• Title/Summary/Keyword: Epoxy composite

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An Experimental Evaluation of Mechanical Properties and Failure Processing in Composite Laminate (복합재료의 기계적 성질 및 파손과정 평가)

  • J.W.,Ong;K.H.,Song;R.W.,Sung;B.S.,Shim
    • Bulletin of the Society of Naval Architects of Korea
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    • v.25 no.4
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    • pp.58-68
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    • 1988
  • This paper is concerned with mechanical properties of unidirectional laminate $[(0^{\circ})_{8T},\;(90^{\circ})_{8T}]$, composed of angle plies $[({\pm}15^{\circ})_{2S},\;({\pm}30^{\circ})_{2S},\;({\pm}45^{\circ})_{2S},\;({\pm}60^{\circ})_{2S},\;({\pm}75^{\circ})_{2S}$ and laminate $[(9^{\circ}/90^{\circ})_{2S},\;(90^{\circ}/{\pm}45^{\circ}/0^{\circ})_S,\;({\pm}45^{\circ}/0^{\circ}/{\pm}90^{\circ})_S,\;({\pm}45^{\circ}/90^{\circ}/0^{\circ})_S,\;(0^{\circ}/90^{\circ}/{\pm}45^{\circ})_S,\;(90^{\circ}/0^{\circ}/{\pm}45^{\circ})_S]$ under the condition of uniform strain tension. Also, experimental investigation was conducted $[10]_{8T}$, off-axis tensile test for intralaminar shear characterization. The experimental data on the failure criterion of tensor polynomial were compared with those from the classical laminate theory. Acoustic Emission experiments have been carried out to investigate the changes of the amplitude distributions of Acoustic Emission monitored during failure of tensile tests on Carbon/Epoxy composites.

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Optimization of Slurry Preparation Process for Soft Magnetic Green Sheet (연자성 복합체 후막용 슬러리 제조공정의 최적화)

  • Oh, Sea Moon;Lee, Chang Hyun;Shin, Hyo Soon;Yeo, Dong Hun;Kim, Jin Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.28 no.12
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    • pp.792-796
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    • 2015
  • With high integration of electronic components, power inductors are also miniaturized. Recently, thick film processes for small size power inductors were developed and commercialized. However, the thick film process to prepare soft magnetic green sheets was not reported enough. In this study, we used Fe-Si magnetic and CIP (carbonyl iron powders) as starting materials to lead to a bimodal particle size distribution in the sheet. We proposed a newly developed 'Modified slurry preparation process' to get well dispersed condition even at high solid contents. Using the new process, it was possible to prepare a well dispersed slurry over 70 vol% of solid. BYK-103 was better than BYK-111 as dispersant in this slurry and the optimum amount was 0.6 wt%. The optimized slurry was formed into a sheet by tape casting process and then the sheet was laminated. We conformed that small size powder, large size powder, and epoxy resin were well dispersed in the green sheet.

A Study on Microfailure Mechanism of Single-Fiber Composites using Tensile/Compressive Broutman Fragmentation Techniques and Acoustic Emission (인장/압축 Broutman Fragmentation시험법과 음향방출을 이용한 단섬유 복합재료의 미세파괴 메커니즘의 연구)

  • Park, Joung-Man;Kim, Jin-Won;Yoon, Dong-Jin
    • Composites Research
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    • v.13 no.4
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    • pp.54-66
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    • 2000
  • Interfacial and microfailure properties of carbon fiber/epoxy matrix composites were evaluated using both tensile fragmentation and compressive Broutman tests with an aid of acoustic emission (AE) monitoring. A polymeric maleic anhydride coupling agent and a monomeric amino-silane coupling agent were used via the electrodeposition (ED) and the dipping applications, respectively. Both coupling agents exhibited significant improvements in interfacial shear strength (IFSS) compared to the untreated case under tensile and compressive tests. The typical microfailure modes including fiber break of cone-shape, matrix cracking, and partial interlayer failure were observed during tensile test, whereas the diagonal slippage in fiber ends was observed under compressive test. For both loading types, fiber breaks occurred around just before and after yielding point. In both the untreated and treated cases AE amplitudes were separately distributed for the tensile testing, whereas they were closely distributed for the compressive tests. It is because of the difference in failure energies of carbon fiber between tensile and compressive loading. The maximum AE voltage for the waveform of carbon or basalt fiber breakages under tensile tests exhibited much larger than those under compressive tests, which can provide the difference in the failure energy of the individual failure processes.

