• 제목/요약/키워드: Experiment sample

검색결과 1,312건 처리시간 0.027초

촉매적(觸媒的) 제탄(製炭)에 관(關)한 시험(試驗) (Studies on the catalytic charcoaling)

  • 박태식;박명규
    • 한국산림과학회지
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    • 제3권1호
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    • pp.18-22
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    • 1963
  • 1. Objects The experiments of catalytic aharcoaling were carried out for the fallowing purposes. (1) To determine the economically desirable amount of catalytic materials to be used when a catalytic charcoaling is practiced. (2) To observe the rate of carbonization of non-treated charcoal wood when the catalytic charcoaling is proceeded in the same charcoal pit. 2. Meterials (1) Small sample chips made of oak (Q. accutissima Carr.), measured by 0.5cm in width and thickness, respectively, and 1cm in length, were used as charcoal wood in each experiment. (2) Ammonium chloride was used as a catalytic material and electric kiln as a charcoaling apparatus. 3. Experiment (1) The sample chips were put into a electric oven for three hours at the temperature $60^{\circ}{\sim}70^{\circ}C$ in order to reduce some water contents. (2) Oven dried sample chips were then soaked for an hour in solution of ammonium chloride. Three kinds of solution were prepared, that is, 2.5%, 5%, and 10%, solution in which the amount of ammonium chloride used was weighed at the rate of 0.5%, 1.0%, and 2.0% to the total weight of the sample chips, resppectivelly. (3) Soaked sample chips were put in the air for 12 hours to reduce some water contents, and then were put into electric oven for 2 hours at the temperature $105^{\circ}{\sim}110^{\circ}C$. (4) Dried sample chips were kept in a desiccator with control sample chips which were treated excarly the same process as the treated sample chips except only not using the ammonium chloride in the process of soking. (5) Sample chips kept in the desiccator were used at random in each charcoaling experiment. (6) Charcoaling in the electric kiln were carried out by using small crucibles with complete cover to reduce the amount of ash. At each charcoaling experiment four crucibles filled with sample ships, weighed about 20gr, were put into electric kiln. The charcoaling was continued for an hour at the temperature $400^{\circ}{\sim}450^{\circ}C$. (7) In order to investigate the influence given by the gases produced during the catalytic charcoaling to the rate of carbonization of non-treated sample chips, the following experiment was done. (a) A crueible was divided into two parts by inserting a fine iron net at the middle of the crucible, and then non-treated sample chips, weighed about 10gr, were put in the upper part of the crucible and treated sample chips, weighed also about 10gr, were put in the under part. (b) The crucibles filled with two kinds of sample chips were put into a electric kiln for an hour at the temperature $400^{\circ}{\sim}450^{\circ}C$. 4. Results. Results for two replications (with four crucibles in one replication) for each experiment designed are as follows : (1) The rats of carbonization of the non treated sample chips, and that of the treated sample chips with ammonium chloride at the rate of 1.5%, 1.0%, and 2.0% to the total weight of the sample chips used were averaged at 19.85%, 22.63%, 24.14%, and 26.60%, respectively. (2) The rats of carbonization of the non-treated sample chips were averaged at (a) 20.04% (0.5% treatment), (b) 20.28% (1.0% treatment), and (c) 20.61% (2.0% treatment) when the treated sample chips were carbonized in the same crucible.

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고온가열된 어류의 돌연변이성 검색을 위한 시료 추출방법 (Method for the Detection of Mutagenicity of Fried Fish)

