• 한국재료학회지
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• 제20권6호
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• pp.319-325
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• 2010

3-D IC integration enables the smallest form factor and highest performance due to the shortest and most plentiful interconnects between chips. Direct metal bonding has several advantages over the solder-based bonding, including lower electrical resistivity, better electromigration resistance and more reduced interconnect RC delay, while high process temperature is one of the major bottlenecks of metal direct bonding because it can negatively influence device reliability and manufacturing yield. We performed quantitative analyses of the interfacial properties of Al-Al bonds with varying process parameters, bonding temperature, bonding time, and bonding environment. A 4-point bending method was used to measure the interfacial adhesion energy. The quantitative interfacial adhesion energy measured by a 4-point bending test shows 1.33, 2.25, and $6.44\;J/m^2$ for 400, 450, and $500^{\circ}C$, respectively, in a $N_2$ atmosphere. Increasing the bonding time from 1 to 4 hrs enhanced the interfacial fracture toughness while the effects of forming gas were negligible, which were correlated to the bonding interface analysis results. XPS depth analysis results on the delaminated interfaces showed that the relative area fraction of aluminum oxide to the pure aluminum phase near the bonding surfaces match well the variations of interfacial adhesion energies with bonding process conditions.

• Tribology and Lubricants
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• 제26권1호
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• pp.14-20
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• 2010

Tribological properties of nanoporous structured alumina film was investigated. Alumina film (AAO: anodic aluminum oxide) of $60{\mu}m$ thickness having nanopores of 45 nm diameter with 105 nm interpore-diatance was fabricated by mild anodization process. Reciprocating ball-on-flat sliding friction tests using 1 mm diameter steel ball as a counterpart were carried out with wide range of normal load from 1 mN to 1 N in an ambient environment. The morphology of worn surfaces were analyzed using scanning electron microscopy. The friction coefficient was strongly influenced by the applied normal load. Smooth layer patches were formed on the worn surface of both AAO and steel ball at relatively high load (100 mN and 1 N) due to tribochemical reaction and compaction of wear debris. These tribolayers contributed to the lower friction at high loads. Extremely thin layer patches, due to mild plastic deformation of surface layer, were sparsely distributed on the worn surface of AAO at low loads (1 mN and 10 mN) without the evidence of tribochemical reaction. Delaminated wear particles were generated at high loads by fatigue due to repeated loading and sliding.

• The Journal of Advanced Prosthodontics
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• 제3권4호
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• pp.221-228
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• 2011

PURPOSE. Veneering porcelain might be delaminated from underlying zirconia-based ceramics. The aim of this study was the evaluation of the effect of different surface treatments and type of zirconia (white or colored) on shear bond strength (SBS) of zirconia core and its veneering porcelain. MATERIALS AND METHODS. Eighty zirconia disks (40 white and 40 colored; 10 mm in diameter and 4 mm thick) were treated with three different mechanical surface conditioning methods (Sandblasting with $110{\mu}m$ $Al_2O_3$ particle, grinding, sandblasting and liner application). One group had received no treatment. These disks were veneered with 3 mm thick and 5 mm diameter Cercon Ceram Kiss porcelain and SBS test was conducted (cross-head speed = 1 mm/min). Two and one way ANOVA, Tukey's HSD Past hoc, and T- test were selected to analyzed the data (${\alpha}=0.05$). RESULTS. In this study, the factor of different types of zirconia ceramics (P=.462) had no significant effect on SBS, but the factors of different surface modification techniques (P=.005) and interaction effect (P=.018) had a significant effect on SBS. Within colored zirconia group, there were no significant differences in mean SBS among the four surface treatment subgroups (P=0.183). Within white zirconia group, "Ground group" exhibited a significantly lower SBS value than "as milled" or control (P=0.001) and liner (P=.05) groups. CONCLUSION. Type of zirconia did not have any effect on bond strength between zirconia core and veneer ceramic. Surface treatment had different effects on the SBS of the different zirconia types and grinding dramatically decreased the SBS of white zirconia- porcelain.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집A
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• pp.250-255
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• 2000

