• 제목/요약/키워드: Ferric oxide

검색결과 116건 처리시간 0.029초

표준물첨가 및 희석법을 이용한 주석 슬랙중$Ta_2O_5$,$Nb_2O_5$$SnO_2$의 X-선 분광분석 (X-Ray Spectrometric Analysis of $Ta_2O_5$,$Nb_2O_5$ and $SnO_2$in Tin Slags using Standard Addition and Dilution Method)

  • 김영상;이동휘
    • 대한화학회지
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    • 제27권6호
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    • pp.424-482
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    • 1983
  • 분석시료에 일정량의 표준물을 첨가한 후 희석제로 묽히는 방법을 이용하여 주석슬랙중의 $Ta_2O_5$,$Nb_2O_5$$SnO_2$를 X-선 분광 분석법으로 정량하였다. 희석제로는 $SiO_2$$Fe_2O_3$를 사용하였으며 첨가시료와 1:1의 비로 희석 시켰다. $Ta_2O_5$$SnO_2$ 의 분석결과는 $Fe_2O_3$보다 $SiO_2$로 희석시킨 것이 표준 검정곡선법에 의해 얻은 분석값과 더 잘 일치하고, $Nb_2O_5$는 이와 반대로 $SiO_2$보다 $Fe_2O_3$로 희석시킨 것이 더 잘 일치함을 보여주었다.

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연소촉매 FeOOH를 포함하는 고체추진제 특성 연구: FeOOH의 소성온도 영향 (A study on the Properties of Solid Propellant Containing FeOOH Combustion Catalyst: Effect of FeOOH Calcination Temperature)

  • 전수아;박성준;김운재;박정호
    • 한국추진공학회지
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    • 제24권6호
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    • pp.10-15
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    • 2020
  • 본 연구는 동일한 제조법을 가지는 연소촉매 FeOOH와 Fe2O3를 제조하여 고체추진제에 적용 후 기계적 물성 및 연소 특성의 변화에 관한 내용이다. 동일한 제조방법을 가지는 FeOOH와 Fe2O3를 만들기 위하여 FeOOH를 200, 300, 400, 500℃에서 2시간 동안 소성시킨 후 XRD 결과를 확인하였다. 또한, 제조된 촉매를 고체추진제에 적용 후 기계적 물성 및 연소 특성의 변화를 나타내었다. XRD 결과상으로 FeOOH는 200~300℃사이에서 Geothite에서 Hematite로 결정상이 변화하는 것을 확인하였다. 추진제의 응력은 연소촉매의 소성온도가 높아짐에 따라 변화가 거의 없지만 연신율은 소성을 진행한 촉매를 적용 시 증가하였다. 연소속도는 소성을 하지 않은 FeOOH가 다른 촉매에 비해 약 3~5% 빠르다는 것을 확인하였다.

화학 첨가제와 밀가루의 열처리가 제빵 특성에 미치는 효과 (Effects of chemical additives and heat treatment on the baking properties of wheat flour dough)

  • 이지은;고봉경
    • 한국식품조리과학회지
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    • 제20권2호
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    • pp.119-125
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    • 2004
  • Mixograph를 이용하여 반죽의 물성에 미치는 화학첨가제의 영향을 조사한 결과 ammonium ferric citrate와 ferric sulfate는 0.1% 수준에서는 밀가루 반죽의 탄성에 뚜렷한 영향을 미치지 않았으나, MgSO$_4$, CaCl$_2$ 및 ZnO는 반죽의 탄성을 증가시키며 최적반죽시간을 연장시켜 반죽 시간이 길어졌다. 그러나 Ca과 Mg을 각각 갖는 calcium citrate와 MgCl$_2$는 반죽 시간이나 탄성에 뚜렷한 영향을 나타내지 않았다. 빵의 부피에 미치는 영향은 0.1% MgSO$_4$와 CaCl$_2$가 브롬산 칼륨을 전혀 첨가하지 않은 대조구보다 부피 팽창이 더 커져서 브롬산 칼륨과 같은 팽창제로서의 기능을 확인하였으며, 이들을 첨가한 빵의 속과 겉껍질의 색은 모두 대조구보다 더 밝아서 첨가한 화학첨가제들이 빵의 색을 밝게 하는 것을 확인할 수 있었다. 밀가루의 내재된 효소를 불활성화 시키기 위하여 볶음처리와 UV 및 microwave 조사된 밀가루는 최적 반죽시간을 초과하여 계속 반죽하여도 최적반죽시간 후 반죽의 탄성저하현상이 처리하지 않은 대조구에 비하여 감소되어 반죽의 안정성이 향상되었으나, 열처리한 밀가루로 제조한 빵은 부피가 대조구에 비하여 적었으므로 열처리는 반죽의 안정성은 향상시킬 수는 있으나 빵의 부피 증가에는 효과적이지 못하였다.