  • 이은주;반경녀;이영근;심기환;하영래
    • 한국환경성돌연변이발암원학회지
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    • 제15권2호
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    • pp.106-114
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    • 1995
  • A method was developed to detect total mutagenicity of fried fish for S. typhimurium TA98, using Ames assay. Method described herein circumvented problems associated with the sample preparation for Ames assay, i.e., a multi-purification step of sample and interference with solvent residuals. Experiment A, the best method developed in the present study, consisted of two important steps: pH adjustment of the aqueous sample solution from fried fish samples to remove impurities, and simultaneous distillation extraction (SDE) for partially purified samples to remove volatile compounds from solvents. The procedure and results were described as below. Fillet of gizzard shad (Konosirus punctatus) fish sample fried for 10 min each side on the temperature-controlled fry-pan (210$\circ$C) was homogenized in an aqueous acidic solution (pH 2) with a homogenizer, followed by filtration through Celite. The tiltrate (pH 2), removed some impurities by extraction with chloroform:methanol (2:1, v/v) mixture, was adjusted pH to 10 and then centrifuged to remove precipitate. The ethylacetate extract from the tiltrate of pH 10 was rotoevaporated and purified by SDE apparatus for 2 hours. Experiment A revealed significantly higher revertants (1928 per 25 g fried sample) than other Experiment (B, C, or D) tested. Experiment A gave good results in the mutagenicity test of fried fish sample with few purification steps using only 25 g fried sample and 650 ml of solvents; and thus this method could be a useful tool for the screening the mutagenicity or antimutagenicity of other foods as well.

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Analysis of Protein and Moisture Contents in Pea(Pisum sativum L. Using Near-Infrared Reflectance Spectroscopy

  • Jung, Chan-Sik;Kim, Byung-Joo;Kwon, Yil-Chan;Han, Won-Young;Kwack, Yong-Ho
    • 한국작물학회지
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    • 제43권2호
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    • pp.101-104
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    • 1998
  • This study was conducted to establish a rapid analysis method for determining protein and moisture contents of pea. Ninety and eighty pea (Pisum sativum L.) lines were analyzed to determine protein and moisture contents, respectively using near-infrared reflectance spectroscopy. Simple correlations (${\gamma}$) of protein content in a ground sample and an intact grain sample by an automatic regression method were 0.978 and 0.910, respectively. Simple correlations by partial least square regression/principal component analysis (PLS/PCA) methods were 0.982 and 0.925, respectively. Standard error of performance (SEP) in protein content was the lowest value, 0.446 in ground sample by PLS/PCA methods. Simple correlation of moisture content was the highest at 0.871 in ground samples. when using a standard regression method. Accuracy for the moisture content was slightly lower than for protein content. It was concluded that the NIRS method would be applicable only for rapid determination of protein content in pea.

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향부자팔물탕(香附子八物湯)이 흰쥐의 방사형 미로학습(迷路學習)과 기억(記億)에 미치는 영향(影響) (The Experimental Study on the Effects of Hangbujapalmultang on Enhancing Learning and Memory in Rats with Radial Arm Maze)

  • 유재면;김종우;항의완;김현택;이홍재
    • 동의신경정신과학회지
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    • 제9권2호
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    • pp.45-51
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    • 1998
  • Purpose : This study has an experiment on finding how Hyangbujapamultang advanced the learning and memory of rat to find the method to improve the failure of memory which is the symptom of dementia.Method : In the experiment, rats were divided the control group (14 rat) which medicate the excipient into the sample group (17 rat) which medicates Hyangbujapalmutang. And the learning ability test and the memorv test was practiced to using the task of radial arm maze.The learning ability test had the presupposition that, when a rat which frequents 8 tracks makes am error not exceeding one time for 3 days without a break, it passes the test.First experiment compared total days when the control group passed the test with total days when the sample group it.The memory test practiced after 24 hours when the learning ability test was over. When a rat frequents 4 tracks, the gates is cut off during 30 seconds. Here the number of error at the control group with that of the sample group.Result: In the learning ability test, the sample group needed 5.82${\pm}$0.37 days to pass the test and the control group needed 6.43${\pm}$0.67 days. In the memory test, the sample group errored 0.29${\pm}$0.37 times and the control group errored 1.86${\pm}$0.78 times.Conclusion : In the learning ability test, the sample group passed the test earlier than the control group, but any statistical correlationship couldn't be found in it. In the memory test, the sample group had the pregnant reduction of the number of error in comparison with the control group.

