• Journal of Adhesion and Interface
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• v.21 no.1
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• pp.20-26
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• 2020

Single lap-shear joints (SLJ) specimens with and without partial round fillets were fabricated to measure the average shear strength of adhesives. The effects of the length of the adherend on the SLJ specimens were also investigated. An epoxy adhesive was used to bond aluminum alloy. Tensile tests were performed on the adhesive bulk specimens to measure the mechanical properties. The finite element analysis (FEA) method was used to measure the adhesive stress distributions, i.e., the peel and shear stresses, on the bonded part. The experimental results revealed that the specimen consisting short length of adherend and without the partial round fillets exhibited the smallest average shear strength of adhesive among the investigated specimens. FEA revealed that the low average shear strength for the specimen with a short adherend length was caused by high stress concentrations on the adhesive at the edge of the bonded part.

• Journal of Power Electronics
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• v.13 no.6
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• pp.1080-1089
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• 2013

In this paper, the superposition principle of a heat sink temperature rise is verified based on the mathematical model of a plate-fin heat sink with two mounted heat sources. According to this, the distributed coupling thermal impedance matrix for a heat sink with multiple devices is present, and the equations for calculating the device transient junction temperatures are given. Then methods to extract the heat sink thermal impedance matrix and to measure the Epoxy Molding Compound (EMC) surface temperature of the power Metal Oxide Semiconductor Field Effect Transistor (MOSFET) instead of the junction temperature or device case temperature are proposed. The new thermal impedance model for the power converters in Switched Reluctance Motor (SRM) drivers is implemented in MATLAB/Simulink. The obtained simulation results are validated with experimental results. Compared with the Finite Element Method (FEM) thermal model and the traditional thermal impedance model, the proposed thermal model can provide a high simulation speed with a high accuracy. Finally, the temperature rise distributions of a power converter with two control strategies, the maximum junction temperature rise, the transient temperature rise characteristics, and the thermal coupling effect are discussed.

• Korean Chemical Engineering Research
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• v.54 no.3
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• pp.410-418
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• 2016

In this study, we prepared electrically conducting composites using epoxy resin of diglycidyl ether of bisphenol A (DGEBA) as a matrix, triethylenetetramine (TETA) as a hardener and nickel powder or multi-walled carbon nanotubes (MWCNTs) grafted with $-NH_2$ groups (MWCNT-$NH_2$) as electrically conducting fillers. Electrical conductivity of composite films were measured by coating on the slide glass with a doctor blade. We measured modification reactions of MWCNT and reaction of MWCNT-$NH_2$ with DGEBA epoxy resin by fourier transform infrared spectrometer (FTIR), thermogravimetric analyzer (TGA) and elemental analyzer (EA). Morphology of composites was investigated by scanning electron microscope (SEM) and sheet resistances of composites were measured by 4-point probe. We found $(9.87{\pm}1.09){\times}10^4{\Omega}/sq$ of sheet resistance for epoxy composite containing both 40 wt% nickel powder and 0.5 wt% of MWCNT-$NH_2$ as fillers, equivalent to epoxy composite containing 53.3 wt% nickel powder only as a filler.

• Composites Research
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• v.29 no.5
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• pp.306-314
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• 2016

In this study, to improve the thermal stabilities of the epoxy composite specimens in addition to the enhanced mechanical properties, those were reinforced with carbon nanotubes and micrometer-sized silica particles. To disperse the filler in matrix relatively simple physical process, specimens were fabricated using shear mixing and sonication. Tensile strength, coefficients of thermal expansion and thermal conductivity of the specimens were measured with varied contents of the two fillers. The mechanical and thermal properties were also discussed, and the experimental results of thermal expansion related to the thermal stability of the specimens were compared with those from several micromechanics models. The hybrid composites specimens incorporating 0.6 wt％ of carbon nanotubes and 50 wt％ of silica particles showed better mechanical properties than the others with increase in tensile strength up to 11％, with respect to those of the baseline specimens. As the silica contents were increased the thermal expansion was reduced down to 36%, and the thermal stability was improved with the decreased thermal deformation. Thermal conductivity of the epoxy composite specimens incorporating 50 wt％ of silica particles was enhanced, which demonstrate improvement of 72%. The mechanical and thermal properties of the hybrid composites specimens incorporating the two fillers were improved simultaneously.