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Impact Behaviors of Ni-plated Carbon Fibers-reinforced Epoxy Matrix Composites (니켈도금된 탄소섬유 강화 에폭시 수지 복합재료의 충격 특성)

  • 박수진;김병주;이종문
    • Polymer(Korea)
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    • v.27 no.1
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    • pp.52-60
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    • 2003
  • In this work, two types of Ni-plating, namely electrolytical and electroless Ni-platings on carbon fiber surfaces, were carried out to enhance the impact resistance of composites. And the comparison between electrolytical and electroless methods on their impact properties of composite system was studied. The surface properties of carbon fibers were characterized using XRD, SEM, and contact angle measurements. The impact behaviors were investigated using an Izod type impact tester. As experimental results, it was observed that electrolessly plated Ni layers had Ni-P alloys on carbon fiber surfaces as revealed by XRD, and electrolytically Ni-plated carbon fibers showed higher surface free energies than those of the electrolessly Ni-plated carbon fibers. In particular, the impact strengths of electrolessly Ni-plated carbon fibers-reinforced plastics were strongly increased. These results were probably due to the difference of wettabilities according to the different types of Ni-plating methods.

Structural Behavior Evaluation of Mg-GFRP Composite Single-Lap Bonded Joints With Different End Shapes (한 끝단 형상에 따른 마그네슘 합금과 유리섬유 복합소재 단일겹치기 본드 조인트 거동 분석)

  • Kim, Jung-Seok;Im, Jae-Young;Lee, Woo-Geun
    • Journal of the Korean Society for Railway
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    • v.17 no.6
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    • pp.391-396
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    • 2014
  • In this study, the strength of magnesium-GFRP/epoxy single-lap bonded joints are experimentally evaluated with different end shapes. In order to achieve this, four different single-lap joints with different end shapes are fabricated and the failure load is measured under tensile loading tests. From the test results, the single-lap joint with a square end exhibits the lowest failure load while the single-lap joint with reverse tapering and a spew fillet has the highest stress values. It has 11.1% higher failure strength than the single-lap joint with a square end.

Elasto-plastic behaviour of joint by inserting length of H-beam and structural laminated timber (H형강과 구조용집성재의 삽입길이에 따른 접합부의 탄소성 거동)

  • Kim, Soon Chul;Yang, Il Seung;Moon, Youn Joon
    • Journal of Korean Society of Steel Construction
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    • v.18 no.2
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    • pp.251-259
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    • 2006
  • In some cases, wooden structures are used for medium-rise buildings. It is therefore necessary to develop and test a new structural system for medium-rise buildings using wooden structures. This study deals with high-performance, laminated, timber-based composite members, which consist of structural laminated timber and H-beam. Simple beam tests were performed to determine the strength, stress distributions, and failure patterns of laminated timber. The main parameters are the insertinglength (1, 1.5, and 2 times the H-beam height) and the epoxy between the top/bottom flange of the H-beam and the top/bottom flange of the laminated timber. The results of the test show that the specimen with an inserting length that is 2 times the H-beam height was characterized by fairly god strength and stiffness.

Failure Behavior of Pin-jointed Composites under Hygrothermal Environments (열습환경을 고려한 핀 체결부 복합재 파괴거동)

  • Kim, Changyu;Hwang, Youngeun;Yoon, Sungho
    • Journal of the Korean Society of Propulsion Engineers
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    • v.17 no.2
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    • pp.31-38
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    • 2013
  • This research analyzed the acoustic emission signals collected from the pin loading tests and investigated the effect of hygrothermal exposure on the fracture behavior of the pin-jointed carbon fiber/epoxy composites. The composite specimens include: the Base specimen that has not been exposed to any environments, the RT specimen that has been immersed in room temperature water, and the HT specimen that has been immersed in high temperature water. According to the pin loading test, the RT and the HT specimens showed 2.2% and 13% decreases in the bearing strength compared to the Base specimen, respectively. The analysis of the acoustic emission signals showed different fracture acceleration points for three types of the specimens. Furthermore, for the RT and the HT specimens, the event from the matrix crack signals in the composites decreased. This shows the effect of the hygrothermal conditions on the acoustic emission signals. Additionally, upon investigating the fracture behaviors of the pin-jointed composites, the exposing specimens to hygrothermal environments decreases the interfacial characteristics of the composites.

