• Mass Spectrometry Letters
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• 제2권1호
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• pp.16-19
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• 2011

Oxidation products of ceftiofur were formed in hydrogen peroxide solution. The structures of the ceftiofur oxidation products were characterized by high-performance liquid chromatography/electrospray ionization/tandem mass spectrometry (HPLC/ESI/MS/MS). The products were identified as compounds oxidized at the sulfur of a cephem ring. For further analysis, experiments were performed using $O^{18}$-labeled hydrogen peroxide. In addition, density-functional calculations were carried out for six possible oxidation products to support the experimental results.

• 한국염색가공학회지
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• 제11권2호
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• pp.27-37
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• 1999

Polypropylene(PP) films were treated with plasma glow discharge to produce peroxy radicals on the surfaces. The peroxy radicals formed on the PP film surfaces were subsequently used for the graft polymerization of acrylic acid and acrylamide in an aqueous solution by heating, respectively. Introduction of acrylic acid and acrylamide on the PP film could be confirmed by the observation of carbonyl and primary amine absorptions based on carboxylic acid and amide, respectively. And introduction of functional group could be confirmed by weight analysis and ESCA. The water contact angle(90$^{\circ}$) of PP film was constant, irrespective of elapsed time, while plasma-treated and functional monomer-grafted PP films were slowly increased with elapsed time, showing the rearrangement of surface polar groups in air condition. The water contact angle$(90^\circ)$ of PP film was decreased by the plasma treatment$(56^\circ)$ and further decreased by the grafting of acrylic acid$(34^\circ)$ and acrylamide$(37^\circ)$, indicating increased hydrophilicity of the modified surfaces. The water contact angle of plasma-treated PP film increased a little as time elapsing. The half-life periods of surface voltage on acrylic acid-(31sec) and acrylamide-grafted PP(42sec) were significantly decreased when compared to those on PP(950sec) and plasma-treated PP film(241sec). In the experiments using acid, basic and disperse dyes, absorbance and $\Delta{E}$ values of functional monomer-grafted PP films were significantly increased than that of oxygen plasma-treated one.

• 한국의류학회지
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• 제46권5호
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• pp.910-926
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• 2022

Suitability for the human body, freedom to move and thermal insulation are important design considerations in military clothing. This study investigates the performance and wearer-satisfaction of the functional inner winter uniform currently used in Korea; it is hoped that our data can inform the development of a future version. Interviews were conducted, in which the participants suggested various improvements. The uniforms were mainly worn for guard duty or as daily attire in cold weather. The participants chose how many layers to wear according to the current situation, rather than sticking to the layering recommended in the manual. Layering choices did not significantly affect combat efficiency but were found to affect wearers' comfort. Wearers' satisfaction was found to depend on the convenience of the clothing, whether it was in the appropriate size, freedom to move and thermal insulation. Also, this study suggests a problem with the current size system, as the analysis of size distribution, across all sizes, the range of current production is insufficient to cover the demand.

• Macromolecular Research
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• 제11권6호
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• pp.495-500
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• 2003

UV-induced graft polymerization of glycidyl methacrylate (GMA) to a polypropylene (PP) membrane was carried out in the vapor phase with benzophenone (BP) as a photoinitiator. Attenuated total reflection Fourier transform infrared spectroscopy, atomic force microscopy (AFM), and scanning electron microscopy (SEM) were utilized to characterize the copolymer. The degree of grafting increased with increasing reaction time, increased UV irradiation source intensity, and increased immersion concentration of the BP solution. The optimum synthetic condition for the PP-g-GMA membrane was obtained with a reaction time of 2 hrs, a UV irradiation source intensity of 450 W, and an immersion concentration of the BP solution of 0.5 mol/L. The pure water flux decreased upon increasing the degree of grafting and increasing the amount of diethylamino functional group introduced. The analysis of AFM and SEM images shows that the graft chains and diethylamino groups of PP-g-GMA grew on the PP membrane surface, resulting in a change in surface morphology.

• Korean Membrane Journal
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• 제5권1호
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• pp.61-67
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• 2003

Various characteristics of ion transport properties of a charged mosaic membrane with a parallel array of positive and negative functional charges were investigated, From the analysis of the volume flux, it was found that the salt flux based on nonequilibrium thermodynamics, preferential salt transport across the charged mosaic membrane. Transport properties of the magnesium sulfate(MgSO$_4$) and sucrose across the charged mosaic membrane were estimated. As a result, metal salts transport depended largely on the charged states and molecular weight otherwise nonelectrolyte solution was rejected under all experimental conditions. On the other hand, the reflection coefficient s indicated the negative value that suggested preferential material transport and was independent of charged mosaic thickness.

• Nonlinear Functional Analysis and Applications
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• 제26권2호
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• pp.411-432
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• 2021

In this paper, an inertial Halpern-type forward backward iterative algorithm for approximating solution of a monotone inclusion problem whose solution is also a fixed point of some nonlinear mapping is introduced and studied. Strong convergence theorem is established in a real Hilbert space. Furthermore, our theorem is applied to variational inequality problems, convex minimization problems and image restoration problems. Finally, numerical illustrations are presented to support the main theorem and its applications.

• Nonlinear Functional Analysis and Applications
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• 제26권2호
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• pp.303-322
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• 2021

The concepts of new classes of mappings are introduced in the spaces which are more general space than the usual metric spaces. The existence and uniqueness of common fixed points and fixed point results are established in the setting of complete complex valued b-metric spaces. An illustration is given by establishing the existence of solution of periodic differential equations in the framework of a complete complex valued b-metric spaces.

• Nonlinear Functional Analysis and Applications
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• 제26권4호
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• pp.839-853
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• 2021

Let 𝕽ⁿ be an Euclidean space and g : 𝕽ⁿ → 𝕽ⁿ be a monotone and continuous mapping. Suppose the convex constrained nonlinear monotone equation problem x ∈ 𝕮 s.t g(x) = 0 has a solution. In this paper, we construct an inertial-type algorithm based on the three-term derivative-free projection method (TTMDY) for convex constrained monotone nonlinear equations. Under some standard assumptions, we establish its global convergence to a solution of the convex constrained nonlinear monotone equation. Furthermore, the proposed algorithm converges much faster than the existing non-inertial algorithm (TTMDY) for convex constrained monotone equations.

• Nonlinear Functional Analysis and Applications
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• 제27권3호
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• pp.471-497
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• 2022

In this paper, we study a system of nonlinear wave equations associated with the helical flows of Maxwell fluid. By constructing a N-order iterative scheme, we prove the local existence and uniqueness of a weak solution. Furthermore, we show that the sequence associated with N-order iterative scheme converges to the unique weak solution at a rate of N-order.

• Nonlinear Functional Analysis and Applications
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• 제27권3호
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• pp.679-689
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• 2022

In this paper, we establish sufficient conditions for the existence and uniqueness of solution for a class of initial boundary value problems with Dirichlet condition in regard to a category of fractional-order partial differential equations. The results are established by a method based on the theorem of Lax Milligram.