• Title/Summary/Keyword: Direct extraction Method

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고상미량추출장치(SPME)를 이용한 유류 오염 지하수 평가 기법 연구

  • 조현정;백기태;박지연;양지원
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2001.09a
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    • pp.148-150
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    • 2001
  • Solid-phase microextraction (SPME) was investigated to understand the BTEX extraction behavior of SPME in groundwater. Analytical procedure was conducted In both conventional and headspace mode. And the conventional direct extraction method and the headspace analysis method were compared. Data obtained with direct and headspace SPME were very similar and showed successful results. In headspace analysis, the linearity was better and RSD (relative standard deviation, %) was smaller than direct extraction.

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Direct identification of aeroelastic force coefficients using forced vibration method

  • Herry, Irpanni;Hiroshi, Katsuchi;Hitoshi, Yamada
    • Wind and Structures
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    • v.35 no.5
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    • pp.323-336
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    • 2022
  • This study investigates the applicability of the direct identification of flutter derivatives in the time domain using Rational Function Approximation (RFA), where the extraction procedure requires either a combination of at least two wind speeds or one wind speed. In the frequency domain, flutter derivatives are identified at every wind speed. The ease of identifying flutter derivatives in the time domain creates a paradox because flutter derivative patterns sometimes change in higher-order polynomials. The first step involves a numerical study of RFA extractions for different deck shapes from existing bridges to verify the accurate wind speed combination for the extraction. The second step involves validating numerical simulation results through a wind tunnel experiment using the forced vibration method in one degree of freedom. The findings of the RFA extraction are compared to those obtained using the analytical solution. The numerical study and the wind tunnel experiment results are in good agreement. The results show that the evolution pattern of flutter derivatives determines the accuracy of the direct identification of RFA.

Comparison of Preparation Methods for the Quantification of Ginsenosides in Raw Korean Ginseng

  • Hong, Hee-Do;Sim, Eun-Mi;Kim, Kyung-Tack;Rho, Jeong-Hae;Rhee, Young-Kyung;Cho, Chang-Won
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.565-569
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    • 2009
  • This study was conducted to evaluate the effects of different preparation methods on the recovery and quantification of ginsenosides in raw Korean ginseng (Panax ginseng C.A. Meyer). Eight major ginsenosides ($Rb_1$, $Rb_2$, $Rb_3$, Rc, Rd, Re, Rf, and $Rg_1$) were analyzed by high performance liquid chromatography (HPLC), after which the recovery and repeatability of the extraction of those ginsenosides using 3 different preparation methods were compared [A. direct extraction (DE) method, hot MeOH extraction/evaporation/direct dissolution; B. solid phase extraction (SPE) method, hot MeOH extraction/evaporation/dissolution/$C_{18}$ cartridge adsorption/MeOH elution; C. liquid-liquid extraction (LLE) method, hot MeOH extraction/evaporation/dissolution/n-BuOH fractionation]. Use of the DE method resulted in a significantly higher recovery of total ginsenosides than other methods and a relatively clear peak resolution. Use of the SPE and LLE methods resulted in clearer peak resolution, but lower ginsenoside recovery than the DE method. The LLE method showed the lowest ginsenoside recovery and repeatability among the 3 methods. Given that the DE method employed only extraction, evaporation, and a dissolution step (avoiding complicate and time consuming purification), this technique may be an effective method for the preparation and quantification of ginsenosides from raw Korean ginseng.

A Study on the Effective Scattering Center Analysis for Radar Cross Section Reduction of Complex Structures (복합구조물의 RCS 저감을 위한 효율적 산란중심 해석에 관한 연구)

  • Kim, Kook-Hyun;Kim, Jin-Hyeong;Cho, Dae-Seung
    • Journal of the Society of Naval Architects of Korea
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    • v.42 no.4 s.142
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    • pp.421-426
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    • 2005
  • Scattering center extraction schemes for radar cross section reduction of large complex targets, like warships, was developed, which are an 1-D radar image method(range profile), and a direct analysis based on an object precision method. The analysis result of partial dihedral model shows that the presented direct analysis method is more efficient than the 1-D radar image method for scattering center extraction of interested targets, in terms of radar cross section reduction design, not signal processing. In order to verify the accuracy of the direct analysis method, a scattering center analysis of an naval weapon system was carried out, and the result was coincident with that of another well-known RCS analysis program. Finally, an analysis result of RCS and its scattering center of an 120m class warship-like model presented that the direct analysis method can be an efficient and powerful tools for radar cross section reduction of large complex targets.

Analysis of Effective Gate resistance characteristics in Nano-scale MOSFET for RFIC (RFIC를 위한 Nano-scale MOSFET의 Effective gate resistance 특성 분석)

  • 윤형선;임수;안정호;이희덕
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.41 no.11
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    • pp.1-6
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    • 2004
  • Effective gate resistance, extracted by direct extraction method, is analyzed among various gate length, in nanoscale MOSFET for RFIC. Extracted effective gate resistance is compared to measured data and verified with simplified model. Extracted parameters are accurate to 10GHz. In the same process technology effect has a different kind of gate voltage dependency and frequency dependency compared with general effective gate resistance. Particularly, the characteristic of effective gate resistance before and after threshold voltage is noticeable. When gate voltage is about threshold voltage, effective gate resistance is abnormally high. This characteristic will be an important reference for RF MOSFET modeling using direct extraction method.