• Composites Research
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• v.30 no.3
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• pp.169-174
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• 2017

Demand of glass fiber reinforced composites (GFRC) increased with developing aircraft and defense industries using resin transfer molding (RTM) process to produce complex product. In this research, wetting, interfacial, and mechanical properties were evaluated with different Cross-linking Density by Molecular Weight of Hardener. Epoxy resin as matrices was used bisphenol-A type and amine-type hardeners with different molecular weight. Specimens were manufactured via RTM and wetting property of resin and glass fiber (GF) mat was evaluated to viscosity of epoxy and injection time of epoxy matrix. Mechanical property of GFRC was determined via flexural strength whereas interfacial properties were determined by interlaminar shear strength (ILSS) and interfacial shear strength (IFSS). The difference in mechanical property depends upon the fiber weight fraction (wt %) of GFRC by RTM as well as the different Molecular Weight of Hardener.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.39 no.6
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• pp.567-573
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• 2015

This paper aims to evaluate the variation in the mechanical properties of carbon/epoxy composites under in situ low- and high-temperature environments. In situ low- and high-temperature environments were simulated with temperature ranging from $-40^{\circ}C$ to $220^{\circ}C$ using an environmental chamber and furnace. The variation in the mechanical properties of the composites was measured for longitudinal and transverse tensile properties, in-plane shear properties and interlaminar shear strength. Under the low temperature of $-40^{\circ}C$, all mechanical properties increased moderately compared to the baseline properties measured at room temperature. The changes in the longitudinal tensile properties decreased moderately with increasing temperature. However, transverse tensile properties, in-plane shear properties and interlaminar shear strength each showed a significant drop due to the glass transition behavior of the matrix after $140^{\circ}C$. Notably, the tensile property value near $100^{\circ}C$ increased compared to baseline property value, which was an unusual occurrence. This behavior was a direct result of post-curing of the epoxy resin due to its exposure to high temperature.

• Composites Research
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• v.16 no.3
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• pp.25-31
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• 2003

In this work the effect of surface treated SiC on thermal stability and mechanical interfacial properties of carbon fiber/epoxy resin composites. The surface properties of the SiC were determined by acid/base values and contact angles. The thermal stabilities of carbon fiber/epoxy resin composites were investigated by TGA. The mechanical interfacial properties of the composites were studied in ILSS, critical stress intensity factor ($\textrm{K}_{IC}$), and critical strain energy release rate($\textrm{G}_{IC}$) measurements. As a result, the acidically treated SiC(A-SiC) had higher acid value than untreated SiC(V-SiC) or basically treated SiC(B-SiC). According to the contact angle measurements, it was observed that chemical treatments led to an increase of surface free energy of the SiC surfaces, mainly due to the increase of the specific(polar) component. The mechanical interfacial properties of the composites including ILSS, $\textrm{K}_{IC}$, and $\textrm{G}_{IC}$ had been improved in the specimens treated by chemical solutions. These results were explained that good wetting played an important role in improving the degree of adhesion at interfaces between SiC and epoxy resin matrix.

• Applied Chemistry for Engineering
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• v.19 no.5
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• pp.471-476
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• 2008

The thermal and mechanical properties and morphology of epoxy/polyamide/DDS/2E4MZ-CNS reactive blends with various amounts of polyamide were investigated. The amount of polyamide was 10, 20, and 30 phr and 2 phr of catalyst was added to the blend to cure at $180^{\circ}C$ for 30 min. By adding the catalyst, 2E4MZ-CNS, to the blend, the cure reaction occurred at a lower temperature. From the SEM images, it was found that the boundary of separated-phase was unclear and the phase was co-continuous. Without the catalyst, however, the boundary of separated-phase was clear. The control of cure temperature and morphology could be achieved by using a proper catalyst and consequently the mechanical strength increased by 20% compared to the blend without the catalyst due to the strong interaction between epoxy matrix and phase-separated polyamide at the interface.

• Composites Research
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• v.26 no.3
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• pp.175-181
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• 2013

The evaluation and prediction for the absorbed energy, residual velocity, and impact damage are the key things to characterize the impact behavior of composite laminated panel subjected to high-velocity impact. In this paper, the method to predict the residual velocity and the absorbed energy of Carbon/Epoxy laminated panel subjected to high velocity impact are proposed and examined by using quasi-static perforation test and high-velocity impact test. Total absorbed energy of specimen due to the high-velocity impact can be grouped with static energy and kinetic energy. The static energy are consisted of energy due to the failure of the fiber and matrix and static elastic energy, which are related to the quasi-static perforation energy. The kinetic energy are consisted of kinetic energy of moving part of specimen, which are modelled by three modified kinetic model. The high-velocity impact test were conducted by using air gun impact facility and compared with the predicted values. The damage area of specimen were examined by C-scan image. In the high initial impact velocity above the ballistic limit, both the static energy and the kinetic energy are known to be the major contribution of the total absorbed energy.

• Composites Research
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• v.27 no.3
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• pp.90-95
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• 2014

Cure shrinkage during cure process of polymer matrix composites develope residual stress that cause some structural deformation, such as spring-in, spring-out and warpage. The carbon/epoxy prepreg used in this study is Hexply M21EV/34%/UD268NFS/IMA-12K supplied by Hexcel corp. Cure shrinkage and degree of cure measured by TMA(thermomechanical analyzer) and DSC(differential scanning calorimetry). Cure shrinkages are measured by TMA within a temperature range of $140{\sim}240^{\circ}C$ in a nitrogen atmosphere, and degree of cure determined by the heat of reaction using dynamic and isothermal DSC runs in argon atmosphere. As a result, the cure shrinkage is increased dramatically in a degree of cure range between 27~80%. the higher the cure temperature, the lower the degree of cure occurring to begin cure shrinkage.