Damage induced by low velocity impact loading in aircraft composite laminates is the form of failure which is occurred frequently in aircraft. Low velocity impact can be caused either by maintenance accidents with tool drops or by in-flight impacts with debris. As the consequences of impact loading in composite laminates, matrix cracking, delamination and eventually fiber breakage for higher impact energies can be occurred. Even when no visible impact damage is observed, damage can exist inside of composite laminates and the carrying load of the composite laminates is considerably reduced. The reduction of strength and stiffness by impact loading occurs in compressive loading due to laminate buckling in the delaminated areas. The objective of this study is to determine inside damage of composite laminates by impact loading and to determine residual compressive strength and the damage growth mechanisms of impacted composite laminates. For this purpose a series of impact and compression after impact tests are carried out on composite laminates made of carbon fiber reinforced epoxy resin matrix with lay up pattern of $[({\pm}45)(0/90)_2]s$ and $[({\pm}45)(0)_3(90)(0)_3({\pm}45)]$. UT-C scan is used to determine impact damage characteristics and CAI(Compression After Impact) tests are carried out to evaluate quantitatively reduction of compressive strength by impact loading.

• 마이크로전자및패키징학회지
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• 제27권2호
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• pp.19-26
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• 2020

Flexible displays have been evolved into curved, foldable, and rollable as the degree of bending increases. Due to the presence of brittle electrodes (e.g. indium-tin oxide (ITO)) that easily cracked and delaminated under severe bending deformation, lowering mechanical stress of the electrodes has been critical issue. Because of this, mechanical stress of brittle electrode in flexible displays has been analyzed mostly in terms of bending radius. On the other hand, in order to make rollable display, various mechanical components such as roller and spring are needed to roll-up or extend the screen for the rollable display apparatus. By these mechanical components, brittle electrode in the rollable display is subjected to the excessive tensile stress due to the retracting force as well as the bending stress by the roller. In this study, mechanical deformation of rollable OLED display was modeled considering boundary conditions of the apparatus. An analytical modeling based on the classical beam theory was introduced in order to investigate the mechanical behavior of the rollable display. In addition, finite element analysis (FEA) was used to analyze the effect of mechanical components in the apparatus on the brittle electrode. Furthermore, a strategy for improving the mechanical reliability of the rollable display was suggested through controlling the stiffness of adhesives in the display panel.

• 한국광학회지
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• 제26권5호
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• pp.261-264
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• 2015

본 논문에서는 인쇄회로기판의 감광층 보호필름을 532 nm 파장의 나노초 레이저의 단일펄스로 박리할 수 있음을 보여준다. 인쇄회로기판의 가장자리를 9 mm 크기의 레이저 빔으로 국부적으로 박리시킨 후 스카치테이프를 레이저 조사에 의해 초기 박리 된 영역에 붙여 전체 보호필름을 떼어내었는데, 160 - 170 mJ의 펄스에너지 범위에서는 10회의 반복된 실험 모두에서 감광층 손상 없는 박리에 성공하였다. 보호필름 초기 박리에 레이저를 사용하는 방식은 기계적 압착에 바탕을 둔 기존의 널링방식과는 달리 감광층에 손상을 유발하지 않는 비접촉 방식으로써, 인쇄회로기판 제조공정에 보다 효율적으로 사용될 수 있을 것으로 판단된다.

• 한국세라믹학회지
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• 제51권6호
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• pp.598-604
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• 2014

Considerable research efforts have been explored attempting to enhance the thermal durability of thermal barrier coatings (TBCs) at the high operating temperatures of gas turbines. In this study, the suspension plasma spray (SPS) process was applied to produce TBCs with a segmented structure by using an yttria-stabilized zirconia (YSZ) suspension. Four different experiment sets were carried out by controlling the ratio between surface roughness of the bond coat and feed stock size ($R_a/D_{50}$) in order to examine the effect of $R_a/D_{50}$ ratio on the microstructure of SPS-prepared coatings. When the $R_a/D_{50}$ had a high value of 11.8, a deposited thick coating turned out to have a cone-type columnar microstructure. In contrast, at the low $R_a/D_{50}$ values of 2.9 and 0.18, a deposited thick coating appeared to have a dense, vertically-cracked microstructure. However, with the very low $R_a/D_{50}$ value of 0.05 the coating was delaminated.