Multi-stage Compression Molding Technology of Fast Curing CF/Epoxy Prepreg (속경화용 탄소섬유/에폭시 프리프레그의 다단 압축 성형기술)

  • Kwak, Seong-Hun;Mun, Ji-Hun;Hong, Sang-Hwui;Kwon, Soon-Deok;Kim, Byung-Ha;Kim, Tae-Yong
    • Composites Research
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    • v.34 no.5
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    • pp.269-276
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    • 2021
  • PCM (Prepreg Compression Molding) process is a high-speed molding technology that can manufacture high-quality CFRP (Carbon Fiber Reinforced Plastic) parts. Compared to the autoclave process, it generates less waste and can significantly reduce cycle time, so various studies are being conducted in the aerospace and automobile industries. In this study, in order to improve the quality of the PCM process, a molding method was developed to increase the compression pressure of the press step by step according to the curing behavior of the prepreg. It was confirmed that this multi-stage compression molding technology is a good means to produce high-quality CFRP products and shorten cycle times. And, the laminated prepreg at room temperature was immediately put into the mold and preheated and molded at the same time, so that it could be molded without a separate preheating process. In addition, as a result of applying the same process conditions optimized for flat plate molding to three-dimensional shapes, a product similar to a flat plate in appearance could be made without the process of establishing process conditions.

Surface Modification of Nano Silica Prepared by Sol-gel Process and Subsequent Application towards Gas-barrier Films (졸-겔 공정으로 제조한 나노 실리카의 표면개질 및 가스차단성 필름으로의 응용)

  • Jang, Hyo Jun;Chang, Mi Jung;Nam, Kwang Hyun;Chung, Dae-won
    • Applied Chemistry for Engineering
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    • v.30 no.1
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    • pp.68-73
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    • 2019
  • We prepared hydrophobic silica particles by a sol-gel process from tetraethyl orthosilicate (TEOS), followed by coupling the reaction with octyltrimethoxysilane (OTMS) or hexadecyltrimethoxysilane (HDTMS) under various reaction conditions. We confirmed the extent of silica surface modification with organic compounds by SEM-EDS, thermogravimetry and elemental analysis. The silica particles obtained after the hydrolysis reaction of TEOS in ethanol at $50^{\circ}C$ for 24 h and the coupling reaction with OTMS for 2 h at the same temperature displayed the optimum performance in terms of the dispersity in an organic solvent and the surface roughness of films composited with epoxy resins. The oxygen permeability of the composite film with modified-silica was 12% lower than that of using the film without modified-silica.

Development of Curing Process for EMC Encapsulation of Ultra-thin Semiconductor Package (초박형 반도체 패키지의 EMC encapsulation을 위한 경화 공정 개발)

  • Park, Seong Yeon;On, Seung Yoon;Kim, Seong Su
    • Composites Research
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    • v.34 no.1
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    • pp.47-50
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    • 2021
  • In this paper, the Curing process for Epoxy Molding Compound (EMC) Package was developed by comparing the performance of the EMC/Cu Bi-layer package manufactured by the conventional Hot Press process system and Carbon Nanotubes (CNT) Heater process system of the surface heating system. The viscosity of EMC was measured by using a rheometer for the curing cycle of the CNT Heater. In the EMC/Cu Bi-layer Package manufactured through the two process methods by mentioned above, the voids inside the EMC was analyzed using an optical microscope. In addition, the interfacial void and warpage of the EMC/Cu Bi-layer Package were analyzed through C-Scanning Acoustic Microscope and 3D-Digital Image Correlation. According to these experimental results, it was confirmed that there was neither void in the EMC interior nor difference in the warpage at room temperature, the zero-warpage temperature and the change in warpage.