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측정을 목적으로 시료에 변형을 가하지 않아도 되는 새로운 관성모멘트 실험 장치의 개발 (Development of a New Moment of Inertia Experiment Apparatus That Does Not Require Deformation of a Sample for Measurement Purpose)

  • 남형주
    • 공학교육연구
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    • 제23권3호
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    • pp.32-40
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    • 2020
  • A new moment of inertia experiment apparatus different from the existing one has been developed, which does not require deformation of a sample in order to fix it to the apparatus. This new experiment apparatus was able to experiment with constant-shaped objects that did not deform the samples, so that it enabled them for conducting an experiment which is close to an ideal rigid model dealt in the general physics course. The new experimental apparatus was easy and accurate in measuring the physical quantity by using the experimental principle of physical pendulum. In the results of the measurement of the moments of inertia of the six samples, all measurements were made to be accurate enough to measure with very small errors within 1%. In addition, it has been found to be useful as an experiment apparatus to understand the concept of the moment of inertia and to prove the formula for moment of inertia. Therefore, if the new moment of inertia experiment apparatus developed in this study is used in students' experiments, it is expected that students will be able to greatly increase their understanding of the concept of moment of inertia.

A Bayesian Multiple Testing of Detecting Differentially Expressed Genes in Two-sample Comparison Problem

  • Oh Hyun-Sook;Yang Wan-Youn
    • Communications for Statistical Applications and Methods
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    • 제13권1호
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    • pp.39-47
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    • 2006
  • The Bayesian approach to multiple testing procedure for one sample testing problem proposed by Scott and Berger (2003) is extended to two-sample comparison problem in microarray experiments. The prior distribution of each gene's mean for one sample is given conditionally on the corresponding gene's mean for the other sample. Posterior distributions of interesting parameters are derived and estimated based on an importance sampling method. A simulated example is given for illustration.

작약근의 박피와 시료형태가 건조시간 및 Paeoniflorin 함량에 미치는 영향 (Effects of Peeling and Sample types on Drying Time and Paeoniflorin Contents of Peony Root)

  • 김기재;박준홍;박소득;김재철;박경석
    • 한국약용작물학회지
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    • 제10권1호
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    • pp.24-28
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    • 2002
  • 작약의 양질약재 생산을 위한 기초 자료를 얻고자 건조과정중 박피시간별 절단과 무절단 그리고 열풍건조 온도를 달리하여 시험한 결과를 요약하면 다음과 같다. 박피시간이 길어질수록 건조시간은 통뿌리보다 절단한 것이 건조온도가 단축되었으며, $30^{\circ}C$에서 $60^{\circ}C$까지의 건조온도에서 건조온도가 상승할수록 온도상승의 효과는 감소하였다. 작약의 주 약용성분인 paeoniflorin 함량은 무박피 절단형태로 열풍온도 $30^{\circ}C$에서 건조한 작약이 3.48%로 가장 높은 함량을 유지하였고, 120분 박피후 통뿌리로 $60^{\circ}C$에 열풍건조한 작약은 2.29%로 건조과정중 많은 양이 손실되어 가장 낮게 나타났다. 건조작약의 외부색택은 통뿌리로 $60^{\circ}C$에서 열풍건조했을 때 흑갈색으로 변하는 정도가 가장 심했다. 따라서 작약 수확후 건조과정 중 건조시간 단축과 약효성분 그리고 색택면에서 건조전의 처리 방법은 무박피 절단형태가 장시간 박피 원형형태보다 우수한 것으로 판단된다.