Three-phase Four-wire Series Active Power Filter Control Strategy for The Compensation of Harmonics and Reactive Power Based-on Direct Compensating Voltage Extraction Method (직접 보상전압 추출기법을 이용하여 고조파전류와 무효전력을 보상하는 3상 4선식 직렬 형 능동전력필터의 제어법)

  • 김진선;김영석
    • The Transactions of the Korean Institute of Power Electronics
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    • v.9 no.3
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    • pp.213-221
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    • 2004
  • In recent years, since more and more diode rectifiers with smoothing dc capacitor are used in electronic equipments, household appliances and ac drives, harmonics generated by these loads have become a major issue. In addition, 3-phase 4-wire system is widely employed in distributing electric energy to several office building and manufacturing plants. This systems show excessive currents in the neutral. These neutral currents are fundamentally third harmonic, and their presence is tied to wiring failure, elevating of neutral potentials, transformer overheating, etc. In response to the concerns, this paper proposes a series active power filter scheme based on direct compensating voltage extraction method and the advantage of this control algorithm is direct extraction of compensation voltage reference without multiplying gain. Therefore, the calculation of the compensation voltage reference will becom much simpler than other control algorithm. To verify the effectiveness of the proposed algorithm, a prototype active power filter is built and some experiments are carried out.

Effect of Pretreatment Method on Lipid Extraction from Enteromorpha intestinalis (해조류 파래로부터 지질 추출에 미치는 전처리 방법의 영향)

  • Jeong, Gwi-Taek;Park, Don-Hee
    • KSBB Journal
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    • v.29 no.1
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    • pp.22-28
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    • 2014
  • In this study, we investigate the effect of pretreatment method on lipid extraction from Enteromorpha intestinalis using physical, thermo-chemical, and enzymatic process such as ultrasonication, high temperature treatment, freezing, microwave irradiation, osmotic shock, pH shock, homogenizing, and enzymatic treatment. In pretreatment with separated lipid extraction, the high extraction yield was obtained by high temperature treatment ($121^{\circ}C$ for 5 min) with 0.1 N HCl, which is 1.4 times higher than that of control. In pretreatment with direct lipid extraction, the high extraction yields were obtained by 0.1 N HCl pretreatment, microwave irradiation (700W, 1 min with twice), and 10% NaCl pretreatment, which is 1.45 times higher than that of control. In the result of enzymatic pretreatment with 17 kinds of enzymes, Cellic CTec II showed the high extraction yield of 5.3%, and which is 1.9 times higher than that of control. Moreover, the extraction yield was increased by the increase of enzyme amounts. In 10% enzyme amount, about 5.8% yield was obtained.

Direct Extraction of DNA from Soil for Amplification of 16S rRNA Gene Sequences by Polymerase Chain Reaction

  • Cho, Jae-Chang;Lee, Dong-Hun;Cheol, Cho-Young;Cho, Jang-Cheon;Kim, Sang-Jong
    • Journal of Microbiology
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    • v.34 no.3
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    • pp.229-235
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    • 1996
  • Microgram quantities of DNA per gram soil were recovered with SDS- based and freeze-and thaw procedures. The average DNA fragment size was > 23 Kb. This method generated minimal shearing of extracted DNA. However, the DNA extracts still contained considerable amounts of humic impurities sufficient to inhibit PCR. Several approaches were used to reduce the interferences with the PCR (use of CTAF in extraction step, Elutip-d column purification, addition of BSA to PCR buffer) to accomplish PCR with DNA extract as a template. Most of the DNA extracts were not digested completely by restriction endonuclease, and CTAB-TREATED ane Elutip-d column purified DNA extracts were partially digested. Regarding as restriction enzyme digestion, all PCRs failed to amplify 16S rRNA gene fragments in the DNA extracts. In the case of DNA extracts only where BSA was added to PCR buffer, PCR was successfully conducted whether the DNA extracts were treated with CTAB or purified with columns. However, these two treatments were indispensable for humic impurity-rich DNA extracts to generate the PCR-compatible DNA samples. Direct extraction of DNA, coupled with these procedures to remove and relieve interferences by humic impurities and followed by the PCR, can be rapid and simple method for molecular microbiological study on soil microorganisms.

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Scalable HBT Modeling using Direct Extraction Method of Model Parameters (파라메터 직접 추출법을 이용한 스케일 가능한 HBT의 모델링)

  • Suh Youngsuk
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.9 no.2
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    • pp.316-321
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    • 2005
  • A new HBT current source model and the corresponding direct parameter extraction methods are presented. Exact analytical expressions for the current source model parameters are derived. This method is applied to scalable modeling of HBT, Some techniques to reduce redundancy of the parameters are introduced. The model based on this method can accurately predict the measured data for the change of ambient temperature, size, and bias.

Equivalent Circuit Model Parameter Extraction for Packaged Bipolar Transistors (패키지된 바이폴라 트랜지스터의 등가회로 모델 파라미터 추출)

  • Lee Seonghearn
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.41 no.12
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    • pp.21-26
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    • 2004
  • In this paper, a direct method is developed to extact RF equivalent circuit of a packaged BJT without optimization. First, parasitic components of plastic package are removed from measured S-parameters using open and short package patterns. Using package do-embedded S-parameters, a direct and simple method is proposed to extract bonding wire inductance and chip pad capacitance between package lead and chip pad. The small-signal model parameters of internal BJT are next determined by Z and Y-parameter formula derived from RF equivalent circuit. The modeled S-parameters of packaged BJT agree well with measured ones, verifying the accuracy of this new extraction method.