 nm to ca. 40 nm) was controlled precisely by varying the processing parameters, such as the type of reducing agent and the chain length of the carboxylate in the Ag(I) carboxylate. The optical properties, surface composition and crystallinity of the Ag NPs were characterized by ultraviolet-visible spectroscopy, gas chromatography-mass spectrometry, thermal gravimetric analysis, transmission electron microscopy and X-ray diffraction.

• 한국식품과학회지
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• 제37권2호
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• pp.301-303
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• 2005

건강한 지원자를 대상으로 전기압력밥솥으로 조리한 수원464 백미와 일품종 백미를 섭취시켜 혈당의 반응을 비교한 결과식후 60분 후에서 수원464 백미섭취군의 혈당이 일품종 백미섭취군에 비해 유의성있게 더 감소하였다(p<0.01). 수원464의 혈당치가 일부 구간에서 현저히 낮은 이유는 수원464의 난소화성전분함량이 일반쌀에 비하여 높기 때문이라고 해석된다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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• pp.207-208
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• 2007

Recently, high performance microelectronic devices are designed in multi-layer structure in order to make dense wiring of metal conductors in compact size. Imprint lithography have received significant attention due to an alternative technology for photolithography on such devices. In this work, we synthesized dielectric composite materials based on epoxy resin, and investigated their thermal stabilities and dynamic mechanical properties for thermal imprint lithography. In order to enhance the mechanical properties and toughness of dielectric material, various modified polyetherimide(PEI) was applied in the resin system. Curing behaviours, thermal stabilities, and dynamic mechanical properties of the dielectric materials cured with various conditions were studied using dynamic differential scanning calorimetry (DSC), thermo gravimetric analysis (TGA), and Universal Test Method (INSTRON).

• Bulletin of the Korean Chemical Society
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• 제21권8호
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• pp.817-822
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• 2000

Crack-free hard coating siIica films were prepared by sol-gel processfrom twokinds of silicon alkoxide (tetra-ethoxysilane and methyltrimethoxysilane) and two kinds of alcohol (methanol and isopropyl alcohol) with an acid catalyst,acetic acid. A silicate framework of the precursor solution was investigated by infrared spectros-copy (IR) in the process of hydrolysis and condensation. Theextent of the condensation in the intermediates was elucidated by gel permeation chromatography (GPC) and 29Si-NMR spectroscopy. The hard coating films werecharacterized by IR,scanning electron microscope (SEM), thermo gravimetric analyzer (TGA) and dif-ferential scanning calroimeter (DSC). The synthetic condition for the crack-free and transparent silica film for-mation was optimized interms of starting materials for the precursor solution as well as preparation method of the silica film.

• Journal of Electrochemical Science and Technology
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• 제10권2호
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• pp.139-147
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• 2019

Incorporation of CuO nanoparticles during the polymerization of aniline in the presence of ammonium peroxydisulphate as an oxidizing agent and sodium salt of dodecylbenzene sulphonic acid as dopant as well as surfactant yielded water soluble CuO-PANI composite. Comparison of recorded spectra like FTIR, XRD and SEM with reported one confirm the formation of the composite. Analysis by gravimetric method exposes that the synthesized composite is having resistivity against corrosion, with slight variation in efficiency on extending the time duration up to eight hours in strong acidic condition. OCP measurement, potentiodynamic polarization and EIS studies also confirms the suppression ability of composite against corrosion. Riskless working environment could be provided by the synthesized composite during industrial cleaning process.

• Bulletin of the Korean Chemical Society
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• 제9권4호
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• pp.244-248
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• 1988

Multilayer adsorption isotherms of nitrogen on hexagonal boron nitride, ${\gamma}$-alumina, and silica-gel powders are determined at the liquid nitrogen temperature using a gravimetric adsorption apparatus. The volume (V) of the adsorbed gas are plotted against the statistical thickness(t) of the adsorbed layer, and the t-method area are calculated from the slope of these V-t plots to compare with the BET area. A number of universal adsorption isotherms and the Frenkel-Halsey-Hill equation are used one after another in calculating the statistical thickness. The appropriateness of the FHH equation as an universal adsorption isotherm is discussed finally.

• 대한화학회지
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• 제35권5호
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• pp.539-544
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• 1991

X-ray Compton 산란선의 강도를 측정하여 내지문처리재(Anti-fingerprint Steel)의 표면에 Coating 되어 있는 Silicone resin film의 두께를 신속하게 측정할 수 있는 새로운 분석방법을 연구하였다. Silicone resin과 같은 유기수지들은 C, H, O, Si 등과 같은 경원소들로 구성되어 있어 compton 산란선의 강도가 높게 나타나는데 이러한 성질을 이용, X-ray tube로부터 발생된 RhK$_{\alpha}$ 선을 시료표면에 조사한 후 발생된 RhK$_{\alpha}$ compton 산란선의 강도를 측정하여 silicone resin film의 두께를 구하였다. 검량곡선 작성결과 0.2 ~ 5.0 ${mu}$m 범위에서 직선성을 나타냈으며 두께측정에 대한 정확도는 0.22 ${mu}$m 이었다.

• 대한화학회지
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• 제35권3호
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• pp.204-210
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• 1991

Citrate 공침법으로 합성한 여러가지 perovskite형 복합산화물 흡착제에 대한 질소와 아르곤의 흡착등온곡선을 액체질소 온도에서 BET 중량 흡착장치를 사용하여 측정하였다. 여러 universal adsorption isotherm을 이용하여 흡착층의 통계적 두께 t를 구한 후, 측정한 흡착량을 각각의 통계적 두께 t에 대해서 도시하였다. 이 V-t plot으로부터 얻은 t-method 표면적과 BET 표면적을 비교하였다. 그리고 이 도시 결과에 입각해서 여러 universal adsorption isotherm의 적합성을 고찰하였다.