운전 중 실내 소음의 유형 및 강도에 따른 주관적 속도감에 관한 연구 (A Driving Study on Driver's Subjective Speed Estimation as a Function of the Vehicle Noise Types and Intensity)

  • 공대호;이준범;이재식
    • 한국심리학회지 : 문화 및 사회문제
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    • 제11권2호
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    • pp.31-46
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    • 2005
  • 본 연구는 운전 중 발생하는 청각 자극의 유형 및 정도가 운전자가 지각하는 주관적 속도감에 어떠한 영향을 미치는지를 알아보고자 수행되었다. 본 연구에서 사용된 청각 자극은 엔진 소음과 음악 소리였으며 전자는 자동차의 속도에 따라 함께 변하는 청각 단서인 반면 후자는 자동차의 속도와는 무관하게 변화하는 비단서 소음으로 사용되었다. 엔진 소음의 강도만 조작되어 제시된 실험 1에서는 엔진 소음의 크기에 따라 운전자가 느끼는 주관적 속도감이 다르게 나타나 운전자들은 엔진 소음이 작을수록 기준속도보다 더 빨리 주행한 반면 엔진 소음이 클수록 더 천천히 주행하는 것이 관찰되었다. 실험 2에서는 엔진 소음과 음악 소리를 모두 들려주었는데, 그 결과 엔진 소음의 크기변화에 따른 주관적 속도감의 차이는 여전히 나타났으나 음악 소리의 크기변화에 따른 속도감의 차이는 보이지 않았다. 또한 실험 1과 2를 통합하여 음악 소리의 유무효과를 분석해 본 결과 음악 소리가 엔진 소음을 차폐시킬 만큼 크고 엔진 소음이 작을 경우에는 음악 소리가 없는 경우보다 속도를 더 내는 것으로 나타났다. 이는 음악 소리가 속도감에 영향을 주는 직접요인은 아니지만 간접적으로 영향을 미친다는 가능성을 시사한다.

소양인(少陽人) 형방도적산(荊防導赤散)의 효능(效能)에 관(關)한 실험적(實驗的) 연구(硏究) (Experimental Studies on the Effects of Soyangin - Hyongbangdojoksan)

  • 최병일
    • 사상체질의학회지
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    • 제2권1호
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    • pp.167-178
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    • 1990
  • In order to investigate experimentally the clinical effect of Soyangin-Hyongbangdojoksan (少陽人荊防導赤散) that was prescribed to cure the Bisuhanpyohanbyong (脾受寒表寒病) of Soyangin (少陽人). The author experimented various activities of dried extract from hyongbangdojoksan (Sample-I) and mixed extract of each dried extract of hyongbangdojoksan (Sample-II) by the methods prescribed in the experimental parts. The results summarized as follows. 1. In the acetic acid method experiment, analgesic effect was noted in sample-I & Sample-II. 2. Anti-inflammatory effect on the edema induced by carrageenin was noted in Sample-I. 3. Antipyretic effect is not noted in Sample-I and Sample-II. 4. On urinary volume change and blood electrolyte clearance, the result is not significant, on the contrary the urine electrolyte discharge is effective in Sample-I and Sample-II. According to the above results, the effects based on oriental medical references approximate to the actual experimental results.

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자동차 시트의 인간공학적 디자인에 따른 착좌 안락감 및 압력분포 평가 (Evaluation of Seat Comfort and Pressure Distribution According to the Ergonomic Design of Automobile Seats)

  • 정하림;최준원;양승완;박준규;김도용;송창현;김종배;김한성
    • 대한의용생체공학회:의공학회지
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    • 제44권2호
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    • pp.157-165
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    • 2023
  • The purpose of this study was to evaluate the importance of developing slim seats with ergonomic design to improve seat comfort and expand the interior space. Two seats were used for the experiment: a sample seat designed based on hip shape and spinal alignment and a normal seat with a flat design without curves. Subjects sat in both the sample seat and a normal seat applied to the vehicle simulator and the experiment was conducted. The next part of the experiment was conducted in two different postures: a driving posture and a relaxed posture. The subjects filled out a comfort questionnaire immediately after sitting and after 30 minutes. The results showed that the comfort in the sample seat was found to be more comfortable than the normal seat. However, no significant difference was noted for the relaxation posture. Pressure distribution was also recorded immediately after sitting and after 30 minutes. In the case of pressure distribution, it was confirmed that the pressure in the sample seat was more evenly distributed in both the driving and relaxed postures than in the normal seat. The results showed that the ergonomically designed sample seat greatly improved seating comfort and pressure distribution compared to the normal seat, which is a general vehicle seat design.