스테키히트 시험용 자동 발색 인지 시스템 개발을 위한 기초연구(I) - Stockigt 사이즈도 시험법에 영향을 주는 요인 분석 - (Automatic Color Recognition System for Stockigt Sizing Test (I) - Bias of Stockigt sizing test based on observer's subjectiveness -)

  • 김재옥;김철환;박종열
    • 펄프종이기술
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    • 제36권1호
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    • pp.1-8
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    • 2004
  • One of the most frequently used method for measurement of the degree of sizing (viz., hydrophobicity) is the Stockigt test. However, the Stockigt test was influenced by various factors such as dropping height, dropping amount, dropping speed and viewing angle. The resultant data of the sizing degree on the same specimen also varied according to different testers. Thus, the Stockigt test should be modified to be regarded as a highly reliable and reproducible standard method. For modifying the Stockigt test, it was required to quantify red coloration by reaction between 1% ferric chloride and 2% ammonium thiocyante during Stockigt testing. The cameras capturing the serial images during the red coloration process were the CMOS (Complementary Metal Oxide Semiconductor)-type and CCD (Charge Coupled Device)-type cameras. For measurement based on KS M 7025, the CCD-type camera must be used due to its high resolution, and on the other hand, for measurement based on Tappi Useful Method 429, the CMOS-type camera may be used owing to its low resolution. It was needed to covert the RGB values of a droplet image into HSV(Hue, Saturation, and Value) values because the human eyes are much closer to HSV than RGB. Among HSV values, the Hue value was accepted as the most reliable index consistent with the red coloration process by excluding the surrounding conditions such as light, tester's movement etc.

방글라데시 식물 추출물의 항산화 및 항염 효과 연구 (Antioxidant and Anti-inflammatory Effects of Plant Extracts from Bangladesh)

  • 유소현;김건희
    • 한국식생활문화학회지
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    • 제35권6호
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    • pp.605-612
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    • 2020
  • In this study, 11 plant extracts from Bangladesh were used to evaluate the total phenolic and flavonoid content, in vitro antioxidant activities using 2,2-diphenyl-1-picrylhydrazyl (DPPH), 2,2-azinobis-(3-ethylbenzthiazolin-6-sulfonic acid) (ABTS), and ferric reducing antioxidant power (FRAP) assay. Also, the inhibitory effect of nitric oxide (NO) production in RAW 264.7 macrophage cell line and the neuroprotective effect on H2O2-induced PC12 cells were tested. Our results revealed that Piper betle L. showed the highest total phenolic content (162.2 mg GAE/g extract) among the 11 plants from Bangladesh. Most plants showed strong radical scavenging effects and ferric reducing antioxidant power. Besides, Piper betle L. protected PC12 neuronal cells against H2O2 related oxidative stress in LPS-induced PC12 cells. Regarding the anti-inflammatory effect, Piper betle L. significantly inhibited NO accumulation in LPS-induced RAW 264.7 cells. Our results provide evidence that Piper betle L. could be useful for the development of functional health foods.

Direct and Indirect Reduction of Cr(VI) by Fermentative Fe(III)-Reducing Cellulomonas sp. Strain Cellu-2a

  • Khanal, Anamika;Hur, Hor-Gil;Fredrickson, James K.;Lee, Ji-Hoon
    • Journal of Microbiology and Biotechnology
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    • 제31권11호
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    • pp.1519-1525
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    • 2021
  • Hexavalent chromium (Cr(VI)) is recognized to be carcinogenic and toxic and registered as a contaminant in many drinking water regulations. It occurs naturally and is also produced by industrial processes. The reduction of Cr(VI) to Cr(III) has been a central topic for chromium remediation since Cr(III) is less toxic and less mobile. In this study, fermentative Fe(III)-reducing bacterial strains (Cellu-2a, Cellu-5a, and Cellu-5b) were isolated from a groundwater sample and were phylogenetically related to species of Cellulomonas by 16S rRNA gene analysis. One selected strain, Cellu-2a showed its capacity of reduction of both soluble iron (ferric citrate) and solid iron (hydrous ferric oxide, HFO), as well as aqueous Cr(VI). The strain Cellu-2a was able to reduce 15 μM Cr(VI) directly with glucose or sucrose as a sole carbon source under the anaerobic condition and indirectly with one of the substrates and HFO in the same incubations. The heterogeneous reduction of Cr(VI) by the surface-associated reduced iron from HFO by Cellu-2a likely assisted the Cr(VI) reduction. Fermentative features such as large-scale cell growth may impose advantages on the application of bacterial Cr(VI) reduction over anaerobic respiratory reduction.