• 한국재료학회지
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• 제21권11호
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• pp.596-603
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• 2011

The very high temperature gas reactor (VHTR) is one of the next generation nuclear reactors for its safety, long-term stability, and proliferation-resistance. The high operating temperature of over 800$^{\circ}C$ enables various applications with high energy efficiency. Heat is transferred from the primary helium loop to the secondary helium loop through the intermediate heat exchanger (IHX). The IHX material requires creep resistance, oxidation resistance, and corrosion resistance in a helium environment at high operating temperatures. A Ni-based superalloy such as Alloy 617 is considered as a primary candidate material for the intermediate heat exchanger. In this study, the microstructures of Alloy 617 crept in pure helium and air environments at 950$^{\circ}C$ were observed. The rupture time in helium was shorter than that in air under small applied stresses. As the exposure time increased, the thickness of outer oxide layer of the specimens clearly increased but delaminated after a long creep time. The depth of the carbide-depleted zone was rather high in the specimens under high applied stress. The reason was elucidated by the comparison between the ruptured region and grip region of the samples. It is considered that decarburization caused by minor gas impurities in a helium environment caused the reduction in creep rupture time.

• 대한기계학회논문집A
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• 제28권2호
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• pp.174-180
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• 2004

If Fiber Reinforced Metal Laminates(FRMLs) were delaminated, the decrease of stiffness and fiber bridging effect would result in the sudden aggravation of fatigue characteristics. It was reported that the delamination of FRMLs resulted from the crack of metal layers and that it depended on the crack growth. While cracks were made in FRMLs containing a saw-cuts under fatigue loading, cracks could be produced or not in FRMLs with circular holes under the same condition. When the FRMLs with the circular holes produce not the crack but the delamination, it is not possible to analyze it by the conventional fracture parameters expressed as the function of the crack. And so, this research suggests a new analytical model of the delamination to make the comparison of the delamination behavior possible whenever the cracks occur or not. Therefore, a new analytical model called Pseudo Crack Model(PCM) was suggested to compare the delaminations whether cracks were made or not. The relationship between the crack energy consumption rate( $E_{crack}$) and the delamination energy consumption rate( $E_{del}$) was discussed and it was also known that the effect of $E_{del}$ was larger than that of $E_{crack}$.

• Smart Structures and Systems
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• 제28권6호
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• pp.745-760
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• 2021

Dynamic buckling of structure is one of the failure modes that needs to be considered since it may result in catastrophic failure of the structure in a short period of time. For a thin fiber-reinforced polymer (FRP) plate under compression, buckling is an inherent hazard which will be intensified by the existence of defects like holes, cracks, and delamination. On the other hand, the growth of the delamination is another prime concern for thin FRP plates. In the current paper, reinforcing the plates against buckling is realized by using SMA wires in the form of stitches. A numerical framework is proposed to simulate the dynamic instability emphasizing the effect of the SMA stitches in suppressing delamination growth. The suggested algorithm is more accurate than the other methods when considering the transformation point of the SMA wires and the modeling of the cohesive zone using simple and yet reliable technique. The computational design of the method by producing the line by line orders leads to a simple algorithm for simulating the super-elastic behavior. The Lagoudas constitutive model of the SMA material is implemented in the form of user material subroutines (VUMAT). The normal bilinear spring model is used to reproduce the cohesive zone behavior. The nonlinear finite element formulation is programmed into FORTRAN using the Newmark-beta numerical time-integration approach. The obtained results are compared with the results obtained by the finite element method using ABAQUS/Explicit solver. The obtained results by the proposed algorithm and those by ABAQUS are in good agreement.