Comparison of Low Concentration and High Concentration Arsenic Removal Techniques and Evaluation of Concentration of Arsenic in Ground Water: A Case Study of Lahore, Pakistan

  • Yasar, Abdullah;Tabinda, Amtul Bari;Shahzadi, Uzma;Saleem, Pakeeza
    • Korean Chemical Engineering Research
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    • 제52권5호
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    • pp.620-626
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    • 2014
  • The main focus of this study was the evaluation of arsenic concentration in the ground water of Lahore at different depth and application of different mitigation techniques for arsenic removal. Twenty four hours of solar oxidation gives 90% of arsenic removal as compared to 8 hr. or 16 hr. Among oxides, calcium oxide gives 96% of As removal as compared to 93% by lanthanum oxide. Arsenic removal efficiency was up to 97% by ferric chloride, whereas 95% by alum. Activated alumina showed 99% removal as compared to 97% and 95% removal with bauxite and charcoal, respectively. Elemental analysis of adsorbents showed that the presence of phosphate and silica can cause a reduction of arsenic removal efficiency by activated alumina, bauxite and charcoal. This study has laid a foundation for further research on arsenic in the city of Lahore and has also provided suitable techniques for arsenic removal.

Antioxidant and Oxidative DNA Damage Protection Potential of Methanol Extract of Red Tea Stem

  • Yadav, Anil Kumar;Kang, Sun Chul
    • Current Research on Agriculture and Life Sciences
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    • 제31권2호
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    • pp.101-107
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    • 2013
  • This study was undertaken to determine free radical scavenging capacity and oxidative DNA damage protecting activity of methanol extract of red tea stem. The extract was subjected to assess their antioxidant potential using various in vitro systems such as $DPPH^{\bullet}$, $ABTS^{{\bullet}+}$, super oxide and nitric oxide free radicals and it exhibited $IC_{50}$ values of $68.88{\pm}1.1$, $12.08{\pm}0.65$, $404.38{\pm}1.6$, $93.6{\pm}2.7{\mu}g/mL$ respectively. Red tea extract also showed ferric reducing ability (FRAP) with 2606.85 mmol Fe (II)/g of extract. Furthermore, Methanol extract of red tea stem showed significant DNA damage protecting activity in concentration dependent manner against $H_2O_2+UV$ induced photolysis on pUC19 plasmid DNA. Results of this study showed that the methanol extract of Red Tea stem has strong antioxidant potential along oxidative DNA damage protecting capacity that would be the significant sources of natural antioxidants, which might be helpful in preventing the progress of various oxidative stress generated diseases. Further study is necessary for isolation and characterization of the active antioxidants, which may serve as a potential source of natural antioxidant.

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Antioxidant and NO-scavenging Activities of Acanthopanax senticosus var. subinermis Leaf Extracts Prepared Using Ethanol and Extrusion Processing

  • Lee, Sung-Hee;Oh, Hea-Young;Leem, Jae-Yoon;Yoon, Sun
    • Food Science and Biotechnology
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    • 제18권5호
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    • pp.1124-1131
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    • 2009
  • Acanthopanax senticosus has been used in East Asia as a traditional medicine. The purpose of this study is the investigation of an extraction method for A. senticosus var subinermis (ASvS) leaves to improve their antioxidant and anti-inflammatory activities. Six extracts were prepared: extracted with water (W), ethanol (Eth), water or ethanol after ultra high pressure (WP, EthP), and water or ethanol after an extrusion process (WEx, EthEx). Diphenylpicrylhydrazyl (DPPH) radical scavenging activity and ferric reducing ability showed that all extracts had a significant antioxidant activity. In anti-inflammatory activities, Eth and EthEx significantly inhibited the release of lipopolysaccharide (LPS)-induced nitric oxide (NO), tumor necrosis factor (TNF)-${\alpha}$, and interleukin (IL)-$1{\beta}$ independent of cell viability in RAW 264.7 macrophage cells. Inducible NO synthase (iNOS) protein was significantly decreased by EthEx. These findings present that Eth and EthEx extracts of ASvS leaves have anti-inflammatory activities, and EthEx extract suppresses LPS-induced NO through the down-regulation of iNOS and pro-inflammatory cytokines.

황색산화철을 포함하는 혼합형 고체추진제의 특성에 관한 연구 (2) (Composite Solid Propellants for Propulsion System Including a Yellow Iron Oxide (2))

  • 박성준;김경민;박정호;노태호;최성한
    • 한국추진공학회지
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    • 제24권3호
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    • pp.12-17
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    • 2020
  • 황색 산화철을 적용한 추진제의 기계적 특성은 적색산화철을 적용한 추진제와 비교하여 기계적물성이 다소 증가하였다. 또한 황색산화철을 적용한 추진제는 두 종류의 AP 입자를 사용하였으며 총량을 유지하고 작은 입자의 AP 비율 증가 시 연소속도가 증가하였다. 황색산화철을 첨가한 추진제는 압력 지수 값이 0.5인 17.5 mm/sec 이하의 운용조건에서 추진기관에 적용 가능하다. 혼합 믹서 Scale-up 시연소속도 감소, 최대인장강도 감소, 최대인장강도에서의 연신율은 증가하였다. 황색산화철은 내열재/라이너/추진제 사이의 접착력에는 큰 영향을 끼치지 않는다.